appendix laboratory analytical results · 99-193 aiea heights drive, suite 121 aiea, hi 96701 *...

APPENDIX B Laboratory Analytical Results

Bulk Material Analytical Results

99-193 Aiea Heights Drive, Suite 121 Aiea, HI 96701 * 808-486-5227 * Fax 808-486-2456

March 05, 2010

Client:

Attn:

Work Order:

Project Name:

Project Number:

Date Received:

PVT Landfill

[none]

HTB0121

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report were

performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless otherwise noted

in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This report shall not be

reproduced, except in full, without written permission from TestAmerica.

TestAmerica Analytical Testing Corporation certifies that the analytical results contained herein apply only to the specific sample(s) analyzed.

The Chain(s) of Custody, 2 pages, are included and are an integral part of this report. This entire report was reviewed and approved for

release.

If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at 1-(808)486-5227

02/22/10

Waianae, HI 96792

PVT Land Company

87-2020 Farrington Hwy.

Steve Joseph

LABORATORY REPORT

Case Narrative: Two buckets of wood, plastic, waste and other material were provided by client. Three samples were collected

by TestAmerica Honolulu from the material for the analyses following the composition details provided by client, to the best

possible and with the best representative material.

SPLP Pentachlorophenol and SPLP RCRA8 were added for all samples by phone after the COC was submitted.

Mercury was detected in the SPLP method blank and the SPLP client sample at a similar level. It is possible that the mercury

hit found in the client sample was contributed from contamination similar to the associated method blank.

syl 3/5/10

Samples were received into laboratory at a temperature of 25 °C.

NELAC states that samples which require thermal preservation shall be considered acceptable if the arrival temperature is within

2 degrees C of the required temperature or the method specified range. For samples with a temperature requirement of 4 degrees C,

an arrival temperature from 0 degrees C to 6 degrees C meets specifications. Samples that are delivered to the laboratory on the

same day that they are collected may not meet these criteria. In these cases, the samples are considered acceptable if there is

evidence that the chilling process has begun, such as arrival on ice.

The reported results were obtained in compliance with the 2003 NELAC standards unless otherwise noted.

Approved By:

Project Manager

Samuel A. Lui

NELAC Certification # E87907

Page 1 of 9


Waianae, HI 96792 Project:

Work Order:

PVT Landfill

HTB0121 Received:

Project Number: [none]

02/22/10PVT Land Company


Steve Joseph

Reported: 03/05/10 13:53

SAMPLE IDENTIFICATION LAB NUMBER COLLECTION DATE AND TIME

HTB0121-01222-01 02/22/10 12:00

HTB0121-02222-02 02/22/10 12:00

HTB0121-03222-03 02/22/10 12:00

Page 2 of 9



Work Order:

PVT Landfill

HTB0121 Received:




Steve Joseph

Reported: 03/05/10 13:53

ANALYTICAL REPORT

Analyte

Data

QualifiersSample

Result UnitsSeq/

Batch

Prep

DateDil Method

Date

AnalyzedRpt Limit

Sample ID: HTB0121-01 (222-01 - Solid/Soil) Sampled: 02/22/10 12:00 Recvd: 02/22/10 14:50

SPLP Metals

0.200ND 1 SW1312/6010B02/24/10 16:19 02/24/10mg/L 10B0182Arsenic

0.200ND " "" "" "Barium

0.0500ND " "" "" "Cadmium

0.0500ND " "" "" "Chromium

0.0500ND " "" "" "Lead

B 0.0001250.000500 " SW1312/747002/25/10 15:27 02/25/10" 10B0197Mercury

0.200ND " SW1312/6010B02/24/10 16:19 02/24/10" 10B0182Selenium

0.100ND " "" "" "Silver

TCLP Mercury per EPA 7000 Series Methods

0.00250ND 1 SW1311/747002/23/10 17:31 02/23/10mg/L 10B0174Mercury

TCLP Metals


5.00ND " "" "" "Barium

0.0500ND " "" "" "Cadmium

0.100ND " "" "" "Chromium

0.200ND " "" "" "Lead

0.500ND " "" "" "Selenium

0.300ND " "" "" "Silver

Total Metals by SW 846 Series Methods

11.0233 10 SW6010B02/24/10 19:13 02/24/10mg/kg 10B0183Arsenic

22.0ND " "" "" "Barium

11.0ND " "" "" "Cadmium

11.0299 " "" "" "Chromium

22.031.6 " "" "" "Lead

0.005000.0477 1 SW747102/24/10 15:53 "" 10B0179Mercury

22.0ND 10 SW6010B02/24/10 19:13 "" 10B0183Selenium

11.0ND " "" "" "Silver


SPLP Metals


0.200ND " "" "" "Barium

0.0500ND " "" "" "Cadmium

0.05000.0630 " "" "" "Chromium

0.0500ND " "" "" "Lead

B 0.0001250.000550 " SW1312/747002/25/10 15:33 02/25/10" 10B0197Mercury

0.200ND " SW1312/6010B02/24/10 16:29 02/24/10" 10B0182Selenium

0.100ND " "" "" "Silver



TCLP Metals


5.00ND " "" "" "Barium

0.0500ND " "" "" "Cadmium


Page 3 of 9



Work Order:

PVT Landfill

HTB0121 Received:




Steve Joseph

Reported: 03/05/10 13:53

ANALYTICAL REPORT

Analyte

Data

QualifiersSample

Result UnitsSeq/

Batch

Prep

DateDil Method

Date

AnalyzedRpt Limit

Sample ID: HTB0121-02 (222-02 - Solid/Soil) - cont. Sampled: 02/22/10 12:00 Recvd: 02/22/10 14:50

TCLP Metals - cont.

0.200ND " "" "" "Lead


0.300ND " "" "" "Silver



19.820.4 " "" "" "Barium

9.91ND " "" "" "Cadmium

9.91148 " "" "" "Chromium

19.8ND " "" "" "Lead

0.005000.0385 1 SW747102/24/10 15:54 "" 10B0179Mercury

19.8ND 10 SW6010B02/24/10 19:17 "" 10B0183Selenium

9.91ND " "" "" "Silver


SPLP Metals


0.200ND " "" "" "Barium

0.0500ND " "" "" "Cadmium

0.0500ND " "" "" "Chromium

0.0500ND " "" "" "Lead

B 0.0001250.000650 " SW1312/747002/25/10 15:34 02/25/10" 10B0197Mercury

0.200ND " SW1312/6010B02/24/10 16:34 02/24/10" 10B0182Selenium

0.100ND " "" "" "Silver



TCLP Metals


5.00ND " "" "" "Barium

0.0500ND " "" "" "Cadmium


0.200ND " "" "" "Lead


0.300ND " "" "" "Silver



20.3ND " "" "" "Barium

10.1ND " "" "" "Cadmium

10.1161 " "" "" "Chromium

20.3ND " "" "" "Lead

0.005000.0613 1 SW747102/24/10 15:55 "" 10B0179Mercury

20.3ND 10 SW6010B02/24/10 19:22 "" 10B0183Selenium

10.1ND " "" "" "Silver

Page 4 of 9



Work Order:

PVT Landfill

HTB0121 Received:




Steve Joseph

Reported: 03/05/10 13:53

LABORATORY BLANK QC DATA

Analyte ResultUnits

Spike

LevelDup

Result

%

REC

Dup

%REC

% REC

Limits RPD

RPD

Limit Q

Source

Result MDL MRL

SPLP Metals

Batch\Seq: 10B0182 Extracted: 02/24/10

Blank Analyzed: 02/24/2010 (10B0182-BLK1)

ND0.200N/Amg/LArsenic

ND0.200N/Amg/LBarium

ND0.0500N/Amg/LCadmium

ND0.0500N/Amg/LChromium

0.06970.0500N/Amg/LLead A-01,B

ND0.200N/Amg/LSelenium

ND0.100N/Amg/LSilver



0.0002500.000125N/Amg/LMercury B




ND0.00250N/Amg/LMercury


ND0.00250N/Amg/LMercury

TCLP Metals




ND5.00N/Amg/LBarium



ND0.200N/Amg/LLead





ND5.00N/Amg/LBarium



ND0.200N/Amg/LLead






ND0.00500N/Amg/kgMercury



ND1.00N/Amg/kgArsenic

ND2.00N/Amg/kgBarium

Page 5 of 9



Work Order:

PVT Landfill

HTB0121 Received:




Steve Joseph

Reported: 03/05/10 13:53

LABORATORY BLANK QC DATA

Analyte ResultUnits

Spike

LevelDup

Result

%

REC

Dup

%REC

% REC

Limits RPD

RPD

Limit Q

Source

Result MDL MRL




ND1.00N/Amg/kgCadmium

ND1.00N/Amg/kgChromium

ND2.00N/Amg/kgLead

ND2.00N/Amg/kgSelenium

ND1.00N/Amg/kgSilver

Page 6 of 9



Work Order:

PVT Landfill

HTB0121 Received:




Steve Joseph

Reported: 03/05/10 13:53

LCS/LCS DUPLICATE QC DATA

Analyte ResultUnits

Spike

LevelDup

Result

%

REC

Dup

%REC

% REC

Limits RPD

RPD

Limit Q

Source

Result MDL MRL

SPLP Metals


LCS Analyzed: 02/24/2010 (10B0182-BS1)

80-12020.0 10020.00.200N/Amg/LArsenic

80-12020.0 9819.50.200N/Amg/LBarium

80-12020.0 9719.50.0500N/Amg/LCadmium

80-12020.0 9719.50.0500N/Amg/LChromium

80-12020.0 9218.30.0500N/Amg/LLead

80-12020.0 10120.30.200N/Amg/LSelenium

80-1202.00 1002.010.100N/Amg/LSilver


LCS Analyzed: 02/25/2010 (10B0197-BS1)

80-1200.0100 1010.01010.000125N/Amg/LMercury



LCS Analyzed: 02/23/2010 (10B0174-BS1)

80-1200.0100 990.009900.00250N/Amg/LMercury

TCLP Metals


LCS Analyzed: 02/23/2010 (10B0169-BS1)

80-12020.0 10521.00.500N/Amg/LArsenic

80-12020.0 10019.95.00N/Amg/LBarium

80-12020.0 8917.90.0500N/Amg/LCadmium

80-12020.0 9519.00.100N/Amg/LChromium

80-12020.0 10621.30.200N/Amg/LLead

80-12020.0 10721.40.500N/Amg/LSelenium

80-1202.00 901.800.300N/Amg/LSilver



LCS Analyzed: 02/24/2010 (10B0179-BS1)

80-1200.524 1020.5370.0500N/Amg/kgMercury


LCS Analyzed: 02/24/2010 (10B0183-BS1)

80-120100 10110110.0N/Amg/kgArsenic

80-120100 10110120.0N/Amg/kgBarium

80-120100 10210210.0N/Amg/kgCadmium

80-120100 9898.310.0N/Amg/kgChromium

80-120100 9594.620.0N/Amg/kgLead

80-120100 10010020.0N/Amg/kgSelenium

80-12010.0 979.6510.0N/Amg/kgSilver

Page 7 of 9



Work Order:

PVT Landfill

HTB0121 Received:




Steve Joseph

Reported: 03/05/10 13:53

MATRIX SPIKE/MATRIX SPIKE DUPLICATE QC DATA

Analyte ResultUnits

Spike

LevelDup

Result

%

REC

Dup

%REC

% REC

Limits RPD

RPD

Limit Q

Source

Result MDL MRL

SPLP Metals

Batch\Seq: 10B0182 Extracted: 02/24/10 QC Source Sample: HTB0121-01Matrix Spike Analyzed: 02/24/2010 (10B0182-MS1)

2080-12020.0 101 620.2 9519.0ND 0.200N/Amg/LArsenic

2080-12020.0 98 619.7 9218.60.104 0.200N/Amg/LBarium

2080-12020.0 99 419.7 9518.9ND 0.0500N/Amg/LCadmium

2080-12020.0 98 519.6 9318.6ND 0.0500N/Amg/LChromium

2080-12020.0 92 518.4 8817.5ND 0.0500N/Amg/LLead

2080-12020.0 103 520.6 9819.5ND 0.200N/Amg/LSelenium

2080-1202.00 97 31.95 941.89ND 0.100N/Amg/LSilver


2075-1250.0100 98 10.0102 980.01030.000500 0.000125N/Amg/LMercury



2075-1250.0100 102 10.0102 1010.0101ND 0.00250N/Amg/LMercury

TCLP Metals


2080-12020.0 108 121.7 10721.50.0593 0.500N/Amg/LArsenic

2080-12020.0 103 121.8 10221.61.26 5.00N/Amg/LBarium

2080-12020.0 93 118.6 9418.70.00660 0.0500N/Amg/LCadmium

2080-12020.0 100 020.0 10020.0ND 0.100N/Amg/LChromium

2080-12020.0 104 020.9 10420.90.0192 0.200N/Amg/LLead

2080-12020.0 107 021.5 10821.5ND 0.500N/Amg/LSelenium

2080-1202.00 92 01.83 911.82ND 0.300N/Amg/LSilver



2075-1250.524 101 10.555 1000.5530.0270 0.0500N/Amg/kgMercury


2080-12098.2 44 2050.0 5561.26.90 9.82N/Amg/kgArsenic M1

2080-12098.2 43 23168 86211125 19.6N/Amg/kgBarium M1,R

2080-12098.2 69 2467.5 8785.8ND 9.82N/Amg/kgCadmium M1,R

2080-12098.2 43 15207 78242165 9.82N/Amg/kgChromium M1

2080-12098.2 75 2676.2 9798.62.43 19.6N/Amg/kgLead M1,R

2080-12098.2 40 1641.1 4748.31.88 19.6N/Amg/kgSelenium M1

2080-1209.82 70 149.58 8411.02.71 9.82N/Amg/kgSilver M1

Page 8 of 9



Work Order:

PVT Landfill

HTB0121 Received:




Steve Joseph

Reported: 03/05/10 13:53

CERTIFICATION SUMMARY

Method Matrix

TestAmerica Honolulu

Nelac Hawaii

XSolid/SoilSW1311/6010B

XSolid/SoilSW1311/7470

Solid/SoilSW1312/6010B

Solid/SoilSW1312/7470

XSolid/SoilSW6010B

XSolid/SoilSW7471

Subcontracted Laboratories

STL - Seattle, WA

5755 8th Street East - Tacoma,, WA 98424

Analysis Performed: 8270D SPLP

Samples: HTB0121-01, HTB0121-02, HTB0121-03

Analysis Performed: 8270D TCLP Semivols

Samples: HTB0121-01, HTB0121-02, HTB0121-03

For information concerning certifications of this facility or another TestAmerica facility, please visit our website at

www.TestAmericaInc.com

DATA QUALIFIERS AND DEFINITIONS

A-01 Samples ND data not impacted

B Analyte was detected in the associated Method Blank.

M1 The MS and/or MSD were outside the acceptance limits due to sample matrix interference. See Blank Spike (LCS).

R The RPD exceeded the method control limit due to sample matrix effects. The individual analyte QA/QC recoveries, however,

were within acceptance limits.

ND Not detected at the reporting limit (or method detection limit if shown)

ADDITIONAL COMMENTS

Page 9 of 9

ANALYTICAL REPORTTestAmerica Laboratories Inc.TestAmerica Seattle5755 8th Street EastTacoma, WA 98424Tel: (253)922-2310

TestAmerica Job ID: 580-17956-1Client Project/Site: HTB0121

For:TestAmerica Laboratories, Inc99-193 Aiea Heights DriveSuite 121Aiea, Hawaii 96701

Attn: Marvin D Heskett III

Authorized for release by:2/26/2010 12:55 PM

Pam JohnsonProject Manager [email protected]

This report has been electronically signed and authorized by thesignatory. Electronic signature is intended to be the legally bindingequivalent of a traditionally handwritten signature.

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mailto:[email protected]

https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/AskTheExpert/Expert_index.htm

http://www.testamericainc.com

Analytical DataTestAmerica Job ID: 580-17956-1Client: TestAmerica Laboratories, Inc

Project/Site: HTB0121

Lab Sample ID: 580-17956-1Client Sample ID: HTB0121-01Matrix: SolidDate Collected: 02/22/10 12:00

Date Received: 02/25/10 09:50

Method: 8270C - Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) - SPLP WestAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac

Pentachlorophenol ND 4.5 ug/L 02/25/10 12:00 02/25/10 15:36 1

Surrogate Qualifier Prepared Analyzed Dil Fac % Recovery Limits

2-Fluorophenol 65 44 - 148 02/25/10 12:00 02/25/10 15:36 1

Phenol-d5 45 02/25/10 12:00 02/25/10 15:36 133 - 147

2,4,6-Tribromophenol 99 02/25/10 12:00 02/25/10 15:36 147 - 158






2-Fluorophenol 76 44 - 148 02/25/10 12:00 02/25/10 15:58 1

Phenol-d5 47 02/25/10 12:00 02/25/10 15:58 133 - 147

2,4,6-Tribromophenol 100 02/25/10 12:00 02/25/10 15:58 147 - 158






2-Fluorophenol 76 44 - 148 02/25/10 12:00 02/25/10 16:19 1

Phenol-d5 42 02/25/10 12:00 02/25/10 16:19 133 - 147

2,4,6-Tribromophenol 99 02/25/10 12:00 02/25/10 16:19 147 - 158

TestAmerica Seattle

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Quality Control DataTestAmerica Job ID: 580-17956-1Client: TestAmerica Laboratories, Inc


Method: 8270C - Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)

Client Sample ID: LCS 580-59037/2-ALab Sample ID: LCS 580-59037/2-A

Matrix: Water Prep Type: Total/NA

Analysis Batch: 59033 Prep Batch: 59037

Analyte

Spike

Added

LCS

Result

LCS

Qualifier Unit % Rec.

% Rec.

Limits

Pentachlorophenol 9.82 9.03 ug/L 92 23 - 166

Surrogate Qualifier % Recovery

LCS LCS

Limits

2-Fluorophenol 65 44 - 148

42Phenol-d5 33 - 147

952,4,6-Tribromophenol 47 - 158

Client Sample ID: MB 580-59025/1-BLab Sample ID: MB 580-59025/1-B

Matrix: Solid Prep Type: SPLP West


Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

MB MB

RL MDL


Surrogate % Recovery Qualifier Prepared Analyzed Dil Fac

MB MB

Limits

2-Fluorophenol 76 44 - 148 02/25/10 12:00 02/25/10 14:54 1

49 02/25/10 12:00 02/25/10 14:54 1Phenol-d5 33 - 147

84 02/25/10 12:00 02/25/10 14:54 12,4,6-Tribromophenol 47 - 158

TestAmerica Seattle

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Lab ChronicleClient: TestAmerica Laboratories, Inc TestAmerica Job ID: 580-17956-1


Client Sample ID: HTB0121-01 Lab Sample ID: 580-17956-1Matrix: SolidDate Collected: 02/22/10 12:00


Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared

Or Analyzed Analyst LabPrep Type

SPLP West Leach 1312 1 59025 02/25/10 11:00 SP TestAmerica Seattle

SPLP West Prep 3510C 1 59037 02/25/10 12:00 SP TestAmerica Seattle

SPLP West Analysis 8270C 1 59033 02/25/10 15:36 CM TestAmerica Seattle



Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared







Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





TestAmerica Seattle

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Certification SummaryTestAmerica Job ID: 580-17956-1Client: TestAmerica Laboratories, Inc


Laboratory Program Certification IDAuthority Expiration DateEPA Region

TestAmerica Seattle L2236DoD ELAP L-A-B 0 01/19/13

TestAmerica Seattle L2236ISO/IEC 17025 L-A-B 0 01/19/13

TestAmerica Seattle WA100007NELAC Primary AB Oregon 10 11/06/09

TestAmerica Seattle 1115CANELAC Secondary AB California 9 01/31/10

TestAmerica Seattle UST-022State Program Alaska 10 03/04/10

TestAmerica Seattle C1226State Program Washington 10 02/17/11

TestAmerica Seattle P330-08-00099USDA 05/22/11

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s

current list of certified methods and analytes.

TestAmerica Seattle

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Method SummaryTestAmerica Job ID: 580-17956-1Client: TestAmerica Laboratories, Inc


Method Method Description LaboratoryProtocol

SW8468270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) TAL TAC

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL TAC = TestAmerica Seattle, 5755 8th Street East, Tacoma, WA 98424, TEL (253)922-2310

TestAmerica Seattle

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Sample SummaryTestAmerica Job ID: 580-17956-1Client: TestAmerica Laboratories, Inc


Lab Sample ID Client Sample ID ReceivedSampledMatrix

580-17956-1 HTB0121-01 Solid 02/22/10 12:00 02/25/10 09:50

580-17956-2 HTB0121-02 Solid 02/22/10 12:00 02/25/10 09:50

580-17956-3 HTB0121-03 Solid 02/22/10 12:00 02/25/10 09:50

TestAmerica Seattle

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Login Sample Receipt Check List

Client: TestAmerica Laboratories, Inc Job Number: 580-17956-1

Login Number: 17956

Question T / F/ NA Comment

Creator: Blankinship, Tom

List Source: TestAmerica Tacoma

List Number: 1

Radioactivity either was not measured or, if measured, is at or below

background

True

The cooler's custody seal, if present, is intact. N/A

The cooler or samples do not appear to have been compromised or

tampered with.

True

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and

the COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in

diameter.

N/A

If necessary, staff have been informed of any short hold time or quick TAT

needs

True

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Is the Field Sampler's name present on COC? N/A

Sample Preservation Verified N/A

TestAmerica Seattle

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2-Fluorophenol 65 44 - 148 02/25/10 12:00 02/25/10 15:36 1

Phenol-d5 45 02/25/10 12:00 02/25/10 15:36 133 - 147

2,4,6-Tribromophenol 99 02/25/10 12:00 02/25/10 15:36 147 - 158






2-Fluorophenol 76 44 - 148 02/25/10 12:00 02/25/10 15:58 1

Phenol-d5 47 02/25/10 12:00 02/25/10 15:58 133 - 147

2,4,6-Tribromophenol 100 02/25/10 12:00 02/25/10 15:58 147 - 158






2-Fluorophenol 76 44 - 148 02/25/10 12:00 02/25/10 16:19 1

Phenol-d5 42 02/25/10 12:00 02/25/10 16:19 133 - 147

2,4,6-Tribromophenol 99 02/25/10 12:00 02/25/10 16:19 147 - 158

TestAmerica Seattle

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Analyte

Spike

Added

LCS

Result

LCS


% Rec.

Limits



LCS LCS

Limits

2-Fluorophenol 65 44 - 148

42Phenol-d5 33 - 147

952,4,6-Tribromophenol 47 - 158


Matrix: Solid Prep Type: SPLP West



MB MB

RL MDL



MB MB

Limits

2-Fluorophenol 76 44 - 148 02/25/10 12:00 02/25/10 14:54 1

49 02/25/10 12:00 02/25/10 14:54 1Phenol-d5 33 - 147

84 02/25/10 12:00 02/25/10 14:54 12,4,6-Tribromophenol 47 - 158

TestAmerica Seattle

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Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared







Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared







Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





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580-17956-1 HTB0121-01 Solid 02/22/10 12:00 02/25/10 09:50

580-17956-2 HTB0121-02 Solid 02/22/10 12:00 02/25/10 09:50

580-17956-3 HTB0121-03 Solid 02/22/10 12:00 02/25/10 09:50

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Login Number: 17956


Creator: Blankinship, Tom


List Number: 1


background

True



tampered with.

True








the COC.

True








MS/MSDs

True


diameter.

N/A


needs

True





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Job Narrative

580-17929-1

Comments

No additional comments.

Receipt

All samples were received in good condition within temperature requirements.

GC/MS Semi VOA - Method 8270C

The continuing calibration verification (CCV) for analytical batch 58958 exceeded control criteria for CCC compound di-n-octylphthalate.

All associated samples are being analyzed for PCP only. PCP passes within 20%D.

Phenol-d5 surrogate recovery was outside control limits for the following sample: 58947/1B MB, 580-17929-3MS, 580-17929-3. The

samples are analyzed for PCP only, so only 2,4,6-TBP surrogate is needed.

No other analytical or quality issues were noted.

General Chemistry

No analytical or quality issues were noted.

Organic Prep


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Method: 8270C - Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) - TCLPAnalyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac

Pentachlorophenol ND 35 ug/L 02/24/10 11:40 02/24/10 16:14 1


2,4,6-Tribromophenol 109 47 - 158 02/24/10 11:40 02/24/10 16:14 1






2,4,6-Tribromophenol 103 47 - 158 02/24/10 11:40 02/24/10 16:35 1






2,4,6-Tribromophenol 99 47 - 158 02/24/10 11:40 02/24/10 16:56 1

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Analyte

Spike

Added

LCS

Result

LCS


% Rec.

Limits



LCS LCS

Limits

2,4,6-Tribromophenol 106 47 - 158


Matrix: Solid Prep Type: TCLP



MB MB

RL MDL



MB MB

Limits

2,4,6-Tribromophenol 83 47 - 158 02/24/10 11:40 02/24/10 15:33 1

Client Sample ID: HTB0121-03Lab Sample ID: 580-17929-3 MS



Analyte

Sample

Result

Sample

Qualifier

Spike

Added

MS

Result

MS


% Rec.

Limits

Pentachlorophenol ND 98.2 117 ug/L 119 23 - 166


MS MS

Limits


Client Sample ID: HTB0121-03Lab Sample ID: 580-17929-3 DU



Analyte

Sample

Result

Sample

Qualifier

DU

Result

DU

Qualifier Unit RPD

RPD

Limit

Pentachlorophenol ND ND ug/L NC 45


DU DU

Limits


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Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared


TCLP Leach 1311 1 58947 02/24/10 11:35 SP TestAmerica Seattle

TCLP Prep 3510C 1 58946 02/24/10 11:40 SP TestAmerica Seattle

TCLP Analysis 8270C 1 58958 02/24/10 16:14 CM TestAmerica Seattle



Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared







Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





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580-17929-1 HTB0121-01 Solid 02/22/10 12:00 02/24/10 08:40

580-17929-2 HTB0121-02 Solid 02/22/10 12:00 02/24/10 08:40

580-17929-3 HTB0121-03 Solid 02/22/10 12:00 02/24/10 08:40

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Login Number: 17929


Creator: Gamble, Cathy


List Number: 1


background

True



tampered with.

True








the COC.

True








MS/MSDs

True


diameter.

N/A


needs

True





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Job Narrative

580-17929-1

Comments

No additional comments.

Receipt

All samples were received in good condition within temperature requirements.

GC/MS Semi VOA - Method 8270C

The continuing calibration verification (CCV) for analytical batch 58958 exceeded control criteria for CCC compound di-n-octylphthalate.

All associated samples are being analyzed for PCP only. PCP passes within 20%D.

Phenol-d5 surrogate recovery was outside control limits for the following sample: 58947/1B MB, 580-17929-3MS, 580-17929-3. The

samples are analyzed for PCP only, so only 2,4,6-TBP surrogate is needed.

No other analytical or quality issues were noted.

General Chemistry


Organic Prep


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2,4,6-Tribromophenol 109 47 - 158 02/24/10 11:40 02/24/10 16:14 1






2,4,6-Tribromophenol 103 47 - 158 02/24/10 11:40 02/24/10 16:35 1






2,4,6-Tribromophenol 99 47 - 158 02/24/10 11:40 02/24/10 16:56 1

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Analyte

Spike

Added

LCS

Result

LCS


% Rec.

Limits



LCS LCS

Limits






MB MB

RL MDL



MB MB

Limits

2,4,6-Tribromophenol 83 47 - 158 02/24/10 11:40 02/24/10 15:33 1

Client Sample ID: HTB0121-03Lab Sample ID: 580-17929-3 MS



Analyte

Sample

Result

Sample

Qualifier

Spike

Added

MS

Result

MS


% Rec.

Limits

Pentachlorophenol ND 98.2 117 ug/L 119 23 - 166


MS MS

Limits


Client Sample ID: HTB0121-03Lab Sample ID: 580-17929-3 DU



Analyte

Sample

Result

Sample

Qualifier

DU

Result

DU

Qualifier Unit RPD

RPD

Limit

Pentachlorophenol ND ND ug/L NC 45


DU DU

Limits


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Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared







Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared







Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





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580-17929-1 HTB0121-01 Solid 02/22/10 12:00 02/24/10 08:40

580-17929-2 HTB0121-02 Solid 02/22/10 12:00 02/24/10 08:40

580-17929-3 HTB0121-03 Solid 02/22/10 12:00 02/24/10 08:40

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Login Number: 17929


Creator: Gamble, Cathy


List Number: 1


background

True



tampered with.

True








the COC.

True








MS/MSDs

True


diameter.

N/A


needs

True





TestAmerica Seattle

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Current Processing Operations

Mining Activities

appendix laboratory analytical results · 99-193 aiea heights drive, suite 121 aiea, hi 96701 *...

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