hrp associates, inc. - tranzon.com submittion - vwt inc property... · hrp associates, inc. (hrp)...

103
HRP Associates, Inc. Creating the Right Solutions Together CONNECTICUT 197 Scott Swamp Road Farmington, CT 06032 800-246-9021 860-674-9570 FAX 860-674-9624 501 Kings Highway East Fairfield, CT 06825 203-610-8212 FAX 203-610-8102 FLORIDA 8875 Hidden River Parkway Suite 300 Tampa, FL 33637 888-477-1877 813-975-7178 FAX 813-975-7170 INDIANA 450 East 96 th Street Suite 500 Indianapolis, IN 46240 317-581-6145 FAX 317-581-6146 NEW YORK 100 Saratoga Village Blvd. Suite 27 Malta, NY 12020 888-823-6427 518-899-3011 FAX 518-899-8129 PENNSYLVANIA 1060 First Avenue Suite 400 King of Prussia, PA 19460 866-232-9824 610-768-8061 FAX 610-337-9548 SOUTH CAROLINA 1327 Miller Road Suite D Greenville, SC 29607 800-752-3922 864-289-0311 FAX 864-281-9846 www.hrpassociates.com July 18, 2011 Mr. Jonathan G. McInnis, Program Manager Federal & State Site Assessment Site Assessment Remediation & Revitalization Division Bureau of Land & Waste Management 2600 Bull Street Columbia, South Carolina 29602 RE: Monitoring Well Data Submission; VWT Property 438 Belleview Road, Rock Hill, South Carolina; Site ID: 46-04669, Approval #4070 Dear Mr. McInnis: In accordance with the Temporary Monitoring Well Approval granted by SCDHEC on December 31, 2010, please find the attached the Phase II Environmental Site Assessment Report prepared for the VWT Property in York, S.C.. The Phase II ESA report includes HRPs conclusions regarding the limited investigation as well as the associated laboratory data, and maps indicating the location of the temporary on-Site groundwater monitoring wells. SCDHEC 1903 forms are also included in this correspondence. On behalf of T.D. Bank, N.A., HRP requests a letter of No Further Action based on the findings of this limited investigation. If you have any questions, please do not hesitate to contact us at (864) 289- 0311. Thank you for your time and assistance in this matter. Sincerely, HRP Associates, Inc. Robert T. (Ty) Hawkins Project Manager Tad A. Goetcheus, P.E. Regional Manager Cc: Mr. Joseph Lindsey, T.D. Bank, N.A. (via email only) Attachments

Upload: others

Post on 14-Sep-2019

16 views

Category:

Documents


0 download

TRANSCRIPT

HRP Associates, Inc. Creating the Right Solutions Together

CONNECTICUT

197 Scott Swamp Road Farmington, CT 06032 800-246-9021 860-674-9570 FAX 860-674-9624 501 Kings Highway East Fairfield, CT 06825 203-610-8212 FAX 203-610-8102

FLORIDA 8875 Hidden River Parkway Suite 300 Tampa, FL 33637 888-477-1877 813-975-7178 FAX 813-975-7170

INDIANA

450 East 96th Street Suite 500 Indianapolis, IN 46240 317-581-6145 FAX 317-581-6146

NEW YORK

100 Saratoga Village Blvd. Suite 27 Malta, NY 12020 888-823-6427 518-899-3011 FAX 518-899-8129

PENNSYLVANIA

1060 First Avenue Suite 400 King of Prussia, PA 19460 866-232-9824 610-768-8061 FAX 610-337-9548

SOUTH CAROLINA 1327 Miller Road Suite D Greenville, SC 29607 800-752-3922 864-289-0311 FAX 864-281-9846

www.hrpassociates.com

July 18, 2011 Mr. Jonathan G. McInnis, Program Manager Federal & State Site Assessment Site Assessment Remediation & Revitalization Division Bureau of Land & Waste Management 2600 Bull Street Columbia, South Carolina 29602 RE: Monitoring Well Data Submission;

VWT Property 438 Belleview Road, Rock Hill, South Carolina; Site ID: 46-04669, Approval #4070

Dear Mr. McInnis: In accordance with the Temporary Monitoring Well Approval granted by SCDHEC on December 31, 2010, please find the attached the Phase II Environmental Site Assessment Report prepared for the VWT Property in York, S.C.. The Phase II ESA report includes HRPs conclusions regarding the limited investigation as well as the associated laboratory data, and maps indicating the location of the temporary on-Site groundwater monitoring wells. SCDHEC 1903 forms are also included in this correspondence. On behalf of T.D. Bank, N.A., HRP requests a letter of No Further Action based on the findings of this limited investigation. If you have any questions, please do not hesitate to contact us at (864) 289-0311. Thank you for your time and assistance in this matter. Sincerely, HRP Associates, Inc.

Robert T. (Ty) Hawkins Project Manager

Tad A. Goetcheus, P.E. Regional Manager Cc: Mr. Joseph Lindsey, T.D. Bank, N.A. (via email only) Attachments

H:\C\Carolina First\2010\CAR4750.P2 - VWT, Inc. Phase 2\WP\ECA20090101 - VWT Inc Property Phase II ESA Baird-Ty Edits.doc

HRP Associates, Inc. Creating the Right Solutions Together

January 27, 2011 Mr. Andrew Bailey TD Bank, N.A. 2100 South Bridge Parkway Suite 650 Birmingham, AL 35209 RE: PHASE II ENVIRONMENTAL SITE ASSESSMENT

VWT, Inc. 438 Belleview Road Rock Hill, South Carolina ECA #20090101; HRP #CAR4750.P2

Dear Mr. Bailey: HRP Associates, Inc. (HRP) has completed a limited Phase II Environmental Site Assessment (ESA) at the property occupied by VWT, Inc, located at 2100 Belleview Road in Rock Hill, South Carolina (the Site). A site location map is included as Figure 1. This assessment was conducted in accordance with HRP’s previously authorized Proposal to Conduct an Environmental Investigation dated October 12, 2010. The purpose of the Phase II ESA is to investigate the following recognized environmental condition (REC) and a business environmental risk (BER) identified in the September 27, 2010 Phase I ESA report conducted by HRP:

The historical use of the Site as a metal fabrication and machine shop was considered a REC;

The substantial amount of metal structures and equipment stored on the Site was considered a BER.

In order to assess the aforementioned REC and BER, HRP conducted a limited subsurface soil and groundwater investigation at the Site on January 6, 2011. Utility Clearance Due to the industrial nature of the Site, Palmetto Utility Protection Service (PUPS) was contacted to identify underground utilities at the Site prior to the Phase II investigation. In addition, a ground penetrating radar (GPR) survey was conducted in proximity to the proposed drilling locations to further identify unidentified utility lines. As required by SCDHEC, HRP prepared and submitted a Monitoring Well Application Form (Form 3736) on behalf of VWT, Inc. prior to the installation of temporary

CONNECTICUT

197 Scott Swamp Road Farmington, CT 06032 800-246-9021 860-674-9570 FAX 860-674-9624 999 Oronoque Lane Suite 02 Stratford, CT 06614 203-380-1395 FAX 203-380-1438

FLORIDA

2435 US Highway 19 Suite 550 Holiday, FL 34691 727-942-2115 FAX 727-942-2113

INDIANA

7965 East 106th Street Suite 116 Fishers, IN 46038 317-570-4851 FAX 317-570-4852

NEW YORK

1 Fairchild Square Suite 110 Clifton Park, NY 12065 888-823-6427 518-877-7101 FAX 518-877-8561

SOUTH CAROLINA

1327 Miller Road Suite D Greenville, SC 29607 800-752-3922 864-289-0311 FAX 864-281-9846

TEXAS

Fort Worth Center 5601 Bridge Street Suite 300 Fort Worth, TX 76112 817-492-7092 FAX 817-492-7001

www.hrpassociates.com

Mr. Andrew Bailey TD Bank, N.A.

January 27, 2011 Page 2 of 4

H:\C\Carolina First\2010\CAR4750.P2 - VWT, Inc. Phase 2\WP\ECA20090101 - VWT Inc Property Phase II ESA Baird-Ty Edits.doc

groundwater monitoring wells onto the Subject Property. A copy of the Temporary Monitoring Well Approval #: 46-04669 is included as Attachment # of this report. Soil Investigation On January 6, 2011, six (6) soil borings (SB-1 through SB-6) were installed at locations throughout the Subject Property for the purpose of investigating the aforementioned REC and BER (Figure 2). The location of SB-1 was selected to serve the purpose of a “background” boring, where HRP believed was the least likely location to be affected by potential contamination on the Subject Property. Additional boring descriptions and locations are further discussed in Table 1 following the text portion of this report. A Geoprobe rig was utilized to advance the borings to 25 feet below ground surface (bgs) or until groundwater was encountered, which ever was encountered first. Five-foot soil macro-cores were collected during boring advancement. Each macro-core was screened for volatile organic compounds (VOCs) at one-foot intervals using a calibrated MiniRae 2000 photo-ionization detector (PID). One (1) soil sample was collected from each soil boring based on PID readings. Where no elevated PID readings were observed, soil was collected from the deepest point above the water table. The depth of each soil sample is identified in Table 2 of Attachment A of this report. Soil samples were submitted to a certified South Carolina laboratory (Analytical Environmental Services, Inc.) and analyzed for the following constituents:

Volatile Organic Compounds (VOCs) by EPA Method 8260; Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270; and Total Metals (arsenic, barium, cadmium, chromium, lead, mercury, selenium, and

silver) by EPA Method 6010. Laboratory results are discussed below. Groundwater Investigation Groundwater was detected in each of the six (6) soil borings; therefore, each boring was converted into a temporary monitoring well and renamed MW-1 through MW-6. Temporary wells were constructed of one-inch PVC riser with 10-foot screens and associated sand filter pack. Prior to sampling, each well was developed to remove soil cuttings and ensure low turbidity within the wells. One (1) grab groundwater sample was collected from each temporary monitoring well using a peristaltic pump and submitted to a laboratory certified in the State of South Carolina (Analytical Environmental Services, Inc.) for the analysis of the following constituents:

VOCs by EPA Method 8260; SVOCs by EPA Method 8270; Total Metals by EPA Method 6020A; and Dissolved Metals by EPA Method 6020A.

Mr. Andrew Bailey TD Bank, N.A.

January 27, 2011 Page 3 of 4

H:\C\Carolina First\2010\CAR4750.P2 - VWT, Inc. Phase 2\WP\ECA20090101 - VWT Inc Property Phase II ESA Baird-Ty Edits.doc

During the collection of groundwater samples, insufficient groundwater recharge occurred in MW-4 and MW-5. Due to the extremely low volume of groundwater produced by the temporary monitoring well, only VOCs were analyzed from these two (2) temporary monitoring wells. Analytical Results Soil samples collected during this investigation were compared to the EPA’s Regional Screening Level (RSL) Table (revised November 2010). The following chemical constituents were detected in the soil samples above either the PRG or SSL for the respective constituent:

SB-1 Benz(a)anthracene – 0.91 mg/kg (SSL = 0.01 mg/kg) Benzo(a)pyrene – 0.83 mg/kg (SSL = 0.0035 mg/kg) (RSL = 0.21 mg/kg) Benzo(b)fluoranthene – 0.97 mg/kg (SSL = 0.035 mg/kg) Indeno(1,2,3-cd)pyrene – 0.53 mg/kg (SSL = 0.12 mg/kg)

SB-2

Ethylbenzene – 0.0044 mg/kg (SSL = 0.0017 mg/kg) SB-6

Benz(a)anthracene – 0.69 mg/kg (SSL = 0.01 mg/kg) Benzo(a)pyrene – 0.57 mg/kg (PRG = 0.21 mg/kg) (SSL = 0.0035 mg/kg) Benzo(b)fluoranthene – 0.68 mg/kg (SSL = 0.035 mg/kg)

Metal constituents were detected in all six (6) soil sample locations collected at the Site. The observed levels are within the acceptable range of background metals concentrations according to a 1999 paper by J. Canova entitled Elements in South Carolina Inferred Background Soil and Stream Sediment Samples1. Groundwater samples collected during this investigation were compared to the State Primary Drinking Water and their associated Maximum Contaminant Levels (MCLs): R61-58 (revised September 2003). No chemical constituents were detected in groundwater samples collected during this investigation above their respective regulatory limits. Conclusions and Recommendations A Phase II ESA was performed at the Site on January 6, 2011 for the purpose of investigating one (1) REC identified in the September 27, 2010 Phase I prepared by HRP for the Subject Property. Six (6) soil and six (6) groundwater samples were collected and analyzed in order to evaluate soil and groundwater quality throughout the Property. Several petroleum constituents of concern were detected in soils above action levels in three (3) of six (6) boring locations (SB-1, SB-2 and SB-6). Soil borings SB-1 and SB-2 are located in the northern portion of the Site, while SB-6 is located at the southern portion of the Site.

1 Elements in South Carolina Inferred Background Soil and Stream Sediment Samples, J. Canova, South Carolina Geology, 1999, v.41, p. 11-25.

HRP Associates, Inc.

FIGURES

Site Map

VWT, Inc. 483 Belleview Road Rock Hill, SC 29730

Compiled:

September 17, 2010

HRP Associates, Inc. Creating the Right Solutions Together

1327-D Miller Road

Greenville, SC 29607

WJE
Callout
Subject Property

Figure 2

VWT, Inc. 483 Belleview Road Rock Hill, South Carolina

Compiled:

January 21, 2011

HRP Associates, Inc. Creating the Right Solutions Together

1327-D Miller Road

Greenville, SC 29607

HRP Associates, Inc.

ATTACHMENT A

TABLES

Table 1 – Sample Designations and Locations

Sample Designation

Sample Matrix

Field Screening Results (PPM) /

Depth (feet)

Soil Sample Depth (feet)

Depth to Groundwater

(feet) Sample Location Area of Concern

SB-1 / MW-1 Soil /

Groundwater ND / 14 13 – 14 15

Background boring/well located

at the northern extent of the

Property

Background

SB-2 / MW-2 Soil /

Groundwater 146 / 5 5 - 6 18

Eastern extent of Site along the exterior of the Storage Area

Manufacturing activities

associated with the Storage Area

SB-3 / MW-3 Soil /

Groundwater ND / 18 17 - 18 19

Eastern exterior of the Site along the

exterior of the Fabrication Shop

Manufacturing activities

associated with Fabrication Shop

SB-4 / MW-4 Soil /

Groundwater ND / 17 14 - 15 18

Centrally located on the Site at the southern exterior of the Fabrication

Shop

Manufacturing activities

associated with Fabrication Shop

SB-5 / MW-5 Soil /

Groundwater ND / 17 13 - 14 18

Southern portion of the Site at the

eastern exterior of the Storage Warehouse

Warehouse activities

associated with the Storage Warehouse

SB-6 / MW-6 Soil /

Groundwater ND / 16 14 - 15 18

Southern extent of the Site

Activities associated with metal storage

within southern portions of the

Site ND – None Detected

Sample ID

Field Screening Results for Sampled

Depth

Depth of Sample

(ft)Constituent

Concentration Detected EPA SSL1 RSL for

Industrial Soil1Background Range2

Benz(a)anthracene 0.91 0.01 2.1 N/ABenzo(a)pyrene 0.83 0.0035 0.21 N/ABenzo(b)fluoranthene 0.97 0.035 2.1 N/ABenzo(g,h,i)perylene 0.61 N/A N/A N/AChrysene 1.1 1.1 210 N/AFluoranthene 1.7 160 22,000 N/AIndeno(1,2,3-cd)pyrene 0.53 0.12 2.1 N/APhenanthrene 1.4 N/A N/A N/APyrene 1.9 120 1,700 N/ABarium 47.5 1,600 67,000 ND - 370Chromium 105 380 450 ND - 140Lead 78.1 N/A 800 ND - 200Silver 4.22 1.6 5,100 ND - 61Toluene 0.035 0.69 45,000 N/AEthylbenzene 0.0044 0.0017 27 N/AFluoranthene 0.47 160 22,000 N/ABarium 22.2 1,600 67,000 ND - 370Chromium 52.1 380 450 ND - 140Lead 9.22 N/A 800 ND - 200Barium 79.5 1,600 67,000 ND - 370Chromium 48.0 380 450 ND - 140Barium 76.9 1,600 67,000 ND - 370Chromium 46.3 380 450 ND - 140Barium 161 1,600 67,000 ND - 370Chromium 29.2 380 450 ND - 140Benz(a)anthracene 0.69 0.01 2.1 N/ABenzo(a)pyrene 0.57 0.0035 0.21 N/ABenzo(b)fluoranthene 0.68 0.035 2.1 N/AChrysene 0.65 1 210 N/AFluoranthene 1.5 160 22,000 N/APhenanthrene 1.2 N/A N/A N/APyrene 1.2 120 1,700 N/ABarium 149 1,600 67,000 ND - 370Chromium 10.6 380 450 ND - 140

SB-4 0.0 14-15

SB-5 0.0 13-14

Table 2 - Soil Sample Analytical Results

SB-1 0.0 13-14

SB-2 146.0 4-5

SB-3 0.0 17-18

14-15SB-6 0.0

H:\C\Carolina First\2010\CAR4750.P2 - VWT, Inc. Phase 2\Data\VWT Phase II Data 1

Sample ID

Field Screening Results for Sampled

Depth

Depth of Sample

(ft)Constituent

Concentration Detected EPA SSL1 RSL for

Industrial Soil1Background Range2

Table 2 - Soil Sample Analytical Results

Lead 12.8 N/A 800 ND - 200

All concentrations displayed in Table 2 are only those reported above the analytical detection limit.

Values shaded indicate an exceedence of the RSL for industrial soils

N/A – Not Applicable

2 - Inferred Background Soil Concentration Ranges are based upon to Elements in South Carolina Inferred Background Soil Sediment Samples, South Carolina Geology, 1999, v41, p11-25, Judy Conova

All concentrations are presented in parts per million (mg/kg)

Values in bold indicate concentrations in exceedence of the protection to groundwater SSL

Notes:

1 - EPA's Regional Screening Level (RSL) Summary Table (November 2010)

H:\C\Carolina First\2010\CAR4750.P2 - VWT, Inc. Phase 2\Data\VWT Phase II Data 2

Sample IDDepth of Sample

(ft)Constituent

Concentration Detected

MCL

Barium (Total) 56.9 2,000Barium (Dissolved) 38.4 2,000Chromium (Total) 6.59 100Lead (Total) 1.88 15***Barium (Total) 192 2,000Barium (Dissolved) 39.7 2,000Chromium (Total) 64.5 100Lead (Total) 2.6 15***Barium (Total) 58.6 2,000Barium (Dissolved) 51.2 2,000Lead (Total) 1.28 15***Barium (Total) 63.1 2,000Barium (Dissolved) 44.6 2,000Chromium (Total) 5.92 100Lead 1.56 15***

Notes:

EPA Region 9 - Prelininary Remediation Goals-Tap Water (10-4-2004)

Table 3 - Groundwater Analytical Results

All concentrations displayed in Table 3 are only those reported above the analytical detection limit.

All concentrations are presented in parts per billion (µg/L)

MW-1 24.5

MW-2 24.5

MW-3 24.5

*State Primary Drinking Water and their associated Maximum Contaminant Levels (MCLs): R61-58 Sept. 26, 2003

MW-6 24.7

H:\C\Carolina First\2010\CAR4750.P2 - VWT, Inc. Phase 2\Data\VWT Phase II Data 1

HRP Associates, Inc.

ATTACHMENT B

LABORATORY ANALYTICAL REPORTS

January 17, 2011

Dear Order No:

RE:

Analytical Environmental Services, Inc. received samples on for the analyses presented in following report.

FAX:TEL:

13

No problems were encountered during the analyses. Additionally, all results for the associated

Quality Control samples were within EPA and/or AES established limits. Any discrepancies

associated with the analyses contained herein will be noted and submitted in the form of a

project Case Narrative.

AES’ certifications are as follows:

-NELAC/Florida Certification number E87582 for analysis of Environmental Water,

soil/hazardous waste, and Drinking Water Microbiology, effective 07/01/10-06/30/11.

-AIHA Certification ID #100671 for Industrial Hygiene samples (Organics, Inorganics),

Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)

effective until 09/01/11.

These results relate only to the items tested. This report may only be reproduced in full.

If you have any questions regarding these test results, please feel free to call.

(864) 289-0311(864) 281-9846

Project Manager

1101566

Tim BairdHRP Associates, inc.1327 Miller Rd.Greenville SC 29607

VWT, Inc

Brian Rohr

1/8/2011 9:10:00 AM

Tim Baird:

1 of 80

2 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

Case NarrativeVWT, Inc

HRP Associates, inc.

Lab ID:

Project:

1101566

Sample Receiving Nonconformance:

A Trip Blank was provided, but not listed on the Chain of Custody. Trip blank analyzed at no cost to the client.

Sample MW-4 was received with one HCL preserved vial broken. The laboratory proceeded with the analysis using the other

available vial.

3 of 80

1101566-001

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 9:50:00 AM

SB-1

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

n-Heptane BRL 8.0 N ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Dichlorodifluoromethane BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Chloromethane BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Vinyl chloride BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Bromomethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Chloroethane BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Trichlorofluoromethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,1-Dichloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Acetone BRL 80 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Freon-113 BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Carbon disulfide BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Methyl acetate BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Methylene chloride BRL 16 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Methyl tert-butyl ether BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

trans-1,2-Dichloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,1-Dichloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

cis-1,2-Dichloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

2-Butanone BRL 40 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Chloroform BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,1,1-Trichloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Cyclohexane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Carbon tetrachloride BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Benzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,2-Dichloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Trichloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Methylcyclohexane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,2-Dichloropropane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Bromodichloromethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

cis-1,3-Dichloropropene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

4-Methyl-2-pentanone BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Toluene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

trans-1,3-Dichloropropene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,1,2-Trichloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

2-Hexanone BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Tetrachloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Dibromochloromethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,2-Dibromoethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Chlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Ethylbenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Styrene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Bromoform BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

4 of 80

1101566-001

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 9:50:00 AM

SB-1

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

1,1,2,2-Tetrachloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Isopropylbenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Naphthalene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,3-Dichlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,4-Dichlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,2-Dichlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,2-Dibromo-3-chloropropane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

1,2,4-Trichlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Xylenes, Total BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 13:38 JE

Surr: 4-Bromofluorobenzene 93.3 56-137 %REC 140584 1 01/13/2011 13:38 JE

Surr: Dibromofluoromethane 99.1 73.7-137 %REC 140584 1 01/13/2011 13:38 JE

Surr: Toluene-d8 93.4 69.2-126 %REC 140584 1 01/13/2011 13:38 JE

(SW7471)TOTAL MERCURY SW7471B

Mercury BRL 0.142 mg/Kg-dry 140598 1 01/14/2011 12:18 JY

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2,4,5-Trichlorophenol BRL 2500 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2,4,6-Trichlorophenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2,4-Dichlorophenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2,4-Dimethylphenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2,4-Dinitrophenol BRL 2500 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2,4-Dinitrotoluene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2,6-Dinitrotoluene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2-Chloronaphthalene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2-Chlorophenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2-Methylnaphthalene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2-Methylphenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2-Nitroaniline BRL 2500 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

2-Nitrophenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

3,3´-Dichlorobenzidine BRL 980 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

3-Nitroaniline BRL 2500 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

4,6-Dinitro-2-methylphenol BRL 2500 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

4-Bromophenyl phenyl ether BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

4-Chloro-3-methylphenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

4-Chloroaniline BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

4-Chlorophenyl phenyl ether BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

4-Methylphenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

4-Nitroaniline BRL 2500 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

4-Nitrophenol BRL 2500 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

5 of 80

1101566-001

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 9:50:00 AM

SB-1

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Acenaphthene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Acenaphthylene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Acetophenone BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Anthracene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Atrazine BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Benz(a)anthracene 910 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Benzaldehyde BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Benzo(a)pyrene 830 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Benzo(b)fluoranthene 970 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Benzo(g,h,i)perylene 610 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Benzo(k)fluoranthene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Bis(2-chloroethoxy)methane BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Bis(2-chloroethyl)ether BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Bis(2-chloroisopropyl)ether BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Bis(2-ethylhexyl)phthalate BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Butyl benzyl phthalate BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Caprolactam BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Carbazole BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Chrysene 1100 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Di-n-butyl phthalate BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Di-n-octyl phthalate BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Dibenz(a,h)anthracene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Dibenzofuran BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Diethyl phthalate BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Dimethyl phthalate BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Fluoranthene 1700 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Fluorene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Hexachlorobenzene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Hexachlorobutadiene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Hexachlorocyclopentadiene BRL 970 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Hexachloroethane BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Indeno(1,2,3-cd)pyrene 530 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Isophorone BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

N-Nitrosodi-n-propylamine BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

N-Nitrosodiphenylamine BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Naphthalene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Nitrobenzene BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Pentachlorophenol BRL 2500 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Phenanthrene 1400 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Phenol BRL 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Pyrene 1900 480 ug/Kg-dry 140499 1 01/13/2011 14:43 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

6 of 80

1101566-001

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 9:50:00 AM

SB-1

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Surr: 2,4,6-Tribromophenol 95.5 40.4-136 %REC 140499 1 01/13/2011 14:43 YH

Surr: 2-Fluorobiphenyl 88.2 48.5-120 %REC 140499 1 01/13/2011 14:43 YH

Surr: 2-Fluorophenol 77.2 36.5-120 %REC 140499 1 01/13/2011 14:43 YH

Surr: 4-Terphenyl-d14 94.9 51-125 %REC 140499 1 01/13/2011 14:43 YH

Surr: Nitrobenzene-d5 80 37.6-120 %REC 140499 1 01/13/2011 14:43 YH

Surr: Phenol-d5 85.6 40.1-120 %REC 140499 1 01/13/2011 14:43 YH

(SW3050B) METALS, TOTAL SW6010C

Arsenic BRL 7.24 mg/Kg-dry 140509 1 01/13/2011 16:43 MP

Barium 47.5 7.24 mg/Kg-dry 140509 1 01/13/2011 16:43 MP

Cadmium BRL 3.62 mg/Kg-dry 140509 1 01/13/2011 16:43 MP

Chromium 105 3.62 mg/Kg-dry 140509 1 01/13/2011 16:43 MP

Lead 78.1 7.24 mg/Kg-dry 140509 1 01/13/2011 16:43 MP

Selenium BRL 7.24 mg/Kg-dry 140509 1 01/13/2011 16:43 MP

Silver 4.22 3.62 mg/Kg-dry 140509 1 01/13/2011 16:43 MP

PERCENT MOISTURE D2216

Percent Moisture 32.0 0 wt% R188399 1 01/14/2011 10:00 AS

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

7 of 80

1101566-002

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 10:55:00 AM

SB-2

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

n-Heptane BRL 8.0 N ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Dichlorodifluoromethane BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Chloromethane BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Vinyl chloride BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Bromomethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Chloroethane BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Trichlorofluoromethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,1-Dichloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Acetone BRL 80 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Freon-113 BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Carbon disulfide BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Methyl acetate BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Methylene chloride BRL 16 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Methyl tert-butyl ether BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

trans-1,2-Dichloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,1-Dichloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

cis-1,2-Dichloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

2-Butanone BRL 40 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Chloroform BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,1,1-Trichloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Cyclohexane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Carbon tetrachloride BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Benzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,2-Dichloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Trichloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Methylcyclohexane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,2-Dichloropropane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Bromodichloromethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

cis-1,3-Dichloropropene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

4-Methyl-2-pentanone BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Toluene 35 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

trans-1,3-Dichloropropene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,1,2-Trichloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

2-Hexanone BRL 8.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Tetrachloroethene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Dibromochloromethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,2-Dibromoethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Chlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Ethylbenzene 4.4 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Styrene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Bromoform BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

8 of 80

1101566-002

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 10:55:00 AM

SB-2

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

1,1,2,2-Tetrachloroethane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Isopropylbenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Naphthalene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,3-Dichlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,4-Dichlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,2-Dichlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,2-Dibromo-3-chloropropane BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

1,2,4-Trichlorobenzene BRL 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Xylenes, Total 19 4.0 ug/Kg-dry 140584 1 01/13/2011 14:04 JE

Surr: 4-Bromofluorobenzene 98.8 56-137 %REC 140584 1 01/13/2011 14:04 JE

Surr: Dibromofluoromethane 101 73.7-137 %REC 140584 1 01/13/2011 14:04 JE

Surr: Toluene-d8 99 69.2-126 %REC 140584 1 01/13/2011 14:04 JE

(SW7471)TOTAL MERCURY SW7471B

Mercury BRL 0.135 mg/Kg-dry 140598 1 01/14/2011 12:21 JY

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2,4,5-Trichlorophenol BRL 2300 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2,4,6-Trichlorophenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2,4-Dichlorophenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2,4-Dimethylphenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2,4-Dinitrophenol BRL 2300 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2,4-Dinitrotoluene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2,6-Dinitrotoluene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2-Chloronaphthalene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2-Chlorophenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2-Methylnaphthalene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2-Methylphenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2-Nitroaniline BRL 2300 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

2-Nitrophenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

3,3´-Dichlorobenzidine BRL 910 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

3-Nitroaniline BRL 2300 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

4,6-Dinitro-2-methylphenol BRL 2300 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

4-Bromophenyl phenyl ether BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

4-Chloro-3-methylphenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

4-Chloroaniline BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

4-Chlorophenyl phenyl ether BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

4-Methylphenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

4-Nitroaniline BRL 2300 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

4-Nitrophenol BRL 2300 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

9 of 80

1101566-002

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 10:55:00 AM

SB-2

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Acenaphthene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Acenaphthylene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Acetophenone BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Anthracene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Atrazine BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Benz(a)anthracene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Benzaldehyde BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Benzo(a)pyrene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Benzo(b)fluoranthene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Benzo(g,h,i)perylene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Benzo(k)fluoranthene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Bis(2-chloroethoxy)methane BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Bis(2-chloroethyl)ether BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Bis(2-chloroisopropyl)ether BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Bis(2-ethylhexyl)phthalate BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Butyl benzyl phthalate BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Caprolactam BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Carbazole BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Chrysene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Di-n-butyl phthalate BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Di-n-octyl phthalate BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Dibenz(a,h)anthracene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Dibenzofuran BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Diethyl phthalate BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Dimethyl phthalate BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Fluoranthene 470 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Fluorene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Hexachlorobenzene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Hexachlorobutadiene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Hexachlorocyclopentadiene BRL 900 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Hexachloroethane BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Indeno(1,2,3-cd)pyrene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Isophorone BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

N-Nitrosodi-n-propylamine BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

N-Nitrosodiphenylamine BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Naphthalene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Nitrobenzene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Pentachlorophenol BRL 2300 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Phenanthrene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Phenol BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Pyrene BRL 450 ug/Kg-dry 140499 1 01/13/2011 15:08 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

10 of 80

1101566-002

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 10:55:00 AM

SB-2

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Surr: 2,4,6-Tribromophenol 93.3 40.4-136 %REC 140499 1 01/13/2011 15:08 YH

Surr: 2-Fluorobiphenyl 82.9 48.5-120 %REC 140499 1 01/13/2011 15:08 YH

Surr: 2-Fluorophenol 70.8 36.5-120 %REC 140499 1 01/13/2011 15:08 YH

Surr: 4-Terphenyl-d14 90.1 51-125 %REC 140499 1 01/13/2011 15:08 YH

Surr: Nitrobenzene-d5 72.3 37.6-120 %REC 140499 1 01/13/2011 15:08 YH

Surr: Phenol-d5 78.4 40.1-120 %REC 140499 1 01/13/2011 15:08 YH

(SW3050B) METALS, TOTAL SW6010C

Arsenic BRL 6.37 mg/Kg-dry 140509 1 01/13/2011 16:47 MP

Barium 22.2 6.37 mg/Kg-dry 140509 1 01/13/2011 16:47 MP

Cadmium BRL 3.18 mg/Kg-dry 140509 1 01/13/2011 16:47 MP

Chromium 52.1 3.18 mg/Kg-dry 140509 1 01/13/2011 16:47 MP

Lead 9.22 6.37 mg/Kg-dry 140509 1 01/13/2011 16:47 MP

Selenium BRL 6.37 mg/Kg-dry 140509 1 01/13/2011 16:47 MP

Silver BRL 3.18 mg/Kg-dry 140509 1 01/13/2011 16:47 MP

PERCENT MOISTURE D2216

Percent Moisture 26.6 0 wt% R188399 1 01/14/2011 10:00 AS

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

11 of 80

1101566-003

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 11:40:00 AM

SB-3

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

n-Heptane BRL 9.7 N ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Dichlorodifluoromethane BRL 9.7 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Chloromethane BRL 9.7 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Vinyl chloride BRL 9.7 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Bromomethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Chloroethane BRL 9.7 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Trichlorofluoromethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,1-Dichloroethene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Acetone BRL 97 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Freon-113 BRL 9.7 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Carbon disulfide BRL 9.7 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Methyl acetate BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Methylene chloride BRL 19 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Methyl tert-butyl ether BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

trans-1,2-Dichloroethene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,1-Dichloroethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

cis-1,2-Dichloroethene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

2-Butanone BRL 48 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Chloroform BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,1,1-Trichloroethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Cyclohexane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Carbon tetrachloride BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Benzene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,2-Dichloroethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Trichloroethene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Methylcyclohexane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,2-Dichloropropane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Bromodichloromethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

cis-1,3-Dichloropropene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

4-Methyl-2-pentanone BRL 9.7 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Toluene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

trans-1,3-Dichloropropene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,1,2-Trichloroethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

2-Hexanone BRL 9.7 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Tetrachloroethene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Dibromochloromethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,2-Dibromoethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Chlorobenzene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Ethylbenzene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Styrene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Bromoform BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

12 of 80

1101566-003

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 11:40:00 AM

SB-3

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

1,1,2,2-Tetrachloroethane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Isopropylbenzene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Naphthalene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,3-Dichlorobenzene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,4-Dichlorobenzene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,2-Dichlorobenzene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,2-Dibromo-3-chloropropane BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

1,2,4-Trichlorobenzene BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Xylenes, Total BRL 4.8 ug/Kg-dry 140584 1 01/13/2011 14:29 JE

Surr: 4-Bromofluorobenzene 94.3 56-137 %REC 140584 1 01/13/2011 14:29 JE

Surr: Dibromofluoromethane 103 73.7-137 %REC 140584 1 01/13/2011 14:29 JE

Surr: Toluene-d8 92.6 69.2-126 %REC 140584 1 01/13/2011 14:29 JE

(SW7471)TOTAL MERCURY SW7471B

Mercury BRL 0.141 mg/Kg-dry 140598 1 01/14/2011 12:23 JY

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2,4,5-Trichlorophenol BRL 2400 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2,4,6-Trichlorophenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2,4-Dichlorophenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2,4-Dimethylphenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2,4-Dinitrophenol BRL 2400 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2,4-Dinitrotoluene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2,6-Dinitrotoluene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2-Chloronaphthalene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2-Chlorophenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2-Methylnaphthalene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2-Methylphenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2-Nitroaniline BRL 2400 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

2-Nitrophenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

3,3´-Dichlorobenzidine BRL 940 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

3-Nitroaniline BRL 2400 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

4,6-Dinitro-2-methylphenol BRL 2400 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

4-Bromophenyl phenyl ether BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

4-Chloro-3-methylphenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

4-Chloroaniline BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

4-Chlorophenyl phenyl ether BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

4-Methylphenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

4-Nitroaniline BRL 2400 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

4-Nitrophenol BRL 2400 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

13 of 80

1101566-003

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 11:40:00 AM

SB-3

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Acenaphthene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Acenaphthylene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Acetophenone BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Anthracene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Atrazine BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Benz(a)anthracene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Benzaldehyde BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Benzo(a)pyrene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Benzo(b)fluoranthene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Benzo(g,h,i)perylene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Benzo(k)fluoranthene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Bis(2-chloroethoxy)methane BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Bis(2-chloroethyl)ether BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Bis(2-chloroisopropyl)ether BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Bis(2-ethylhexyl)phthalate BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Butyl benzyl phthalate BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Caprolactam BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Carbazole BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Chrysene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Di-n-butyl phthalate BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Di-n-octyl phthalate BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Dibenz(a,h)anthracene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Dibenzofuran BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Diethyl phthalate BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Dimethyl phthalate BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Fluoranthene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Fluorene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Hexachlorobenzene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Hexachlorobutadiene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Hexachlorocyclopentadiene BRL 930 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Hexachloroethane BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Indeno(1,2,3-cd)pyrene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Isophorone BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

N-Nitrosodi-n-propylamine BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

N-Nitrosodiphenylamine BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Naphthalene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Nitrobenzene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Pentachlorophenol BRL 2400 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Phenanthrene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Phenol BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Pyrene BRL 470 ug/Kg-dry 140499 1 01/12/2011 17:47 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

14 of 80

1101566-003

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 11:40:00 AM

SB-3

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Surr: 2,4,6-Tribromophenol 77.3 40.4-136 %REC 140499 1 01/12/2011 17:47 YH

Surr: 2-Fluorobiphenyl 76.8 48.5-120 %REC 140499 1 01/12/2011 17:47 YH

Surr: 2-Fluorophenol 68.1 36.5-120 %REC 140499 1 01/12/2011 17:47 YH

Surr: 4-Terphenyl-d14 84.1 51-125 %REC 140499 1 01/12/2011 17:47 YH

Surr: Nitrobenzene-d5 63.2 37.6-120 %REC 140499 1 01/12/2011 17:47 YH

Surr: Phenol-d5 71.2 40.1-120 %REC 140499 1 01/12/2011 17:47 YH

(SW3050B) METALS, TOTAL SW6010C

Arsenic BRL 6.56 mg/Kg-dry 140509 1 01/13/2011 16:57 MP

Barium 79.5 6.56 mg/Kg-dry 140509 1 01/13/2011 16:57 MP

Cadmium BRL 3.28 mg/Kg-dry 140509 1 01/13/2011 16:57 MP

Chromium 66.1 3.28 mg/Kg-dry 140509 1 01/13/2011 16:57 MP

Lead BRL 6.56 mg/Kg-dry 140509 1 01/13/2011 16:57 MP

Selenium BRL 6.56 mg/Kg-dry 140509 1 01/13/2011 16:57 MP

Silver BRL 3.28 mg/Kg-dry 140509 1 01/13/2011 16:57 MP

PERCENT MOISTURE D2216

Percent Moisture 29.1 0 wt% R188399 1 01/14/2011 10:00 AS

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

15 of 80

1101566-004

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 12:25:00 PM

SB-4

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

n-Heptane BRL 10 N ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Dichlorodifluoromethane BRL 10 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Chloromethane BRL 10 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Vinyl chloride BRL 10 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Bromomethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Chloroethane BRL 10 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Trichlorofluoromethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,1-Dichloroethene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Acetone BRL 100 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Freon-113 BRL 10 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Carbon disulfide BRL 10 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Methyl acetate BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Methylene chloride BRL 20 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Methyl tert-butyl ether BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

trans-1,2-Dichloroethene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,1-Dichloroethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

cis-1,2-Dichloroethene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

2-Butanone BRL 51 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Chloroform BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,1,1-Trichloroethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Cyclohexane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Carbon tetrachloride BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Benzene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,2-Dichloroethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Trichloroethene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Methylcyclohexane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,2-Dichloropropane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Bromodichloromethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

cis-1,3-Dichloropropene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

4-Methyl-2-pentanone BRL 10 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Toluene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

trans-1,3-Dichloropropene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,1,2-Trichloroethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

2-Hexanone BRL 10 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Tetrachloroethene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Dibromochloromethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,2-Dibromoethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Chlorobenzene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Ethylbenzene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Styrene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Bromoform BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

16 of 80

1101566-004

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 12:25:00 PM

SB-4

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

1,1,2,2-Tetrachloroethane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Isopropylbenzene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Naphthalene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,3-Dichlorobenzene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,4-Dichlorobenzene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,2-Dichlorobenzene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,2-Dibromo-3-chloropropane BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

1,2,4-Trichlorobenzene BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Xylenes, Total BRL 5.1 ug/Kg-dry 140584 1 01/13/2011 14:54 JE

Surr: 4-Bromofluorobenzene 98.1 56-137 %REC 140584 1 01/13/2011 14:54 JE

Surr: Dibromofluoromethane 102 73.7-137 %REC 140584 1 01/13/2011 14:54 JE

Surr: Toluene-d8 96.6 69.2-126 %REC 140584 1 01/13/2011 14:54 JE

(SW7471)TOTAL MERCURY SW7471B

Mercury BRL 0.157 mg/Kg-dry 140598 1 01/14/2011 12:30 JY

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2,4,5-Trichlorophenol BRL 2700 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2,4,6-Trichlorophenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2,4-Dichlorophenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2,4-Dimethylphenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2,4-Dinitrophenol BRL 2700 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2,4-Dinitrotoluene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2,6-Dinitrotoluene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2-Chloronaphthalene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2-Chlorophenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2-Methylnaphthalene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2-Methylphenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2-Nitroaniline BRL 2700 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

2-Nitrophenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

3,3´-Dichlorobenzidine BRL 1100 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

3-Nitroaniline BRL 2700 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

4,6-Dinitro-2-methylphenol BRL 2700 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

4-Bromophenyl phenyl ether BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

4-Chloro-3-methylphenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

4-Chloroaniline BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

4-Chlorophenyl phenyl ether BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

4-Methylphenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

4-Nitroaniline BRL 2700 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

4-Nitrophenol BRL 2700 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

17 of 80

1101566-004

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 12:25:00 PM

SB-4

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Acenaphthene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Acenaphthylene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Acetophenone BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Anthracene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Atrazine BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Benz(a)anthracene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Benzaldehyde BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Benzo(a)pyrene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Benzo(b)fluoranthene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Benzo(g,h,i)perylene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Benzo(k)fluoranthene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Bis(2-chloroethoxy)methane BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Bis(2-chloroethyl)ether BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Bis(2-chloroisopropyl)ether BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Bis(2-ethylhexyl)phthalate BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Butyl benzyl phthalate BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Caprolactam BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Carbazole BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Chrysene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Di-n-butyl phthalate BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Di-n-octyl phthalate BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Dibenz(a,h)anthracene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Dibenzofuran BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Diethyl phthalate BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Dimethyl phthalate BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Fluoranthene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Fluorene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Hexachlorobenzene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Hexachlorobutadiene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Hexachlorocyclopentadiene BRL 1000 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Hexachloroethane BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Indeno(1,2,3-cd)pyrene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Isophorone BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

N-Nitrosodi-n-propylamine BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

N-Nitrosodiphenylamine BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Naphthalene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Nitrobenzene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Pentachlorophenol BRL 2700 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Phenanthrene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Phenol BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Pyrene BRL 520 ug/Kg-dry 140499 1 01/12/2011 18:14 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

18 of 80

1101566-004

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 12:25:00 PM

SB-4

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Surr: 2,4,6-Tribromophenol 74.3 40.4-136 %REC 140499 1 01/12/2011 18:14 YH

Surr: 2-Fluorobiphenyl 72.7 48.5-120 %REC 140499 1 01/12/2011 18:14 YH

Surr: 2-Fluorophenol 65.3 36.5-120 %REC 140499 1 01/12/2011 18:14 YH

Surr: 4-Terphenyl-d14 84.5 51-125 %REC 140499 1 01/12/2011 18:14 YH

Surr: Nitrobenzene-d5 62.8 37.6-120 %REC 140499 1 01/12/2011 18:14 YH

Surr: Phenol-d5 71.2 40.1-120 %REC 140499 1 01/12/2011 18:14 YH

(SW3050B) METALS, TOTAL SW6010C

Arsenic BRL 7.27 mg/Kg-dry 140509 1 01/13/2011 16:18 MP

Barium 76.9 7.27 mg/Kg-dry 140509 1 01/13/2011 16:18 MP

Cadmium BRL 3.63 mg/Kg-dry 140509 1 01/13/2011 16:18 MP

Chromium 46.3 3.63 mg/Kg-dry 140509 1 01/13/2011 16:18 MP

Lead BRL 7.27 mg/Kg-dry 140509 1 01/13/2011 16:18 MP

Selenium BRL 7.27 mg/Kg-dry 140509 1 01/13/2011 16:18 MP

Silver BRL 3.63 mg/Kg-dry 140509 1 01/13/2011 16:18 MP

PERCENT MOISTURE D2216

Percent Moisture 36.6 0 wt% R188399 1 01/14/2011 10:00 AS

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

19 of 80

1101566-005

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 1:55:00 PM

SB-5

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

n-Heptane BRL 8.3 N ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Dichlorodifluoromethane BRL 8.3 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Chloromethane BRL 8.3 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Vinyl chloride BRL 8.3 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Bromomethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Chloroethane BRL 8.3 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Trichlorofluoromethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,1-Dichloroethene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Acetone BRL 83 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Freon-113 BRL 8.3 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Carbon disulfide BRL 8.3 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Methyl acetate BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Methylene chloride BRL 17 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Methyl tert-butyl ether BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

trans-1,2-Dichloroethene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,1-Dichloroethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

cis-1,2-Dichloroethene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

2-Butanone BRL 42 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Chloroform BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,1,1-Trichloroethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Cyclohexane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Carbon tetrachloride BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Benzene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,2-Dichloroethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Trichloroethene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Methylcyclohexane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,2-Dichloropropane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Bromodichloromethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

cis-1,3-Dichloropropene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

4-Methyl-2-pentanone BRL 8.3 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Toluene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

trans-1,3-Dichloropropene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,1,2-Trichloroethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

2-Hexanone BRL 8.3 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Tetrachloroethene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Dibromochloromethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,2-Dibromoethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Chlorobenzene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Ethylbenzene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Styrene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Bromoform BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

20 of 80

1101566-005

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 1:55:00 PM

SB-5

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

1,1,2,2-Tetrachloroethane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Isopropylbenzene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Naphthalene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,3-Dichlorobenzene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,4-Dichlorobenzene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,2-Dichlorobenzene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,2-Dibromo-3-chloropropane BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

1,2,4-Trichlorobenzene BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Xylenes, Total BRL 4.2 ug/Kg-dry 140584 1 01/13/2011 15:33 JE

Surr: 4-Bromofluorobenzene 96 56-137 %REC 140584 1 01/13/2011 15:33 JE

Surr: Dibromofluoromethane 109 73.7-137 %REC 140584 1 01/13/2011 15:33 JE

Surr: Toluene-d8 90.2 69.2-126 %REC 140584 1 01/13/2011 15:33 JE

(SW7471)TOTAL MERCURY SW7471B

Mercury BRL 0.133 mg/Kg-dry 140598 1 01/14/2011 12:32 JY

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2,4,5-Trichlorophenol BRL 2300 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2,4,6-Trichlorophenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2,4-Dichlorophenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2,4-Dimethylphenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2,4-Dinitrophenol BRL 2300 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2,4-Dinitrotoluene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2,6-Dinitrotoluene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2-Chloronaphthalene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2-Chlorophenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2-Methylnaphthalene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2-Methylphenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2-Nitroaniline BRL 2300 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

2-Nitrophenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

3,3´-Dichlorobenzidine BRL 900 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

3-Nitroaniline BRL 2300 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

4,6-Dinitro-2-methylphenol BRL 2300 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

4-Bromophenyl phenyl ether BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

4-Chloro-3-methylphenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

4-Chloroaniline BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

4-Chlorophenyl phenyl ether BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

4-Methylphenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

4-Nitroaniline BRL 2300 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

4-Nitrophenol BRL 2300 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

21 of 80

1101566-005

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 1:55:00 PM

SB-5

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Acenaphthene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Acenaphthylene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Acetophenone BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Anthracene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Atrazine BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Benz(a)anthracene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Benzaldehyde BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Benzo(a)pyrene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Benzo(b)fluoranthene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Benzo(g,h,i)perylene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Benzo(k)fluoranthene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Bis(2-chloroethoxy)methane BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Bis(2-chloroethyl)ether BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Bis(2-chloroisopropyl)ether BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Bis(2-ethylhexyl)phthalate BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Butyl benzyl phthalate BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Caprolactam BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Carbazole BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Chrysene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Di-n-butyl phthalate BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Di-n-octyl phthalate BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Dibenz(a,h)anthracene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Dibenzofuran BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Diethyl phthalate BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Dimethyl phthalate BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Fluoranthene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Fluorene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Hexachlorobenzene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Hexachlorobutadiene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Hexachlorocyclopentadiene BRL 890 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Hexachloroethane BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Indeno(1,2,3-cd)pyrene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Isophorone BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

N-Nitrosodi-n-propylamine BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

N-Nitrosodiphenylamine BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Naphthalene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Nitrobenzene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Pentachlorophenol BRL 2300 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Phenanthrene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Phenol BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Pyrene BRL 440 ug/Kg-dry 140499 1 01/12/2011 16:27 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

22 of 80

1101566-005

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 1:55:00 PM

SB-5

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Surr: 2,4,6-Tribromophenol 84.9 40.4-136 %REC 140499 1 01/12/2011 16:27 YH

Surr: 2-Fluorobiphenyl 77.6 48.5-120 %REC 140499 1 01/12/2011 16:27 YH

Surr: 2-Fluorophenol 67.2 36.5-120 %REC 140499 1 01/12/2011 16:27 YH

Surr: 4-Terphenyl-d14 87.4 51-125 %REC 140499 1 01/12/2011 16:27 YH

Surr: Nitrobenzene-d5 66.3 37.6-120 %REC 140499 1 01/12/2011 16:27 YH

Surr: Phenol-d5 71 40.1-120 %REC 140499 1 01/12/2011 16:27 YH

(SW3050B) METALS, TOTAL SW6010C

Arsenic BRL 6.41 mg/Kg-dry 140509 1 01/13/2011 17:01 MP

Barium 161 6.41 mg/Kg-dry 140509 1 01/13/2011 17:01 MP

Cadmium BRL 3.21 mg/Kg-dry 140509 1 01/13/2011 17:01 MP

Chromium 29.2 3.21 mg/Kg-dry 140509 1 01/13/2011 17:01 MP

Lead BRL 6.41 mg/Kg-dry 140509 1 01/13/2011 17:01 MP

Selenium BRL 6.41 mg/Kg-dry 140509 1 01/13/2011 17:01 MP

Silver BRL 3.21 mg/Kg-dry 140509 1 01/13/2011 17:01 MP

PERCENT MOISTURE D2216

Percent Moisture 25.9 0 wt% R188399 1 01/14/2011 10:00 AS

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

23 of 80

1101566-006

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 3:10:00 PM

SB-6

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

n-Heptane BRL 8.2 N ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Dichlorodifluoromethane BRL 8.2 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Chloromethane BRL 8.2 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Vinyl chloride BRL 8.2 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Bromomethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Chloroethane BRL 8.2 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Trichlorofluoromethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,1-Dichloroethene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Acetone BRL 82 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Freon-113 BRL 8.2 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Carbon disulfide BRL 8.2 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Methyl acetate BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Methylene chloride BRL 16 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Methyl tert-butyl ether BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

trans-1,2-Dichloroethene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,1-Dichloroethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

cis-1,2-Dichloroethene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

2-Butanone BRL 41 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Chloroform BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,1,1-Trichloroethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Cyclohexane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Carbon tetrachloride BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Benzene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,2-Dichloroethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Trichloroethene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Methylcyclohexane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,2-Dichloropropane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Bromodichloromethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

cis-1,3-Dichloropropene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

4-Methyl-2-pentanone BRL 8.2 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Toluene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

trans-1,3-Dichloropropene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,1,2-Trichloroethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

2-Hexanone BRL 8.2 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Tetrachloroethene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Dibromochloromethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,2-Dibromoethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Chlorobenzene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Ethylbenzene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Styrene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Bromoform BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

24 of 80

1101566-006

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 3:10:00 PM

SB-6

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5035)Volatile Organic Compounds by GC/MS SW8260B

1,1,2,2-Tetrachloroethane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Isopropylbenzene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Naphthalene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,3-Dichlorobenzene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,4-Dichlorobenzene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,2-Dichlorobenzene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,2-Dibromo-3-chloropropane BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

1,2,4-Trichlorobenzene BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Xylenes, Total BRL 4.1 ug/Kg-dry 140584 1 01/13/2011 15:58 JE

Surr: 4-Bromofluorobenzene 95.9 56-137 %REC 140584 1 01/13/2011 15:58 JE

Surr: Dibromofluoromethane 102 73.7-137 %REC 140584 1 01/13/2011 15:58 JE

Surr: Toluene-d8 92.9 69.2-126 %REC 140584 1 01/13/2011 15:58 JE

(SW7471)TOTAL MERCURY SW7471B

Mercury BRL 0.125 mg/Kg-dry 140598 1 01/14/2011 12:10 JY

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2,4,5-Trichlorophenol BRL 2100 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2,4,6-Trichlorophenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2,4-Dichlorophenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2,4-Dimethylphenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2,4-Dinitrophenol BRL 2100 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2,4-Dinitrotoluene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2,6-Dinitrotoluene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2-Chloronaphthalene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2-Chlorophenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2-Methylnaphthalene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2-Methylphenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2-Nitroaniline BRL 2100 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

2-Nitrophenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

3,3´-Dichlorobenzidine BRL 840 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

3-Nitroaniline BRL 2100 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

4,6-Dinitro-2-methylphenol BRL 2100 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

4-Bromophenyl phenyl ether BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

4-Chloro-3-methylphenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

4-Chloroaniline BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

4-Chlorophenyl phenyl ether BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

4-Methylphenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

4-Nitroaniline BRL 2100 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

4-Nitrophenol BRL 2100 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

25 of 80

1101566-006

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 3:10:00 PM

SB-6

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Acenaphthene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Acenaphthylene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Acetophenone BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Anthracene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Atrazine BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Benz(a)anthracene 690 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Benzaldehyde BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Benzo(a)pyrene 570 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Benzo(b)fluoranthene 680 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Benzo(g,h,i)perylene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Benzo(k)fluoranthene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Bis(2-chloroethoxy)methane BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Bis(2-chloroethyl)ether BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Bis(2-chloroisopropyl)ether BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Bis(2-ethylhexyl)phthalate BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Butyl benzyl phthalate BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Caprolactam BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Carbazole BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Chrysene 650 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Di-n-butyl phthalate BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Di-n-octyl phthalate BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Dibenz(a,h)anthracene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Dibenzofuran BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Diethyl phthalate BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Dimethyl phthalate BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Fluoranthene 1500 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Fluorene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Hexachlorobenzene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Hexachlorobutadiene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Hexachlorocyclopentadiene BRL 830 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Hexachloroethane BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Indeno(1,2,3-cd)pyrene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Isophorone BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

N-Nitrosodi-n-propylamine BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

N-Nitrosodiphenylamine BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Naphthalene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Nitrobenzene BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Pentachlorophenol BRL 2100 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Phenanthrene 1200 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Phenol BRL 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Pyrene 1200 420 ug/Kg-dry 140499 1 01/13/2011 20:45 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

26 of 80

1101566-006

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Soil

1/6/2011 3:10:00 PM

SB-6

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3550C)TCL-SEMIVOLATILE ORGANICS SW8270D

Surr: 2,4,6-Tribromophenol 84.4 40.4-136 %REC 140499 1 01/13/2011 20:45 YH

Surr: 2-Fluorobiphenyl 81 48.5-120 %REC 140499 1 01/13/2011 20:45 YH

Surr: 2-Fluorophenol 68.2 36.5-120 %REC 140499 1 01/13/2011 20:45 YH

Surr: 4-Terphenyl-d14 88.5 51-125 %REC 140499 1 01/13/2011 20:45 YH

Surr: Nitrobenzene-d5 72.6 37.6-120 %REC 140499 1 01/13/2011 20:45 YH

Surr: Phenol-d5 77.9 40.1-120 %REC 140499 1 01/13/2011 20:45 YH

(SW3050B) METALS, TOTAL SW6010C

Arsenic BRL 6.10 mg/Kg-dry 140509 1 01/13/2011 17:05 MP

Barium 149 6.10 mg/Kg-dry 140509 1 01/13/2011 17:05 MP

Cadmium BRL 3.05 mg/Kg-dry 140509 1 01/13/2011 17:05 MP

Chromium 10.6 3.05 mg/Kg-dry 140509 1 01/13/2011 17:05 MP

Lead 12.8 6.10 mg/Kg-dry 140509 1 01/13/2011 17:05 MP

Selenium BRL 6.10 mg/Kg-dry 140509 1 01/13/2011 17:05 MP

Silver BRL 3.05 mg/Kg-dry 140509 1 01/13/2011 17:05 MP

PERCENT MOISTURE D2216

Percent Moisture 20.7 0 wt% R188399 1 01/14/2011 10:00 AS

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

27 of 80

1101566-007

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 1:30:00 PM

MW-1

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

1,1,1-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,1,2-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,1-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,1-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,2,4-Trichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,2-Dibromo-3-chloropropane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,2-Dibromoethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,2-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,2-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,2-Dichloropropane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,3-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

1,4-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

2-Butanone BRL 50 ug/L 140641 1 01/14/2011 20:56 JT

2-Hexanone BRL 10 ug/L 140641 1 01/14/2011 20:56 JT

4-Methyl-2-pentanone BRL 10 ug/L 140641 1 01/14/2011 20:56 JT

Acetone BRL 50 ug/L 140641 1 01/14/2011 20:56 JT

Benzene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Bromodichloromethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Bromoform BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Bromomethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Carbon disulfide BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Carbon tetrachloride BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Chlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Chloroethane BRL 10 ug/L 140641 1 01/14/2011 20:56 JT

Chloroform BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Chloromethane BRL 10 ug/L 140641 1 01/14/2011 20:56 JT

cis-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

cis-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Cyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Dibromochloromethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Dichlorodifluoromethane BRL 10 ug/L 140641 1 01/14/2011 20:56 JT

Ethylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Freon-113 BRL 10 ug/L 140641 1 01/14/2011 20:56 JT

Isopropylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Methyl acetate BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Methyl tert-butyl ether BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Methylcyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Methylene chloride BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

n-Heptane BRL 10 N ug/L 140641 1 01/14/2011 20:56 JT

Naphthalene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

28 of 80

1101566-007

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 1:30:00 PM

MW-1

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

Styrene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Tetrachloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Toluene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

trans-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

trans-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Trichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Trichlorofluoromethane BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Vinyl chloride BRL 2.0 ug/L 140641 1 01/14/2011 20:56 JT

Xylenes, Total BRL 5.0 ug/L 140641 1 01/14/2011 20:56 JT

Surr: 4-Bromofluorobenzene 89.8 64.7-130 %REC 140641 1 01/14/2011 20:56 JT

Surr: Dibromofluoromethane 90.8 80.7-129 %REC 140641 1 01/14/2011 20:56 JT

Surr: Toluene-d8 85.4 71.1-120 %REC 140641 1 01/14/2011 20:56 JT

(SW3005A)Total Metals by ICP/MS SW6020A

Arsenic BRL 5.00 ug/L 140528 1 01/15/2011 08:07 MW

Barium 56.9 10.0 ug/L 140528 1 01/15/2011 08:07 MW

Cadmium BRL 0.700 ug/L 140528 1 01/15/2011 08:07 MW

Chromium 6.59 5.00 ug/L 140528 1 01/15/2011 08:07 MW

Lead 1.88 1.00 ug/L 140528 1 01/15/2011 08:07 MW

Selenium BRL 5.00 ug/L 140528 1 01/15/2011 08:07 MW

Silver BRL 1.00 ug/L 140528 1 01/15/2011 08:07 MW

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2,4,5-Trichlorophenol BRL 25 ug/L 140453 1 01/13/2011 19:04 YH

2,4,6-Trichlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2,4-Dichlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2,4-Dimethylphenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2,4-Dinitrophenol BRL 25 ug/L 140453 1 01/13/2011 19:04 YH

2,4-Dinitrotoluene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2,6-Dinitrotoluene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2-Chloronaphthalene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2-Chlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2-Methylnaphthalene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2-Methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

2-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:04 YH

2-Nitrophenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

3,3´-Dichlorobenzidine BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

3-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:04 YH

4,6-Dinitro-2-methylphenol BRL 25 ug/L 140453 1 01/13/2011 19:04 YH

4-Bromophenyl phenyl ether BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

29 of 80

1101566-007

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 1:30:00 PM

MW-1

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

4-Chloro-3-methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

4-Chloroaniline BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

4-Chlorophenyl phenyl ether BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

4-Methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

4-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:04 YH

4-Nitrophenol BRL 25 ug/L 140453 1 01/13/2011 19:04 YH

Acenaphthene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Acenaphthylene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Acetophenone BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Anthracene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Atrazine BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Benz(a)anthracene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Benzaldehyde BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Benzo(a)pyrene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Benzo(b)fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Benzo(g,h,i)perylene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Benzo(k)fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Bis(2-chloroethoxy)methane BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Bis(2-chloroethyl)ether BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Bis(2-chloroisopropyl)ether BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Bis(2-ethylhexyl)phthalate BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Butyl benzyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Caprolactam BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Carbazole BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Chrysene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Di-n-butyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Di-n-octyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Dibenz(a,h)anthracene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Dibenzofuran BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Diethyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Dimethyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Fluorene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Hexachlorobenzene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Hexachlorobutadiene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Hexachlorocyclopentadiene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Hexachloroethane BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Indeno(1,2,3-cd)pyrene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Isophorone BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

N-Nitrosodi-n-propylamine BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

N-Nitrosodiphenylamine BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

30 of 80

1101566-007

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 1:30:00 PM

MW-1

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

Naphthalene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Nitrobenzene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Pentachlorophenol BRL 25 ug/L 140453 1 01/13/2011 19:04 YH

Phenanthrene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Phenol BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Pyrene BRL 10 ug/L 140453 1 01/13/2011 19:04 YH

Surr: 2,4,6-Tribromophenol 88 42.2-151 %REC 140453 1 01/13/2011 19:04 YH

Surr: 2-Fluorobiphenyl 82.7 48.2-124 %REC 140453 1 01/13/2011 19:04 YH

Surr: 2-Fluorophenol 54.6 21.6-120 %REC 140453 1 01/13/2011 19:04 YH

Surr: 4-Terphenyl-d14 67.4 40.8-141 %REC 140453 1 01/13/2011 19:04 YH

Surr: Nitrobenzene-d5 78.6 40.2-126 %REC 140453 1 01/13/2011 19:04 YH

Surr: Phenol-d5 37.9 6.98-120 %REC 140453 1 01/13/2011 19:04 YH

(SW7470)Mercury, Total SW7470A

Mercury BRL 0.00020 mg/L 140538 1 01/13/2011 14:44 JY

(SW7470)Mercury, Dissolved SW7470A

Mercury BRL 0.00020 mg/L 140478 1 01/12/2011 17:15 JY

(SAMP_FILT)Dissolved Metals by ICP/MS SW6020A

Arsenic BRL 5.00 ug/L 140533 1 01/15/2011 06:46 MW

Barium 38.4 10.0 ug/L 140533 1 01/15/2011 06:46 MW

Cadmium BRL 0.700 ug/L 140533 1 01/15/2011 06:46 MW

Chromium BRL 5.00 ug/L 140533 1 01/15/2011 06:46 MW

Lead BRL 1.00 ug/L 140533 1 01/15/2011 06:46 MW

Selenium BRL 5.00 ug/L 140533 1 01/15/2011 06:46 MW

Silver BRL 1.00 ug/L 140533 1 01/15/2011 06:46 MW

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

31 of 80

1101566-008

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 2:30:00 PM

MW-2

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

1,1,1-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,1,2-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,1-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,1-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,2,4-Trichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,2-Dibromo-3-chloropropane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,2-Dibromoethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,2-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,2-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,2-Dichloropropane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,3-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

1,4-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

2-Butanone BRL 50 ug/L 140641 1 01/14/2011 21:25 JT

2-Hexanone BRL 10 ug/L 140641 1 01/14/2011 21:25 JT

4-Methyl-2-pentanone BRL 10 ug/L 140641 1 01/14/2011 21:25 JT

Acetone BRL 50 ug/L 140641 1 01/14/2011 21:25 JT

Benzene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Bromodichloromethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Bromoform BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Bromomethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Carbon disulfide BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Carbon tetrachloride BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Chlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Chloroethane BRL 10 ug/L 140641 1 01/14/2011 21:25 JT

Chloroform BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Chloromethane BRL 10 ug/L 140641 1 01/14/2011 21:25 JT

cis-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

cis-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Cyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Dibromochloromethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Dichlorodifluoromethane BRL 10 ug/L 140641 1 01/14/2011 21:25 JT

Ethylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Freon-113 BRL 10 ug/L 140641 1 01/14/2011 21:25 JT

Isopropylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Methyl acetate BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Methyl tert-butyl ether BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Methylcyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Methylene chloride BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

n-Heptane BRL 10 N ug/L 140641 1 01/14/2011 21:25 JT

Naphthalene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

32 of 80

1101566-008

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 2:30:00 PM

MW-2

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

Styrene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Tetrachloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Toluene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

trans-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

trans-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Trichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Trichlorofluoromethane BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Vinyl chloride BRL 2.0 ug/L 140641 1 01/14/2011 21:25 JT

Xylenes, Total BRL 5.0 ug/L 140641 1 01/14/2011 21:25 JT

Surr: 4-Bromofluorobenzene 84.7 64.7-130 %REC 140641 1 01/14/2011 21:25 JT

Surr: Dibromofluoromethane 97.7 80.7-129 %REC 140641 1 01/14/2011 21:25 JT

Surr: Toluene-d8 87.6 71.1-120 %REC 140641 1 01/14/2011 21:25 JT

(SW3005A)Total Metals by ICP/MS SW6020A

Arsenic BRL 5.00 ug/L 140528 1 01/15/2011 08:13 MW

Barium 192 10.0 ug/L 140528 1 01/15/2011 08:13 MW

Cadmium BRL 0.700 ug/L 140528 1 01/15/2011 08:13 MW

Chromium 64.5 5.00 ug/L 140528 1 01/15/2011 08:13 MW

Lead 2.99 1.00 ug/L 140528 1 01/15/2011 08:13 MW

Selenium BRL 5.00 ug/L 140528 1 01/15/2011 08:13 MW

Silver BRL 1.00 ug/L 140528 1 01/15/2011 08:13 MW

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2,4,5-Trichlorophenol BRL 25 ug/L 140453 1 01/13/2011 19:29 YH

2,4,6-Trichlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2,4-Dichlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2,4-Dimethylphenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2,4-Dinitrophenol BRL 25 ug/L 140453 1 01/13/2011 19:29 YH

2,4-Dinitrotoluene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2,6-Dinitrotoluene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2-Chloronaphthalene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2-Chlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2-Methylnaphthalene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2-Methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

2-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:29 YH

2-Nitrophenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

3,3´-Dichlorobenzidine BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

3-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:29 YH

4,6-Dinitro-2-methylphenol BRL 25 ug/L 140453 1 01/13/2011 19:29 YH

4-Bromophenyl phenyl ether BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

33 of 80

1101566-008

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 2:30:00 PM

MW-2

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

4-Chloro-3-methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

4-Chloroaniline BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

4-Chlorophenyl phenyl ether BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

4-Methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

4-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:29 YH

4-Nitrophenol BRL 25 ug/L 140453 1 01/13/2011 19:29 YH

Acenaphthene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Acenaphthylene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Acetophenone BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Anthracene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Atrazine BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Benz(a)anthracene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Benzaldehyde BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Benzo(a)pyrene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Benzo(b)fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Benzo(g,h,i)perylene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Benzo(k)fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Bis(2-chloroethoxy)methane BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Bis(2-chloroethyl)ether BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Bis(2-chloroisopropyl)ether BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Bis(2-ethylhexyl)phthalate BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Butyl benzyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Caprolactam BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Carbazole BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Chrysene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Di-n-butyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Di-n-octyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Dibenz(a,h)anthracene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Dibenzofuran BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Diethyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Dimethyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Fluorene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Hexachlorobenzene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Hexachlorobutadiene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Hexachlorocyclopentadiene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Hexachloroethane BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Indeno(1,2,3-cd)pyrene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Isophorone BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

N-Nitrosodi-n-propylamine BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

N-Nitrosodiphenylamine BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

34 of 80

1101566-008

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 2:30:00 PM

MW-2

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

Naphthalene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Nitrobenzene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Pentachlorophenol BRL 25 ug/L 140453 1 01/13/2011 19:29 YH

Phenanthrene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Phenol BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Pyrene BRL 10 ug/L 140453 1 01/13/2011 19:29 YH

Surr: 2,4,6-Tribromophenol 90.8 42.2-151 %REC 140453 1 01/13/2011 19:29 YH

Surr: 2-Fluorobiphenyl 85.2 48.2-124 %REC 140453 1 01/13/2011 19:29 YH

Surr: 2-Fluorophenol 60.2 21.6-120 %REC 140453 1 01/13/2011 19:29 YH

Surr: 4-Terphenyl-d14 69.5 40.8-141 %REC 140453 1 01/13/2011 19:29 YH

Surr: Nitrobenzene-d5 82.9 40.2-126 %REC 140453 1 01/13/2011 19:29 YH

Surr: Phenol-d5 41.4 6.98-120 %REC 140453 1 01/13/2011 19:29 YH

(SW7470)Mercury, Total SW7470A

Mercury BRL 0.00020 mg/L 140538 1 01/13/2011 14:46 JY

(SW7470)Mercury, Dissolved SW7470A

Mercury BRL 0.00020 mg/L 140478 1 01/12/2011 17:17 JY

(SAMP_FILT)Dissolved Metals by ICP/MS SW6020A

Arsenic BRL 5.00 ug/L 140533 1 01/15/2011 06:52 MW

Barium 39.7 10.0 ug/L 140533 1 01/15/2011 06:52 MW

Cadmium BRL 0.700 ug/L 140533 1 01/15/2011 06:52 MW

Chromium BRL 5.00 ug/L 140533 1 01/15/2011 06:52 MW

Lead BRL 1.00 ug/L 140533 1 01/15/2011 06:52 MW

Selenium BRL 5.00 ug/L 140533 1 01/15/2011 06:52 MW

Silver BRL 1.00 ug/L 140533 1 01/15/2011 06:52 MW

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

35 of 80

1101566-009

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 3:45:00 PM

MW-3

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

1,1,1-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,1,2-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,1-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,1-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,2,4-Trichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,2-Dibromo-3-chloropropane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,2-Dibromoethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,2-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,2-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,2-Dichloropropane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,3-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

1,4-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

2-Butanone BRL 50 ug/L 140641 1 01/14/2011 21:53 JT

2-Hexanone BRL 10 ug/L 140641 1 01/14/2011 21:53 JT

4-Methyl-2-pentanone BRL 10 ug/L 140641 1 01/14/2011 21:53 JT

Acetone BRL 50 ug/L 140641 1 01/14/2011 21:53 JT

Benzene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Bromodichloromethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Bromoform BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Bromomethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Carbon disulfide BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Carbon tetrachloride BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Chlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Chloroethane BRL 10 ug/L 140641 1 01/14/2011 21:53 JT

Chloroform BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Chloromethane BRL 10 ug/L 140641 1 01/14/2011 21:53 JT

cis-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

cis-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Cyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Dibromochloromethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Dichlorodifluoromethane BRL 10 ug/L 140641 1 01/14/2011 21:53 JT

Ethylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Freon-113 BRL 10 ug/L 140641 1 01/14/2011 21:53 JT

Isopropylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Methyl acetate BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Methyl tert-butyl ether BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Methylcyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Methylene chloride BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

n-Heptane BRL 10 N ug/L 140641 1 01/14/2011 21:53 JT

Naphthalene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

36 of 80

1101566-009

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 3:45:00 PM

MW-3

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

Styrene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Tetrachloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Toluene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

trans-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

trans-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Trichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Trichlorofluoromethane BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Vinyl chloride BRL 2.0 ug/L 140641 1 01/14/2011 21:53 JT

Xylenes, Total BRL 5.0 ug/L 140641 1 01/14/2011 21:53 JT

Surr: 4-Bromofluorobenzene 80.1 64.7-130 %REC 140641 1 01/14/2011 21:53 JT

Surr: Dibromofluoromethane 95.1 80.7-129 %REC 140641 1 01/14/2011 21:53 JT

Surr: Toluene-d8 86.9 71.1-120 %REC 140641 1 01/14/2011 21:53 JT

(SW3005A)Total Metals by ICP/MS SW6020A

Arsenic BRL 5.00 ug/L 140528 1 01/15/2011 08:19 MW

Barium 58.6 10.0 ug/L 140528 1 01/15/2011 08:19 MW

Cadmium BRL 0.700 ug/L 140528 1 01/15/2011 08:19 MW

Chromium BRL 5.00 ug/L 140528 1 01/15/2011 08:19 MW

Lead 1.28 1.00 ug/L 140528 1 01/15/2011 08:19 MW

Selenium BRL 5.00 ug/L 140528 1 01/15/2011 08:19 MW

Silver BRL 1.00 ug/L 140528 1 01/15/2011 08:19 MW

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2,4,5-Trichlorophenol BRL 25 ug/L 140453 1 01/13/2011 19:54 YH

2,4,6-Trichlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2,4-Dichlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2,4-Dimethylphenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2,4-Dinitrophenol BRL 25 ug/L 140453 1 01/13/2011 19:54 YH

2,4-Dinitrotoluene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2,6-Dinitrotoluene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2-Chloronaphthalene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2-Chlorophenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2-Methylnaphthalene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2-Methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

2-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:54 YH

2-Nitrophenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

3,3´-Dichlorobenzidine BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

3-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:54 YH

4,6-Dinitro-2-methylphenol BRL 25 ug/L 140453 1 01/13/2011 19:54 YH

4-Bromophenyl phenyl ether BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

37 of 80

1101566-009

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 3:45:00 PM

MW-3

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

4-Chloro-3-methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

4-Chloroaniline BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

4-Chlorophenyl phenyl ether BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

4-Methylphenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

4-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 19:54 YH

4-Nitrophenol BRL 25 ug/L 140453 1 01/13/2011 19:54 YH

Acenaphthene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Acenaphthylene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Acetophenone BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Anthracene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Atrazine BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Benz(a)anthracene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Benzaldehyde BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Benzo(a)pyrene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Benzo(b)fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Benzo(g,h,i)perylene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Benzo(k)fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Bis(2-chloroethoxy)methane BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Bis(2-chloroethyl)ether BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Bis(2-chloroisopropyl)ether BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Bis(2-ethylhexyl)phthalate BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Butyl benzyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Caprolactam BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Carbazole BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Chrysene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Di-n-butyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Di-n-octyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Dibenz(a,h)anthracene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Dibenzofuran BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Diethyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Dimethyl phthalate BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Fluoranthene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Fluorene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Hexachlorobenzene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Hexachlorobutadiene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Hexachlorocyclopentadiene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Hexachloroethane BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Indeno(1,2,3-cd)pyrene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Isophorone BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

N-Nitrosodi-n-propylamine BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

N-Nitrosodiphenylamine BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

38 of 80

1101566-009

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 3:45:00 PM

MW-3

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

Naphthalene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Nitrobenzene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Pentachlorophenol BRL 25 ug/L 140453 1 01/13/2011 19:54 YH

Phenanthrene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Phenol BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Pyrene BRL 10 ug/L 140453 1 01/13/2011 19:54 YH

Surr: 2,4,6-Tribromophenol 85.2 42.2-151 %REC 140453 1 01/13/2011 19:54 YH

Surr: 2-Fluorobiphenyl 82.7 48.2-124 %REC 140453 1 01/13/2011 19:54 YH

Surr: 2-Fluorophenol 55.2 21.6-120 %REC 140453 1 01/13/2011 19:54 YH

Surr: 4-Terphenyl-d14 70 40.8-141 %REC 140453 1 01/13/2011 19:54 YH

Surr: Nitrobenzene-d5 78.3 40.2-126 %REC 140453 1 01/13/2011 19:54 YH

Surr: Phenol-d5 37.3 6.98-120 %REC 140453 1 01/13/2011 19:54 YH

(SW7470)Mercury, Total SW7470A

Mercury BRL 0.00020 mg/L 140538 1 01/13/2011 14:21 JY

(SW7470)Mercury, Dissolved SW7470A

Mercury BRL 0.00020 mg/L 140478 1 01/12/2011 17:19 JY

(SAMP_FILT)Dissolved Metals by ICP/MS SW6020A

Arsenic BRL 5.00 ug/L 140533 1 01/15/2011 05:56 MW

Barium 51.2 10.0 ug/L 140533 1 01/15/2011 05:56 MW

Cadmium BRL 0.700 ug/L 140533 1 01/15/2011 05:56 MW

Chromium BRL 5.00 ug/L 140533 1 01/15/2011 05:56 MW

Lead BRL 1.00 ug/L 140533 1 01/15/2011 05:56 MW

Selenium BRL 5.00 ug/L 140533 1 01/15/2011 05:56 MW

Silver BRL 1.00 ug/L 140533 1 01/15/2011 05:56 MW

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

39 of 80

1101566-010

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 4:20:00 PM

MW-4

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

1,1,1-Trichloroethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,1,2-Trichloroethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,1-Dichloroethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,1-Dichloroethene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,2,4-Trichlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,2-Dibromo-3-chloropropane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,2-Dibromoethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,2-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,2-Dichloroethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,2-Dichloropropane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,3-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

1,4-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

2-Butanone BRL 50 ug/L 140641 1 01/17/2011 11:33 JT

2-Hexanone BRL 10 ug/L 140641 1 01/17/2011 11:33 JT

4-Methyl-2-pentanone BRL 10 ug/L 140641 1 01/17/2011 11:33 JT

Acetone BRL 50 ug/L 140641 1 01/17/2011 11:33 JT

Benzene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Bromodichloromethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Bromoform BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Bromomethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Carbon disulfide BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Carbon tetrachloride BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Chlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Chloroethane BRL 10 ug/L 140641 1 01/17/2011 11:33 JT

Chloroform BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Chloromethane BRL 10 ug/L 140641 1 01/17/2011 11:33 JT

cis-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

cis-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Cyclohexane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Dibromochloromethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Dichlorodifluoromethane BRL 10 ug/L 140641 1 01/17/2011 11:33 JT

Ethylbenzene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Freon-113 BRL 10 ug/L 140641 1 01/17/2011 11:33 JT

Isopropylbenzene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Methyl acetate BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Methyl tert-butyl ether BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Methylcyclohexane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Methylene chloride BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

n-Heptane BRL 10 N ug/L 140641 1 01/17/2011 11:33 JT

Naphthalene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

40 of 80

1101566-010

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 4:20:00 PM

MW-4

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

Styrene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Tetrachloroethene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Toluene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

trans-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

trans-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Trichloroethene BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Trichlorofluoromethane BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Vinyl chloride BRL 2.0 ug/L 140641 1 01/17/2011 11:33 JT

Xylenes, Total BRL 5.0 ug/L 140641 1 01/17/2011 11:33 JT

Surr: 4-Bromofluorobenzene 82.3 64.7-130 %REC 140641 1 01/17/2011 11:33 JT

Surr: Dibromofluoromethane 98.9 80.7-129 %REC 140641 1 01/17/2011 11:33 JT

Surr: Toluene-d8 89 71.1-120 %REC 140641 1 01/17/2011 11:33 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

41 of 80

1101566-011

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 4:30:00 PM

MW-5

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

1,1,1-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,1,2-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,1-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,1-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,2,4-Trichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,2-Dibromo-3-chloropropane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,2-Dibromoethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,2-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,2-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,2-Dichloropropane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,3-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

1,4-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

2-Butanone BRL 50 ug/L 140641 1 01/14/2011 22:22 JT

2-Hexanone BRL 10 ug/L 140641 1 01/14/2011 22:22 JT

4-Methyl-2-pentanone BRL 10 ug/L 140641 1 01/14/2011 22:22 JT

Acetone BRL 50 ug/L 140641 1 01/14/2011 22:22 JT

Benzene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Bromodichloromethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Bromoform BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Bromomethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Carbon disulfide BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Carbon tetrachloride BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Chlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Chloroethane BRL 10 ug/L 140641 1 01/14/2011 22:22 JT

Chloroform BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Chloromethane BRL 10 ug/L 140641 1 01/14/2011 22:22 JT

cis-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

cis-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Cyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Dibromochloromethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Dichlorodifluoromethane BRL 10 ug/L 140641 1 01/14/2011 22:22 JT

Ethylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Freon-113 BRL 10 ug/L 140641 1 01/14/2011 22:22 JT

Isopropylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Methyl acetate BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Methyl tert-butyl ether BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Methylcyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Methylene chloride BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

n-Heptane BRL 10 N ug/L 140641 1 01/14/2011 22:22 JT

Naphthalene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

42 of 80

1101566-011

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 4:30:00 PM

MW-5

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

Styrene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Tetrachloroethene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Toluene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

trans-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

trans-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Trichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Trichlorofluoromethane BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Vinyl chloride BRL 2.0 ug/L 140641 1 01/14/2011 22:22 JT

Xylenes, Total BRL 5.0 ug/L 140641 1 01/14/2011 22:22 JT

Surr: 4-Bromofluorobenzene 86.4 64.7-130 %REC 140641 1 01/14/2011 22:22 JT

Surr: Dibromofluoromethane 102 80.7-129 %REC 140641 1 01/14/2011 22:22 JT

Surr: Toluene-d8 92.4 71.1-120 %REC 140641 1 01/14/2011 22:22 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

43 of 80

1101566-012

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 4:50:00 PM

MW-6

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

1,1,1-Trichloroethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,1,2-Trichloroethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,1-Dichloroethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,1-Dichloroethene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,2,4-Trichlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,2-Dibromo-3-chloropropane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,2-Dibromoethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,2-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,2-Dichloroethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,2-Dichloropropane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,3-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

1,4-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

2-Butanone BRL 50 ug/L 140641 1 01/17/2011 12:01 JT

2-Hexanone BRL 10 ug/L 140641 1 01/17/2011 12:01 JT

4-Methyl-2-pentanone BRL 10 ug/L 140641 1 01/17/2011 12:01 JT

Acetone BRL 50 ug/L 140641 1 01/17/2011 12:01 JT

Benzene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Bromodichloromethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Bromoform BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Bromomethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Carbon disulfide BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Carbon tetrachloride BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Chlorobenzene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Chloroethane BRL 10 ug/L 140641 1 01/17/2011 12:01 JT

Chloroform BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Chloromethane BRL 10 ug/L 140641 1 01/17/2011 12:01 JT

cis-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

cis-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Cyclohexane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Dibromochloromethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Dichlorodifluoromethane BRL 10 ug/L 140641 1 01/17/2011 12:01 JT

Ethylbenzene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Freon-113 BRL 10 ug/L 140641 1 01/17/2011 12:01 JT

Isopropylbenzene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Methyl acetate BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Methyl tert-butyl ether BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Methylcyclohexane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Methylene chloride BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

n-Heptane BRL 10 N ug/L 140641 1 01/17/2011 12:01 JT

Naphthalene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

44 of 80

1101566-012

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 4:50:00 PM

MW-6

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

Styrene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Tetrachloroethene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Toluene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

trans-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

trans-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Trichloroethene BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Trichlorofluoromethane BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Vinyl chloride BRL 2.0 ug/L 140641 1 01/17/2011 12:01 JT

Xylenes, Total BRL 5.0 ug/L 140641 1 01/17/2011 12:01 JT

Surr: 4-Bromofluorobenzene 82.3 64.7-130 %REC 140641 1 01/17/2011 12:01 JT

Surr: Dibromofluoromethane 104 80.7-129 %REC 140641 1 01/17/2011 12:01 JT

Surr: Toluene-d8 88 71.1-120 %REC 140641 1 01/17/2011 12:01 JT

(SW3005A)Total Metals by ICP/MS SW6020A

Arsenic BRL 5.00 ug/L 140528 1 01/15/2011 07:17 MW

Barium 63.1 10.0 ug/L 140528 1 01/15/2011 07:17 MW

Cadmium BRL 0.700 ug/L 140528 1 01/15/2011 07:17 MW

Chromium 5.92 5.00 ug/L 140528 1 01/15/2011 07:17 MW

Lead 1.56 1.00 ug/L 140528 1 01/15/2011 07:17 MW

Selenium BRL 5.00 ug/L 140528 1 01/15/2011 07:17 MW

Silver BRL 1.00 ug/L 140528 1 01/15/2011 07:17 MW

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

1,1´-Biphenyl BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2,4,5-Trichlorophenol BRL 25 ug/L 140453 1 01/13/2011 20:20 YH

2,4,6-Trichlorophenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2,4-Dichlorophenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2,4-Dimethylphenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2,4-Dinitrophenol BRL 25 ug/L 140453 1 01/13/2011 20:20 YH

2,4-Dinitrotoluene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2,6-Dinitrotoluene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2-Chloronaphthalene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2-Chlorophenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2-Methylnaphthalene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2-Methylphenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

2-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 20:20 YH

2-Nitrophenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

3,3´-Dichlorobenzidine BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

3-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 20:20 YH

4,6-Dinitro-2-methylphenol BRL 25 ug/L 140453 1 01/13/2011 20:20 YH

4-Bromophenyl phenyl ether BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

45 of 80

1101566-012

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 4:50:00 PM

MW-6

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

4-Chloro-3-methylphenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

4-Chloroaniline BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

4-Chlorophenyl phenyl ether BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

4-Methylphenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

4-Nitroaniline BRL 25 ug/L 140453 1 01/13/2011 20:20 YH

4-Nitrophenol BRL 25 ug/L 140453 1 01/13/2011 20:20 YH

Acenaphthene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Acenaphthylene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Acetophenone BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Anthracene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Atrazine BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Benz(a)anthracene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Benzaldehyde BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Benzo(a)pyrene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Benzo(b)fluoranthene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Benzo(g,h,i)perylene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Benzo(k)fluoranthene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Bis(2-chloroethoxy)methane BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Bis(2-chloroethyl)ether BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Bis(2-chloroisopropyl)ether BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Bis(2-ethylhexyl)phthalate BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Butyl benzyl phthalate BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Caprolactam BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Carbazole BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Chrysene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Di-n-butyl phthalate BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Di-n-octyl phthalate BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Dibenz(a,h)anthracene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Dibenzofuran BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Diethyl phthalate BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Dimethyl phthalate BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Fluoranthene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Fluorene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Hexachlorobenzene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Hexachlorobutadiene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Hexachlorocyclopentadiene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Hexachloroethane BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Indeno(1,2,3-cd)pyrene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Isophorone BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

N-Nitrosodi-n-propylamine BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

N-Nitrosodiphenylamine BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

46 of 80

1101566-012

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Groundwater

1/6/2011 4:50:00 PM

MW-6

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW3510B)TCL-SEMIVOLATILE ORGANICS SW8270D

Naphthalene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Nitrobenzene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Pentachlorophenol BRL 25 ug/L 140453 1 01/13/2011 20:20 YH

Phenanthrene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Phenol BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Pyrene BRL 10 ug/L 140453 1 01/13/2011 20:20 YH

Surr: 2,4,6-Tribromophenol 93.2 42.2-151 %REC 140453 1 01/13/2011 20:20 YH

Surr: 2-Fluorobiphenyl 86.1 48.2-124 %REC 140453 1 01/13/2011 20:20 YH

Surr: 2-Fluorophenol 61.3 21.6-120 %REC 140453 1 01/13/2011 20:20 YH

Surr: 4-Terphenyl-d14 81.1 40.8-141 %REC 140453 1 01/13/2011 20:20 YH

Surr: Nitrobenzene-d5 81.1 40.2-126 %REC 140453 1 01/13/2011 20:20 YH

Surr: Phenol-d5 42.4 6.98-120 %REC 140453 1 01/13/2011 20:20 YH

(SW7470)Mercury, Total SW7470A

Mercury BRL 0.00020 mg/L 140538 1 01/13/2011 14:28 JY

(SW7470)Mercury, Dissolved SW7470A

Mercury BRL 0.00020 mg/L 140478 1 01/12/2011 17:20 JY

(SAMP_FILT)Dissolved Metals by ICP/MS SW6020A

Arsenic BRL 5.00 ug/L 140533 1 01/15/2011 06:58 MW

Barium 44.6 10.0 ug/L 140533 1 01/15/2011 06:58 MW

Cadmium BRL 0.700 ug/L 140533 1 01/15/2011 06:58 MW

Chromium BRL 5.00 ug/L 140533 1 01/15/2011 06:58 MW

Lead BRL 1.00 ug/L 140533 1 01/15/2011 06:58 MW

Selenium BRL 5.00 ug/L 140533 1 01/15/2011 06:58 MW

Silver BRL 1.00 ug/L 140533 1 01/15/2011 06:58 MW

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

47 of 80

1101566-013

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Aqueous

1/6/2011

TRIP BLANK

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

1,1,1-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,1,2-Trichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,1-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,1-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,2,4-Trichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,2-Dibromo-3-chloropropane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,2-Dibromoethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,2-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,2-Dichloroethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,2-Dichloropropane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,3-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

1,4-Dichlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

2-Butanone BRL 50 ug/L 140641 1 01/14/2011 20:28 JT

2-Hexanone BRL 10 ug/L 140641 1 01/14/2011 20:28 JT

4-Methyl-2-pentanone BRL 10 ug/L 140641 1 01/14/2011 20:28 JT

Acetone BRL 50 ug/L 140641 1 01/14/2011 20:28 JT

Benzene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Bromodichloromethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Bromoform BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Bromomethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Carbon disulfide BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Carbon tetrachloride BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Chlorobenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Chloroethane BRL 10 ug/L 140641 1 01/14/2011 20:28 JT

Chloroform BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Chloromethane BRL 10 ug/L 140641 1 01/14/2011 20:28 JT

cis-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

cis-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Cyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Dibromochloromethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Dichlorodifluoromethane BRL 10 ug/L 140641 1 01/14/2011 20:28 JT

Ethylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Freon-113 BRL 10 ug/L 140641 1 01/14/2011 20:28 JT

Isopropylbenzene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Methyl acetate BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Methyl tert-butyl ether BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Methylcyclohexane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Methylene chloride BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

n-Heptane BRL 10 N ug/L 140641 1 01/14/2011 20:28 JT

Naphthalene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

48 of 80

1101566-013

17-Jan-11Date:Analytical Environmental Services, Inc

Analyses Date AnalyzedDilution

FactorBatchIDUnitsQual

Reporting

LimitResult

Client:

Aqueous

1/6/2011

TRIP BLANK

Matrix:

Collection Date:

Client Sample ID:

VWT, Inc

HRP Associates, inc.

Lab ID:

Project:

Analyst

(SW5030B)Volatile Organic Compounds by GC/MS SW8260B

Styrene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Tetrachloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Toluene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

trans-1,2-Dichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

trans-1,3-Dichloropropene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Trichloroethene BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Trichlorofluoromethane BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Vinyl chloride BRL 2.0 ug/L 140641 1 01/14/2011 20:28 JT

Xylenes, Total BRL 5.0 ug/L 140641 1 01/14/2011 20:28 JT

Surr: 4-Bromofluorobenzene 89.5 64.7-130 %REC 140641 1 01/14/2011 20:28 JT

Surr: Dibromofluoromethane 93.5 80.7-129 %REC 140641 1 01/14/2011 20:28 JT

Surr: Toluene-d8 86.5 71.1-120 %REC 140641 1 01/14/2011 20:28 JT

Qualifiers: * Value exceeds maximum contaminant level

BRL Below reporting limit

H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

Narr See case narrative

NC Not confirmed

< Less than Result value

> Greater than Result value

49 of 80

50 of 80

Sample ID Client Sample ID Collection Date Matrix Analysis Date

DATES REPORT

18-Jan-11

Lab Order: 1101566

Client: HRP Associates, inc.

Project: VWT, Inc

Analytical Environmental Services, Inc.

Test Name Prep DateTCLP Date

1101566-001A SB-1 1/6/2011 9:50:00 AM Soil Volatile Organic Compounds by GC/MS 1/13/20111/13/2011

1101566-001B PERCENT MOISTURE 1/14/2011

1101566-001C MERCURY 1/14/20111/14/2011

TCL-SEMIVOLATILE ORGANICS 1/13/20111/12/2011

TOTAL METALS BY ICP 1/13/20111/12/2011

1101566-002A SB-2 1/6/2011 10:55:00 AM Volatile Organic Compounds by GC/MS 1/13/20111/13/2011

1101566-002B PERCENT MOISTURE 1/14/2011

1101566-002C MERCURY 1/14/20111/14/2011

TCL-SEMIVOLATILE ORGANICS 1/13/20111/12/2011

TOTAL METALS BY ICP 1/13/20111/12/2011

1101566-003A SB-3 1/6/2011 11:40:00 AM Volatile Organic Compounds by GC/MS 1/13/20111/13/2011

1101566-003B PERCENT MOISTURE 1/14/2011

1101566-003C MERCURY 1/14/20111/14/2011

TCL-SEMIVOLATILE ORGANICS 1/12/20111/12/2011

TOTAL METALS BY ICP 1/13/20111/12/2011

1101566-004A SB-4 1/6/2011 12:25:00 PM Volatile Organic Compounds by GC/MS 1/13/20111/13/2011

1101566-004B PERCENT MOISTURE 1/14/2011

1101566-004C MERCURY 1/14/20111/14/2011

TCL-SEMIVOLATILE ORGANICS 1/12/20111/12/2011

TOTAL METALS BY ICP 1/13/20111/12/2011

TOTAL METALS BY ICP 1/13/20111/12/2011

1101566-005A SB-5 1/6/2011 1:55:00 PM Volatile Organic Compounds by GC/MS 1/13/20111/13/2011

1101566-005B PERCENT MOISTURE 1/14/2011

1101566-005C MERCURY 1/14/20111/14/2011

TCL-SEMIVOLATILE ORGANICS 1/12/20111/12/2011

TOTAL METALS BY ICP 1/13/20111/12/2011

1101566-006A SB-6 1/6/2011 3:10:00 PM Volatile Organic Compounds by GC/MS 1/13/20111/13/2011

1101566-006B PERCENT MOISTURE 1/14/2011

Page 1 of 3

51 of 80

Sample ID Client Sample ID Collection Date Matrix Analysis Date

DATES REPORT

18-Jan-11

Lab Order: 1101566

Client: HRP Associates, inc.

Project: VWT, Inc

Analytical Environmental Services, Inc.

Test Name Prep DateTCLP Date

1101566-006C SB-6 1/6/2011 3:10:00 PM Soil MERCURY 1/14/20111/14/2011

TCL-SEMIVOLATILE ORGANICS 1/13/20111/12/2011

TOTAL METALS BY ICP 1/13/20111/12/2011

1101566-007A MW-1 1/6/2011 1:30:00 PM Groundwater Volatile Organic Compounds by GC/MS 1/14/20111/14/2011

1101566-007B TCL-SEMIVOLATILE ORGANICS 1/13/20111/12/2011

1101566-007C TOTAL MERCURY 1/13/20111/13/2011

Total Metals by ICP/MS 1/15/20111/13/2011

1101566-007D Dissolved Metals by ICP/MS 1/15/20111/13/2011

MERCURY, DISSOLVED 1/12/20111/12/2011

1101566-008A MW-2 1/6/2011 2:30:00 PM Volatile Organic Compounds by GC/MS 1/14/20111/14/2011

1101566-008B TCL-SEMIVOLATILE ORGANICS 1/13/20111/12/2011

1101566-008C TOTAL MERCURY 1/13/20111/13/2011

Total Metals by ICP/MS 1/15/20111/13/2011

1101566-008D Dissolved Metals by ICP/MS 1/15/20111/13/2011

MERCURY, DISSOLVED 1/12/20111/12/2011

1101566-009A MW-3 1/6/2011 3:45:00 PM Volatile Organic Compounds by GC/MS 1/14/20111/14/2011

1101566-009B TCL-SEMIVOLATILE ORGANICS 1/13/20111/12/2011

1101566-009C TOTAL MERCURY 1/13/20111/13/2011

Total Metals by ICP/MS 1/15/20111/13/2011

1101566-009D Dissolved Metals by ICP/MS 1/15/20111/13/2011

MERCURY, DISSOLVED 1/12/20111/12/2011

1101566-010A MW-4 1/6/2011 4:20:00 PM Volatile Organic Compounds by GC/MS 1/17/20111/14/2011

1101566-011A MW-5 1/6/2011 4:30:00 PM Volatile Organic Compounds by GC/MS 1/14/20111/14/2011

1101566-012A MW-6 1/6/2011 4:50:00 PM Volatile Organic Compounds by GC/MS 1/17/20111/14/2011

1101566-012B TCL-SEMIVOLATILE ORGANICS 1/13/20111/12/2011

1101566-012C TOTAL MERCURY 1/13/20111/13/2011

Total Metals by ICP/MS 1/15/20111/13/2011

1101566-012D Dissolved Metals by ICP/MS 1/15/20111/13/2011

Page 2 of 3

52 of 80

Sample ID Client Sample ID Collection Date Matrix Analysis Date

DATES REPORT

18-Jan-11

Lab Order: 1101566

Client: HRP Associates, inc.

Project: VWT, Inc

Analytical Environmental Services, Inc.

Test Name Prep DateTCLP Date

1101566-012D MW-6 1/6/2011 4:50:00 PM Groundwater MERCURY, DISSOLVED 1/12/20111/12/2011

1101566-013A TRIP BLANK 1/6/2011 Aqueous Volatile Organic Compounds by GC/MS 1/14/20111/14/2011

Page 3 of 3

53 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140453

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140453MBLK 01/11/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/11/2011 188196MB-140453

3923332

1,1´-Biphenyl 10BRL 00 0 0 0 0 0 0

2,4,5-Trichlorophenol 25BRL 00 0 0 0 0 0 0

2,4,6-Trichlorophenol 10BRL 00 0 0 0 0 0 0

2,4-Dichlorophenol 10BRL 00 0 0 0 0 0 0

2,4-Dimethylphenol 10BRL 00 0 0 0 0 0 0

2,4-Dinitrophenol 25BRL 00 0 0 0 0 0 0

2,4-Dinitrotoluene 10BRL 00 0 0 0 0 0 0

2,6-Dinitrotoluene 10BRL 00 0 0 0 0 0 0

2-Chloronaphthalene 10BRL 00 0 0 0 0 0 0

2-Chlorophenol 10BRL 00 0 0 0 0 0 0

2-Methylnaphthalene 10BRL 00 0 0 0 0 0 0

2-Methylphenol 10BRL 00 0 0 0 0 0 0

2-Nitroaniline 25BRL 00 0 0 0 0 0 0

2-Nitrophenol 10BRL 00 0 0 0 0 0 0

3,3´-Dichlorobenzidine 10BRL 00 0 0 0 0 0 0

3-Nitroaniline 25BRL 00 0 0 0 0 0 0

4,6-Dinitro-2-methylphenol 25BRL 00 0 0 0 0 0 0

4-Bromophenyl phenyl ether 10BRL 00 0 0 0 0 0 0

4-Chloro-3-methylphenol 10BRL 00 0 0 0 0 0 0

4-Chloroaniline 10BRL 00 0 0 0 0 0 0

4-Chlorophenyl phenyl ether 10BRL 00 0 0 0 0 0 0

4-Methylphenol 10BRL 00 0 0 0 0 0 0

4-Nitroaniline 25BRL 00 0 0 0 0 0 0

4-Nitrophenol 25BRL 00 0 0 0 0 0 0

Acenaphthene 10BRL 00 0 0 0 0 0 0

Acenaphthylene 10BRL 00 0 0 0 0 0 0

Acetophenone 10BRL 00 0 0 0 0 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

54 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140453

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140453MBLK 01/11/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/11/2011 188196MB-140453

3923332

Anthracene 10BRL 00 0 0 0 0 0 0

Atrazine 10BRL 00 0 0 0 0 0 0

Benz(a)anthracene 10BRL 00 0 0 0 0 0 0

Benzaldehyde 10BRL 00 0 0 0 0 0 0

Benzo(a)pyrene 10BRL 00 0 0 0 0 0 0

Benzo(b)fluoranthene 10BRL 00 0 0 0 0 0 0

Benzo(g,h,i)perylene 10BRL 00 0 0 0 0 0 0

Benzo(k)fluoranthene 10BRL 00 0 0 0 0 0 0

Bis(2-chloroethoxy)methane 10BRL 00 0 0 0 0 0 0

Bis(2-chloroethyl)ether 10BRL 00 0 0 0 0 0 0

Bis(2-chloroisopropyl)ether 10BRL 00 0 0 0 0 0 0

Bis(2-ethylhexyl)phthalate 10BRL 00 0 0 0 0 0 0

Butyl benzyl phthalate 10BRL 00 0 0 0 0 0 0

Caprolactam 10BRL 00 0 0 0 0 0 0

Carbazole 10BRL 00 0 0 0 0 0 0

Chrysene 10BRL 00 0 0 0 0 0 0

Di-n-butyl phthalate 10BRL 00 0 0 0 0 0 0

Di-n-octyl phthalate 10BRL 00 0 0 0 0 0 0

Dibenz(a,h)anthracene 10BRL 00 0 0 0 0 0 0

Dibenzofuran 10BRL 00 0 0 0 0 0 0

Diethyl phthalate 10BRL 00 0 0 0 0 0 0

Dimethyl phthalate 10BRL 00 0 0 0 0 0 0

Fluoranthene 10BRL 00 0 0 0 0 0 0

Fluorene 10BRL 00 0 0 0 0 0 0

Hexachlorobenzene 10BRL 00 0 0 0 0 0 0

Hexachlorobutadiene 10BRL 00 0 0 0 0 0 0

Hexachlorocyclopentadiene 10BRL 00 0 0 0 0 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

55 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140453

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140453MBLK 01/11/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/11/2011 188196MB-140453

3923332

Hexachloroethane 10BRL 00 0 0 0 0 0 0

Indeno(1,2,3-cd)pyrene 10BRL 00 0 0 0 0 0 0

Isophorone 10BRL 00 0 0 0 0 0 0

N-Nitrosodi-n-propylamine 10BRL 00 0 0 0 0 0 0

N-Nitrosodiphenylamine 10BRL 00 0 0 0 0 0 0

Naphthalene 10BRL 00 0 0 0 0 0 0

Nitrobenzene 10BRL 00 0 0 0 0 0 0

Pentachlorophenol 25BRL 00 0 0 0 0 0 0

Phenanthrene 10BRL 00 0 0 0 0 0 0

Phenol 10BRL 00 0 0 0 0 0 0

Pyrene 10BRL 00 0 0 0 0 0 0

Surr: 2,4,6-Tribromophenol 0102.8 0100 0 103 42.2 151 0 0

Surr: 2-Fluorobiphenyl 045.60 050 0 91.2 48.2 124 0 0

Surr: 2-Fluorophenol 071.53 0100 0 71.5 21.6 120 0 0

Surr: 4-Terphenyl-d14 048.70 050 0 97.4 40.8 141 0 0

Surr: Nitrobenzene-d5 045.17 050 0 90.3 40.2 126 0 0

Surr: Phenol-d5 050.92 0100 0 50.9 6.98 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140453LCS 01/11/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/11/2011 188196LCS-140453

3923334

2,4-Dinitrotoluene 1095.89 0100 0 95.9 66.5 117 0 0

2-Chlorophenol 1089.17 0100 0 89.2 68.1 120 0 0

4-Chloro-3-methylphenol 1092.48 0100 0 92.5 73.8 122 0 0

4-Nitrophenol 2535.17 0100 0 35.2 20.1 120 0 0

Acenaphthene 1091.10 0100 0 91.1 70.7 120 0 0

N-Nitrosodi-n-propylamine 1095.77 0100 0 95.8 62.3 129 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

56 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140453

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140453LCS 01/11/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/11/2011 188196LCS-140453

3923334

Pentachlorophenol 2576.74 0100 0 76.7 48.1 140 0 0

Phenol 1049.61 0100 0 49.6 23 120 0 0

Pyrene 1098.18 0100 0 98.2 72.7 130 0 0

Surr: 2,4,6-Tribromophenol 0104.5 0100 0 104 42.2 151 0 0

Surr: 2-Fluorobiphenyl 047.50 050 0 95 48.2 124 0 0

Surr: 2-Fluorophenol 069.66 0100 0 69.7 21.6 120 0 0

Surr: 4-Terphenyl-d14 051.88 050 0 104 40.8 141 0 0

Surr: Nitrobenzene-d5 046.58 050 0 93.2 40.2 126 0 0

Surr: Phenol-d5 050.74 0100 0 50.7 6.98 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140453MS 01/11/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/11/2011 1881961101421-041EMS

3923336

2,4-Dinitrotoluene 10105.0 0100 0 105 52.3 120 0 0

2-Chlorophenol 1097.17 0100 0 97.2 49.1 120 0 0

4-Chloro-3-methylphenol 10109.5 0100 0 109 49.2 129 0 0

4-Nitrophenol 2559.38 0100 0 59.4 24.1 120 0 0

Acenaphthene 10103.8 0100 0 104 54.4 120 0 0

N-Nitrosodi-n-propylamine 10105.1 0100 0 105 45.3 128 0 0

Pentachlorophenol 25107.6 0100 0 108 39.6 147 0 0

Phenol 1063.72 0100 0 63.7 24.8 120 0 0

Pyrene 10108.5 0100 0 109 54 125 0 0

Surr: 2,4,6-Tribromophenol 0119.4 0100 0 119 42.2 151 0 0

Surr: 2-Fluorobiphenyl 053.73 050 0 107 48.2 124 0 0

Surr: 2-Fluorophenol 081.36 0100 0 81.4 21.6 120 0 0

Surr: 4-Terphenyl-d14 055.57 050 0 111 40.8 141 0 0

Surr: Nitrobenzene-d5 050.87 050 0 102 40.2 126 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

57 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140453

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140453MS 01/11/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/11/2011 1881961101421-041EMS

3923336

Surr: Phenol-d5 067.65 0100 0 67.6 6.98 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140453MSD 01/11/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/11/2011 1881961101421-041EMSD

3923337

2,4-Dinitrotoluene 1096.25 23.8100 0 96.2 52.3 120 105.0 8.73

2-Chlorophenol 1091.21 24.7100 0 91.2 49.1 120 97.17 6.33

4-Chloro-3-methylphenol 1098.51 24.9100 0 98.5 49.2 129 109.5 10.5

4-Nitrophenol 2549.18 27.8100 0 49.2 24.1 120 59.38 18.8

Acenaphthene 1094.32 22.2100 0 94.3 54.4 120 103.8 9.62

N-Nitrosodi-n-propylamine 1097.02 26.2100 0 97 45.3 128 105.1 8.03

Pentachlorophenol 2597.07 25.1100 0 97.1 39.6 147 107.6 10.3

Phenol 1059.97 30.3100 0 60 24.8 120 63.72 6.06

Pyrene 1094.07 22.7100 0 94.1 54 125 108.5 14.3

Surr: 2,4,6-Tribromophenol 0109.0 0100 0 109 42.2 151 119.4 0

Surr: 2-Fluorobiphenyl 047.94 050 0 95.9 48.2 124 53.73 0

Surr: 2-Fluorophenol 076.70 0100 0 76.7 21.6 120 81.36 0

Surr: 4-Terphenyl-d14 048.07 050 0 96.1 40.8 141 55.57 0

Surr: Nitrobenzene-d5 048.02 050 0 96 40.2 126 50.87 0

Surr: Phenol-d5 062.80 0100 0 62.8 6.98 120 67.65 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

58 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140478

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140478MBLK 01/12/2011Mercury, Dissolved SW7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 01/12/2011 188236MB-140478

3923802

Mercury 0.00020BRL 00 0 0 0 0 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140478LCS 01/12/2011Mercury, Dissolved SW7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 01/12/2011 188236LCS-140478

3923803

Mercury 0.000200.005195 00.005 0 104 85 115 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140478MS 01/12/2011Mercury, Dissolved SW7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 01/12/2011 1882361101252-006BMS

3923805

Mercury 0.000200.005394 00.005 0 108 70 130 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140478MSD 01/12/2011Mercury, Dissolved SW7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 01/12/2011 1882361101252-006BMSD

3923806

Mercury 0.000200.005295 200.005 0 106 70 130 0.005394 1.85

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

59 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140499

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140499MBLK 01/12/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg 01/12/2011 188225MB-140499

3924557

1,1´-Biphenyl 330BRL 00 0 0 0 0 0 0

2,4,5-Trichlorophenol 1700BRL 00 0 0 0 0 0 0

2,4,6-Trichlorophenol 330BRL 00 0 0 0 0 0 0

2,4-Dichlorophenol 330BRL 00 0 0 0 0 0 0

2,4-Dimethylphenol 330BRL 00 0 0 0 0 0 0

2,4-Dinitrophenol 1700BRL 00 0 0 0 0 0 0

2,4-Dinitrotoluene 330BRL 00 0 0 0 0 0 0

2,6-Dinitrotoluene 330BRL 00 0 0 0 0 0 0

2-Chloronaphthalene 330BRL 00 0 0 0 0 0 0

2-Chlorophenol 330BRL 00 0 0 0 0 0 0

2-Methylnaphthalene 330BRL 00 0 0 0 0 0 0

2-Methylphenol 330BRL 00 0 0 0 0 0 0

2-Nitroaniline 1700BRL 00 0 0 0 0 0 0

2-Nitrophenol 330BRL 00 0 0 0 0 0 0

3,3´-Dichlorobenzidine 670BRL 00 0 0 0 0 0 0

3-Nitroaniline 1700BRL 00 0 0 0 0 0 0

4,6-Dinitro-2-methylphenol 1700BRL 00 0 0 0 0 0 0

4-Bromophenyl phenyl ether 330BRL 00 0 0 0 0 0 0

4-Chloro-3-methylphenol 330BRL 00 0 0 0 0 0 0

4-Chloroaniline 330BRL 00 0 0 0 0 0 0

4-Chlorophenyl phenyl ether 330BRL 00 0 0 0 0 0 0

4-Methylphenol 330BRL 00 0 0 0 0 0 0

4-Nitroaniline 1700BRL 00 0 0 0 0 0 0

4-Nitrophenol 1700BRL 00 0 0 0 0 0 0

Acenaphthene 330BRL 00 0 0 0 0 0 0

Acenaphthylene 330BRL 00 0 0 0 0 0 0

Acetophenone 330BRL 00 0 0 0 0 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

60 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140499

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140499MBLK 01/12/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg 01/12/2011 188225MB-140499

3924557

Anthracene 330BRL 00 0 0 0 0 0 0

Atrazine 330BRL 00 0 0 0 0 0 0

Benz(a)anthracene 330BRL 00 0 0 0 0 0 0

Benzaldehyde 330BRL 00 0 0 0 0 0 0

Benzo(a)pyrene 330BRL 00 0 0 0 0 0 0

Benzo(b)fluoranthene 330BRL 00 0 0 0 0 0 0

Benzo(g,h,i)perylene 330BRL 00 0 0 0 0 0 0

Benzo(k)fluoranthene 330BRL 00 0 0 0 0 0 0

Bis(2-chloroethoxy)methane 330BRL 00 0 0 0 0 0 0

Bis(2-chloroethyl)ether 330BRL 00 0 0 0 0 0 0

Bis(2-chloroisopropyl)ether 330BRL 00 0 0 0 0 0 0

Bis(2-ethylhexyl)phthalate 330BRL 00 0 0 0 0 0 0

Butyl benzyl phthalate 330BRL 00 0 0 0 0 0 0

Caprolactam 330BRL 00 0 0 0 0 0 0

Carbazole 330BRL 00 0 0 0 0 0 0

Chrysene 330BRL 00 0 0 0 0 0 0

Di-n-butyl phthalate 330BRL 00 0 0 0 0 0 0

Di-n-octyl phthalate 330BRL 00 0 0 0 0 0 0

Dibenz(a,h)anthracene 330BRL 00 0 0 0 0 0 0

Dibenzofuran 330BRL 00 0 0 0 0 0 0

Diethyl phthalate 330BRL 00 0 0 0 0 0 0

Dimethyl phthalate 330BRL 00 0 0 0 0 0 0

Fluoranthene 330BRL 00 0 0 0 0 0 0

Fluorene 330BRL 00 0 0 0 0 0 0

Hexachlorobenzene 330BRL 00 0 0 0 0 0 0

Hexachlorobutadiene 330BRL 00 0 0 0 0 0 0

Hexachlorocyclopentadiene 660BRL 00 0 0 0 0 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

61 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140499

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140499MBLK 01/12/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg 01/12/2011 188225MB-140499

3924557

Hexachloroethane 330BRL 00 0 0 0 0 0 0

Indeno(1,2,3-cd)pyrene 330BRL 00 0 0 0 0 0 0

Isophorone 330BRL 00 0 0 0 0 0 0

N-Nitrosodi-n-propylamine 330BRL 00 0 0 0 0 0 0

N-Nitrosodiphenylamine 330BRL 00 0 0 0 0 0 0

Naphthalene 330BRL 00 0 0 0 0 0 0

Nitrobenzene 330BRL 00 0 0 0 0 0 0

Pentachlorophenol 1700BRL 00 0 0 0 0 0 0

Phenanthrene 330BRL 00 0 0 0 0 0 0

Phenol 330BRL 00 0 0 0 0 0 0

Pyrene 330BRL 00 0 0 0 0 0 0

Surr: 2,4,6-Tribromophenol 02733 03333 0 82 40.4 136 0 0

Surr: 2-Fluorobiphenyl 01270 01667 0 76.2 48.5 120 0 0

Surr: 2-Fluorophenol 02308 03333 0 69.2 36.5 120 0 0

Surr: 4-Terphenyl-d14 01404 01667 0 84.3 51 125 0 0

Surr: Nitrobenzene-d5 01079 01667 0 64.8 37.6 120 0 0

Surr: Phenol-d5 02420 03333 0 72.6 40.1 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140499LCS 01/12/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg 01/12/2011 188225LCS-140499

3924558

2,4-Dinitrotoluene 3302798 03333 0 83.9 61.9 120 0 0

2-Chlorophenol 3302509 03333 0 75.3 57.7 120 0 0

4-Chloro-3-methylphenol 3302615 03333 0 78.4 59.5 120 0 0

4-Nitrophenol 17001880 03333 0 56.4 43.8 120 0 0

Acenaphthene 3302748 03333 0 82.4 63.1 120 0 0

N-Nitrosodi-n-propylamine 3302792 03333 0 83.8 54.9 118 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

62 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140499

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140499LCS 01/12/2011TCL-SEMIVOLATILE ORGANICS SW8270D

Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg 01/12/2011 188225LCS-140499

3924558

Pentachlorophenol 17002431 03333 0 72.9 42.5 132 0 0

Phenol 3302596 03333 0 77.9 50.9 120 0 0

Pyrene 3302856 03333 0 85.7 73 120 0 0

Surr: 2,4,6-Tribromophenol 02971 03333 0 89.1 40.4 136 0 0

Surr: 2-Fluorobiphenyl 01369 01667 0 82.2 48.5 120 0 0

Surr: 2-Fluorophenol 02390 03333 0 71.7 36.5 120 0 0

Surr: 4-Terphenyl-d14 01464 01667 0 87.8 51 125 0 0

Surr: Nitrobenzene-d5 01155 01667 0 69.3 37.6 120 0 0

Surr: Phenol-d5 02572 03333 0 77.2 40.1 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140499MS 01/12/2011TCL-SEMIVOLATILE ORGANICS SW8270D

SB-5 Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg-dry 01/12/2011 1882251101566-005CMS

3924560

2,4-Dinitrotoluene 4403391 04487 0 75.6 37.1 120 0 0

2-Chlorophenol 4403496 04487 0 77.9 41.7 120 0 0

4-Chloro-3-methylphenol 4403454 04487 0 77 47 117 0 0

4-Nitrophenol 2300BRL 04487 0 48.9 37.6 120 0 0

Acenaphthene 4403544 04487 0 79 52.4 120 0 0

N-Nitrosodi-n-propylamine 4403677 04487 0 82 45.5 120 0 0

Pentachlorophenol 23002630 04487 0 58.6 30.7 126 0 0

Phenol 4403539 04487 0 78.9 37.7 120 0 0

Pyrene 4403555 04487 0 79.2 52.5 116 0 0

Surr: 2,4,6-Tribromophenol 03714 04487 0 82.8 40.4 136 0 0

Surr: 2-Fluorobiphenyl 01818 02243 0 81 48.5 120 0 0

Surr: 2-Fluorophenol 03374 04487 0 75.2 36.5 120 0 0

Surr: 4-Terphenyl-d14 01817 02243 0 81 51 125 0 0

Surr: Nitrobenzene-d5 01627 02243 0 72.5 37.6 120 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

63 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140499

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140499MS 01/12/2011TCL-SEMIVOLATILE ORGANICS SW8270D

SB-5 Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg-dry 01/12/2011 1882251101566-005CMS

3924560

Surr: Phenol-d5 03517 04487 0 78.4 40.1 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140499MSD 01/12/2011TCL-SEMIVOLATILE ORGANICS SW8270D

SB-5 Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg-dry 01/12/2011 1882251101566-005CMSD

3924561

2,4-Dinitrotoluene 4403415 18.14491 0 76 37.1 120 3391 0.707

2-Chlorophenol 4403416 21.24491 0 76.1 41.7 120 3496 2.3

4-Chloro-3-methylphenol 4403461 184491 0 77.1 47 117 3454 0.178

4-Nitrophenol 2300BRL 17.64491 0 47.8 37.6 120 2195 0

Acenaphthene 4403390 17.44491 0 75.5 52.4 120 3544 4.43

N-Nitrosodi-n-propylamine 4403615 18.94491 0 80.5 45.5 120 3677 1.7

Pentachlorophenol 23002881 16.94491 0 64.1 30.7 126 2630 9.11

Phenol 4403502 20.14491 0 78 37.7 120 3539 1.06

Pyrene 4403513 17.24491 0 78.2 52.5 116 3555 1.18

Surr: 2,4,6-Tribromophenol 03710 04491 0 82.6 40.4 136 3714 0

Surr: 2-Fluorobiphenyl 01825 02246 0 81.3 48.5 120 1818 0

Surr: 2-Fluorophenol 03341 04491 0 74.4 36.5 120 3374 0

Surr: 4-Terphenyl-d14 01824 02246 0 81.2 51 125 1817 0

Surr: Nitrobenzene-d5 01610 02246 0 71.7 37.6 120 1627 0

Surr: Phenol-d5 03605 04491 0 80.3 40.1 120 3517 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

64 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140509

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140509MBLK 01/13/2011 METALS, TOTAL SW6010C

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 01/12/2011 188336MB-140509

3925949

Arsenic 0.498BRL 00 0 0 0 0 0 0

Barium 0.498BRL 00 0 0 0 0 0 0

Cadmium 0.249BRL 00 0 0 0 0 0 0

Chromium 0.249BRL 00 0 0 0 0 0 0

Lead 0.498BRL 00 0 0 0 0 0 0

Selenium 0.498BRL 00 0 0 0 0 0 0

Silver 0.249BRL 00 0 0 0 0 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140509LCS 01/13/2011 METALS, TOTAL SW6010C

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 01/12/2011 188336LCS-140509

3925948

Arsenic 5.0051.53 050 0 103 80 120 0 0

Barium 5.0050.66 050 0 101 80 120 0 0

Cadmium 2.5050.17 050 0 100 80 120 0 0

Chromium 2.5052.26 050 0.01151 104 80 120 0 0

Lead 5.0049.98 050 0 100 80 120 0 0

Selenium 5.0050.65 050 0 101 80 120 0 0

Silver 2.505.016 05 0 100 80 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140509MS 01/13/2011 METALS, TOTAL SW6010C

SB-4 Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg-dry 01/12/2011 1883361101566-004CMS

3925952

Arsenic 7.2852.71 072.77 0 72.4 75 125 0 S0

Barium 7.28122.7 072.77 76.86 63.1 75 125 0 S0

Cadmium 3.6469.18 072.77 0 95.1 75 125 0 0

Chromium 3.64118.1 072.77 46.32 98.7 75 125 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

65 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140509

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140509MS 01/13/2011 METALS, TOTAL SW6010C

SB-4 Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg-dry 01/12/2011 1883361101566-004CMS

3925952

Lead 7.2870.30 072.77 4.989 89.7 75 125 0 0

Selenium 7.2850.57 072.77 0 69.5 75 125 0 S0

Silver 3.646.554 07.277 0 90.1 75 125 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140509MSD 01/13/2011 METALS, TOTAL SW6010C

SB-4 Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg-dry 01/12/2011 1883361101566-004CMSD

3925953

Arsenic 7.2953.04 2072.89 0 72.8 75 125 52.71 S0.617

Barium 7.29132.9 2072.89 76.86 76.9 75 125 122.7 7.92

Cadmium 3.6469.63 2072.89 0 95.5 75 125 69.18 0.659

Chromium 3.64118.7 2072.89 46.32 99.3 75 125 118.1 0.505

Lead 7.2990.24 2072.89 4.989 117 75 125 70.30 R24.8

Selenium 7.2950.86 2072.89 0 69.8 75 125 50.57 S0.562

Silver 3.647.666 207.289 0 105 75 125 6.554 15.6

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

66 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140528

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140528MBLK 01/15/2011Total Metals by ICP/MS SW6020A

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 188453MB-140528

3928237

Arsenic 5.00BRL 00 0 0 0 0 0 0

Barium 10.0BRL 00 0 0 0 0 0 0

Cadmium 0.700BRL 00 0 0 0 0 0 0

Chromium 5.00BRL 00 0 0 0 0 0 0

Lead 1.00BRL 00 0 0 0 0 0 0

Selenium 5.00BRL 00 0 0 0 0 0 0

Silver 1.00BRL 00 0 0 0 0 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140528LCS 01/15/2011Total Metals by ICP/MS SW6020A

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 188453LCS-140528

3928230

Arsenic 5.00110.5 0100 0 110 85 115 0 0

Barium 10.0112.3 0100 0 112 85 115 0 0

Cadmium 0.700111.7 0100 0 112 85 115 0 0

Chromium 5.00111.4 0100 0 111 85 115 0 0

Lead 1.00110.3 0100 0 110 85 115 0 0

Selenium 5.00108.7 0100 0 109 85 115 0 0

Silver 1.0011.15 010 0 112 85 115 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140528MS 01/15/2011Total Metals by ICP/MS SW6020A

MW-6 Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 1884531101566-012CMS

3928257

Arsenic 5.0094.79 0100 0 94.8 70 130 0 0

Barium 10.0180.5 0100 63.07 117 70 130 0 0

Cadmium 0.700112.7 0100 0.09900 113 70 130 0 0

Chromium 5.00109.2 0100 5.919 103 70 130 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

67 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140528

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140528MS 01/15/2011Total Metals by ICP/MS SW6020A

MW-6 Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 1884531101566-012CMS

3928257

Lead 1.00114.9 0100 1.565 113 70 130 0 0

Selenium 5.0090.12 0100 0 90.1 70 130 0 0

Silver 1.0010.83 010 0 108 70 130 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140528MSD 01/15/2011Total Metals by ICP/MS SW6020A

MW-6 Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 1884531101566-012CMSD

3928262

Arsenic 5.0094.79 20100 0 94.8 70 130 94.79 0

Barium 10.0182.0 20100 63.07 119 70 130 180.5 0.828

Cadmium 0.700112.5 20100 0.09900 112 70 130 112.7 0.178

Chromium 5.00110.0 20100 5.919 104 70 130 109.2 0.73

Lead 1.00115.2 20100 1.565 114 70 130 114.9 0.261

Selenium 5.0089.43 20100 0 89.4 70 130 90.12 0.769

Silver 1.0010.79 2010 0 108 70 130 10.83 0.37

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

68 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140533

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140533MBLK 01/15/2011Dissolved Metals by ICP/MS SW6020A

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 188451MB-140533

3928193

Arsenic 5.00BRL 00 0 0 0 0 0 0

Barium 10.0BRL 00 0 0 0 0 0 0

Cadmium 0.700BRL 00 0 0 0 0 0 0

Chromium 5.00BRL 00 0 0 0 0 0 0

Lead 1.00BRL 00 0 0 0 0 0 0

Selenium 5.00BRL 00 0 0 0 0 0 0

Silver 1.00BRL 00 0 0 0 0 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140533LCS 01/15/2011Dissolved Metals by ICP/MS SW6020A

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 188451LCS-140533

3928191

Arsenic 5.00102.3 0100 0 102 85 115 0 0

Barium 10.0104.3 0100 0 104 85 115 0 0

Cadmium 0.700104.0 0100 0.03300 104 85 115 0 0

Chromium 5.00103.6 0100 0.1240 103 85 115 0 0

Lead 1.00102.9 0100 0 103 85 115 0 0

Selenium 5.00100.9 0100 0 101 85 115 0 0

Silver 1.0010.42 010 0 104 85 115 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140533MS 01/15/2011Dissolved Metals by ICP/MS SW6020A

MW-3 Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 1884511101566-009DMS

3928213

Arsenic 5.00104.9 0100 0 105 70 130 0 0

Barium 10.0159.0 0100 51.22 108 70 130 0 0

Cadmium 0.700107.7 0100 0.09600 108 70 130 0 0

Chromium 5.00102.7 0100 0 103 70 130 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

69 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140533

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140533MS 01/15/2011Dissolved Metals by ICP/MS SW6020A

MW-3 Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 1884511101566-009DMS

3928213

Lead 1.00106.3 0100 0 106 70 130 0 0

Selenium 5.00104.3 0100 0 104 70 130 0 0

Silver 1.0010.62 010 0 106 70 130 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140533MSD 01/15/2011Dissolved Metals by ICP/MS SW6020A

MW-3 Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/13/2011 1884511101566-009DMSD

3928220

Arsenic 5.00103.5 20100 0 104 70 130 104.9 1.34

Barium 10.0155.6 20100 51.22 104 70 130 159.0 2.16

Cadmium 0.700106.0 20100 0.09600 106 70 130 107.7 1.59

Chromium 5.00100.5 20100 0 100 70 130 102.7 2.17

Lead 1.00103.5 20100 0 104 70 130 106.3 2.67

Selenium 5.00103.6 20100 0 104 70 130 104.3 0.673

Silver 1.0010.48 2010 0 105 70 130 10.62 1.33

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

70 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140538

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140538MBLK 01/13/2011Mercury, Total SW7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 01/13/2011 188322MB-140538

3925479

Mercury 0.00020BRL 00 0 0 0 0 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140538LCS 01/13/2011Mercury, Total SW7470A

Units: Prep Date:Sample ID: Client ID: Run No:mg/L 01/13/2011 188322LCS-140538

3925481

Mercury 0.000200.004966 00.005 0 99.3 85 115 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140538MS 01/13/2011Mercury, Total SW7470A

MW-3 Units: Prep Date:Sample ID: Client ID: Run No:mg/L 01/13/2011 1883221101566-009CMS

3925487

Mercury 0.000200.004719 00.005 0 94.4 70 130 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140538MSD 01/13/2011Mercury, Total SW7470A

MW-3 Units: Prep Date:Sample ID: Client ID: Run No:mg/L 01/13/2011 1883221101566-009CMSD

3925490

Mercury 0.000200.004742 200.005 0 94.8 70 130 0.004719 0.496

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

71 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140584

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140584MBLK 01/13/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg 01/13/2011 188337MB-140584

3925955

1,1,1-Trichloroethane 5.0BRL 00 0 0 0 0 0 0

1,1,2,2-Tetrachloroethane 5.0BRL 00 0 0 0 0 0 0

1,1,2-Trichloroethane 5.0BRL 00 0 0 0 0 0 0

1,1-Dichloroethane 5.0BRL 00 0 0 0 0 0 0

1,1-Dichloroethene 5.0BRL 00 0 0 0 0 0 0

1,2,4-Trichlorobenzene 5.0BRL 00 0 0 0 0 0 0

1,2-Dibromo-3-chloropropane 5.0BRL 00 0 0 0 0 0 0

1,2-Dibromoethane 5.0BRL 00 0 0 0 0 0 0

1,2-Dichlorobenzene 5.0BRL 00 0 0 0 0 0 0

1,2-Dichloroethane 5.0BRL 00 0 0 0 0 0 0

1,2-Dichloropropane 5.0BRL 00 0 0 0 0 0 0

1,3-Dichlorobenzene 5.0BRL 00 0 0 0 0 0 0

1,4-Dichlorobenzene 5.0BRL 00 0 0 0 0 0 0

2-Butanone 50BRL 00 0 0 0 0 0 0

2-Hexanone 10BRL 00 0 0 0 0 0 0

4-Methyl-2-pentanone 10BRL 00 0 0 0 0 0 0

Acetone 100BRL 00 0 0 0 0 0 0

Benzene 5.0BRL 00 0 0 0 0 0 0

Bromodichloromethane 5.0BRL 00 0 0 0 0 0 0

Bromoform 5.0BRL 00 0 0 0 0 0 0

Bromomethane 5.0BRL 00 0 0 0 0 0 0

Carbon disulfide 10BRL 00 0 0 0 0 0 0

Carbon tetrachloride 5.0BRL 00 0 0 0 0 0 0

Chlorobenzene 5.0BRL 00 0 0 0 0 0 0

Chloroethane 10BRL 00 0 0 0 0 0 0

Chloroform 5.0BRL 00 0 0 0 0 0 0

Chloromethane 10BRL 00 0 0 0 0 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

72 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140584

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140584MBLK 01/13/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg 01/13/2011 188337MB-140584

3925955

cis-1,2-Dichloroethene 5.0BRL 00 0 0 0 0 0 0

cis-1,3-Dichloropropene 5.0BRL 00 0 0 0 0 0 0

Cyclohexane 5.0BRL 00 0 0 0 0 0 0

Dibromochloromethane 5.0BRL 00 0 0 0 0 0 0

Dichlorodifluoromethane 10BRL 00 0 0 0 0 0 0

Ethylbenzene 5.0BRL 00 0 0 0 0 0 0

Freon-113 10BRL 00 0 0 0 0 0 0

Isopropylbenzene 5.0BRL 00 0 0 0 0 0 0

Methyl acetate 5.0BRL 00 0 0 0 0 0 0

Methyl tert-butyl ether 5.0BRL 00 0 0 0 0 0 0

Methylcyclohexane 5.0BRL 00 0 0 0 0 0 0

Methylene chloride 20BRL 00 0 0 0 0 0 0

n-Heptane 10BRL 00 0 0 0 0 0 N0

Naphthalene 5.0BRL 00 0 0 0 0 0 0

Styrene 5.0BRL 00 0 0 0 0 0 0

Tetrachloroethene 5.0BRL 00 0 0 0 0 0 0

Toluene 5.0BRL 00 0 0 0 0 0 0

trans-1,2-Dichloroethene 5.0BRL 00 0 0 0 0 0 0

trans-1,3-Dichloropropene 5.0BRL 00 0 0 0 0 0 0

Trichloroethene 5.0BRL 00 0 0 0 0 0 0

Trichlorofluoromethane 5.0BRL 00 0 0 0 0 0 0

Vinyl chloride 10BRL 00 0 0 0 0 0 0

Xylenes, Total 5.0BRL 00 0 0 0 0 0 0

Surr: 4-Bromofluorobenzene 045.99 050 0 92 56 137 0 0

Surr: Dibromofluoromethane 046.81 050 0 93.6 73.7 137 0 0

Surr: Toluene-d8 048.70 050 0 97.4 69.2 126 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

73 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140584

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140584LCS 01/13/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg 01/13/2011 188337LCS-140584

3925957

1,1-Dichloroethene 5.055.62 050 0 111 60 158 0 0

Benzene 5.050.91 050 0 102 68.8 141 0 0

Chlorobenzene 5.052.97 050 0 106 76.2 136 0 0

Toluene 5.052.69 050 0 105 69.8 141 0 0

Trichloroethene 5.052.64 050 0 105 71.2 147 0 0

Surr: 4-Bromofluorobenzene 055.52 050 0 111 56 137 0 0

Surr: Dibromofluoromethane 048.41 050 0 96.8 73.7 137 0 0

Surr: Toluene-d8 049.57 050 0 99.1 69.2 126 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140584MS 01/13/2011Volatile Organic Compounds by GC/MS SW8260B

SB-1 Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg-dry 01/13/2011 1883371101566-001AMS

3925962

1,1-Dichloroethene 7.383.17 073.49 0 113 55.2 163 0 0

Benzene 7.376.51 073.49 0 104 67.4 144 0 0

Chlorobenzene 7.375.76 073.49 0 103 73.6 140 0 0

Toluene 7.376.66 073.49 1.943 102 64.6 145 0 0

Trichloroethene 7.378.66 073.49 0 107 70.1 149 0 0

Surr: 4-Bromofluorobenzene 078.50 073.49 0 107 56 137 0 0

Surr: Dibromofluoromethane 070.66 073.49 0 96.2 73.7 137 0 0

Surr: Toluene-d8 073.06 073.49 0 99.4 69.2 126 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140584MSD 01/13/2011Volatile Organic Compounds by GC/MS SW8260B

SB-1 Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg-dry 01/13/2011 1883371101566-001AMSD

3925965

1,1-Dichloroethene 7.378.45 34.973.49 0 107 55.2 163 83.17 5.84

Benzene 7.367.46 27.273.49 0 91.8 67.4 144 76.51 12.6

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

74 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140584

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140584MSD 01/13/2011Volatile Organic Compounds by GC/MS SW8260B

SB-1 Units: Prep Date:Sample ID: Client ID: Run No:ug/Kg-dry 01/13/2011 1883371101566-001AMSD

3925965

Chlorobenzene 7.367.21 33.473.49 0 91.5 73.6 140 75.76 12

Toluene 7.368.17 26.873.49 1.943 90.1 64.6 145 76.66 11.7

Trichloroethene 7.370.08 3473.49 0 95.4 70.1 149 78.66 11.5

Surr: 4-Bromofluorobenzene 078.38 073.49 0 107 56 137 78.50 0

Surr: Dibromofluoromethane 071.27 073.49 0 97 73.7 137 70.66 0

Surr: Toluene-d8 075.32 073.49 0 102 69.2 126 73.06 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

75 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140598

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140598MBLK 01/14/2011TOTAL MERCURY SW7471B

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 01/14/2011 188378MB-140598

3926798

Mercury 0.100BRL 00 0 0 0 0 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140598LCS 01/14/2011TOTAL MERCURY SW7471B

Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg 01/14/2011 188378LCS-140598

3926799

Mercury 0.1000.3857 00.4 0 96.4 80 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140598MS 01/14/2011TOTAL MERCURY SW7471B

SB-6 Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg-dry 01/14/2011 1883781101566-006CMS

3926801

Mercury 0.1240.5429 00.4966 0 109 70 130 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140598MSD 01/14/2011TOTAL MERCURY SW7471B

SB-6 Units: Prep Date:Sample ID: Client ID: Run No:mg/Kg-dry 01/14/2011 1883781101566-006CMSD

3926802

Mercury 0.1250.5337 300.4985 0 107 70 130 0.5429 1.72

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

76 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140641

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140641MBLK 01/14/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/14/2011 188388MB-140641

3929446

1,1,1-Trichloroethane 5.0BRL 00 0 0 0 0 0 0

1,1,2,2-Tetrachloroethane 5.0BRL 00 0 0 0 0 0 0

1,1,2-Trichloroethane 5.0BRL 00 0 0 0 0 0 0

1,1-Dichloroethane 5.0BRL 00 0 0 0 0 0 0

1,1-Dichloroethene 5.0BRL 00 0 0 0 0 0 0

1,2,4-Trichlorobenzene 5.0BRL 00 0 0 0 0 0 0

1,2-Dibromo-3-chloropropane 5.0BRL 00 0 0 0 0 0 0

1,2-Dibromoethane 5.0BRL 00 0 0 0 0 0 0

1,2-Dichlorobenzene 5.0BRL 00 0 0 0 0 0 0

1,2-Dichloroethane 5.0BRL 00 0 0 0 0 0 0

1,2-Dichloropropane 5.0BRL 00 0 0 0 0 0 0

1,3-Dichlorobenzene 5.0BRL 00 0 0 0 0 0 0

1,4-Dichlorobenzene 5.0BRL 00 0 0 0 0 0 0

2-Butanone 50BRL 00 0 0 0 0 0 0

2-Hexanone 10BRL 00 0 0 0 0 0 0

4-Methyl-2-pentanone 10BRL 00 0 0 0 0 0 0

Acetone 50BRL 00 0 0 0 0 0 0

Benzene 5.0BRL 00 0 0 0 0 0 0

Bromodichloromethane 5.0BRL 00 0 0 0 0 0 0

Bromoform 5.0BRL 00 0 0 0 0 0 0

Bromomethane 5.0BRL 00 0 0 0 0 0 0

Carbon disulfide 5.0BRL 00 0 0 0 0 0 0

Carbon tetrachloride 5.0BRL 00 0 0 0 0 0 0

Chlorobenzene 5.0BRL 00 0 0 0 0 0 0

Chloroethane 10BRL 00 0 0 0 0 0 0

Chloroform 5.0BRL 00 0 0 0 0 0 0

Chloromethane 10BRL 00 0 0 0 0 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

77 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140641

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140641MBLK 01/14/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/14/2011 188388MB-140641

3929446

cis-1,2-Dichloroethene 5.0BRL 00 0 0 0 0 0 0

cis-1,3-Dichloropropene 5.0BRL 00 0 0 0 0 0 0

Cyclohexane 5.0BRL 00 0 0 0 0 0 0

Dibromochloromethane 5.0BRL 00 0 0 0 0 0 0

Dichlorodifluoromethane 10BRL 00 0 0 0 0 0 0

Ethylbenzene 5.0BRL 00 0 0 0 0 0 0

Freon-113 10BRL 00 0 0 0 0 0 0

Isopropylbenzene 5.0BRL 00 0 0 0 0 0 0

Methyl acetate 5.0BRL 00 0 0 0 0 0 0

Methyl tert-butyl ether 5.0BRL 00 0 0 0 0 0 0

Methylcyclohexane 5.0BRL 00 0 0 0 0 0 0

Methylene chloride 5.0BRL 00 0 0 0 0 0 0

Naphthalene 5.0BRL 00 0 0 0 0 0 0

Styrene 5.0BRL 00 0 0 0 0 0 0

Tetrachloroethene 5.0BRL 00 0 0 0 0 0 0

Toluene 5.0BRL 00 0 0 0 0 0 0

trans-1,2-Dichloroethene 5.0BRL 00 0 0 0 0 0 0

trans-1,3-Dichloropropene 5.0BRL 00 0 0 0 0 0 0

Trichloroethene 5.0BRL 00 0 0 0 0 0 0

Trichlorofluoromethane 5.0BRL 00 0 0 0 0 0 0

Vinyl chloride 2.0BRL 00 0 0 0 0 0 0

Xylenes, Total 5.0BRL 00 0 0 0 0 0 0

Surr: 4-Bromofluorobenzene 039.14 050 0 78.3 64.7 130 0 0

Surr: Dibromofluoromethane 048.40 050 0 96.8 80.7 129 0 0

Surr: Toluene-d8 042.87 050 0 85.7 71.1 120 0 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

78 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140641

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140641LCS 01/14/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/14/2011 188388LCS-140641

3929447

1,1-Dichloroethene 5.072.89 050 0 146 51 154 0 0

Benzene 5.055.51 050 0 111 73.6 129 0 0

Chlorobenzene 5.054.19 050 0 108 77.6 125 0 0

Toluene 5.054.91 050 0 110 75.7 128 0 0

Trichloroethene 5.056.82 050 0 114 73.9 132 0 0

Surr: 4-Bromofluorobenzene 040.45 050 0 80.9 64.7 130 0 0

Surr: Dibromofluoromethane 048.32 050 0 96.6 80.7 129 0 0

Surr: Toluene-d8 042.38 050 0 84.8 71.1 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140641MS 01/14/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/14/2011 1883881101692-001AMS

3929450

1,1-Dichloroethene 50000637600 0500000 0 128 46.2 183 0 0

Benzene 50000576100 0500000 9400 113 62.2 143 0 0

Chlorobenzene 50000541800 0500000 0 108 72.2 137 0 0

Toluene 50000589200 0500000 41100 110 57.8 149 0 0

Trichloroethene 50000557800 0500000 0 112 70.5 149 0 0

Surr: 4-Bromofluorobenzene 0410000 0500000 0 82 64.7 130 0 0

Surr: Dibromofluoromethane 0492700 0500000 0 98.5 80.7 129 0 0

Surr: Toluene-d8 0413400 0500000 0 82.7 71.1 120 0 0

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140641MSD 01/14/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/14/2011 1883881101692-001AMSD

3929451

1,1-Dichloroethene 50000621400 20500000 0 124 46.2 183 637600 2.57

Benzene 50000559800 20500000 9400 110 62.2 143 576100 2.87

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

79 of 80

17-Jan-11Date:Analytical Environmental Services, Inc

Client:

BatchID:Workorder:

Project Name:ANALYTICAL QC SUMMARY REPORT

VWT, Inc

1101566

HRP Associates, inc.

140641

RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit

SampleType: BatchID: Analysis Date: Seq No:TestCode: 140641MSD 01/14/2011Volatile Organic Compounds by GC/MS SW8260B

Units: Prep Date:Sample ID: Client ID: Run No:ug/L 01/14/2011 1883881101692-001AMSD

3929451

Chlorobenzene 50000529000 20500000 0 106 72.2 137 541800 2.39

Toluene 50000568600 20500000 41100 106 57.8 149 589200 3.56

Trichloroethene 50000557200 20500000 0 111 70.5 149 557800 0.108

Surr: 4-Bromofluorobenzene 0384200 0500000 0 76.8 64.7 130 410000 0

Surr: Dibromofluoromethane 0492000 0500000 0 98.4 80.7 129 492700 0

Surr: Toluene-d8 0420000 0500000 0 84 71.1 120 413400 0

Qualifiers:

J Estimated value detected below Reporting Limit

BRL Below reporting limit H Holding times for preparation or analysis exceeded

N Analyte not NELAC certified

B Analyte detected in the associated method blank

E Estimated (value above quantitation range)

S Spike Recovery outside limits due to matrix

< Less than Result value> Greater than Result value

R RPD outside limits due to matrix

Rpt Lim Reporting Limit

80 of 80

HRP Associates, Inc.

ATTACHMENT C

SCDHEC MONITORING WELL APPROVAL

Temporary Monitoring Well Approval Approval is hereby granted to: Ty Hawkins, HRP Associates on behalf of: VWT, Inc. Facility: VWT, Inc. 483 Belleview Road Site Identification: MONTRAC Site ID –46-04669 County: York County This approval is for the installation of 6 temporary groundwater-monitoring wells. The temporary wells are to be installed in the locations as illustrated on the submitted map and per the proposed construction details provided by your correspondence dated December 29, 2010. The temporary wells are to be installed following all of the applicable requirements of R.61-71. Please note that R.61-71 requires the following:

1. All wells shall be drilled, constructed, and abandoned by a South Carolina certified well driller per R.61-71.D.1. 2. A Water Well Record Form or other form provided or approved by the Department shall be completed and submitted to

the Department within 30 days after well completion or abandonment unless the Department has approved another schedule. The form should contain the “as-built” construction details and all other information required by R.61-71.H.1.f

3. All analytical data and water levels obtained from each monitoring well shall be submitted to the Department within 30

days of receipt of laboratory results unless another schedule has been approved by the Department as required by R.61-71.H.1.d.

4. All temporary monitoring wells shall be abandoned within 5 days of borehole completion using appropriate methods as

required by R.61-71.H.4.c.

5. If any of the information provided to the Department changes, Jonathan McInnis (803 896-4061, [email protected]) shall be notified a minimum of twenty-four hours prior to well construction as required by R.61-71.H.1.a.

This approval is pursuant to the provisions of Section 44-55-40 of the 1976 South Carolina Code of Laws and R.61-71 of the South Carolina Well Standards and Regulations, dated April 26, 2002.

Date of Issuance: Approval #: 4070 Jonathan G. McInnis, Program Manager Federal & State Site Assessment Site Assessment Remediation & Revitalization Division Bureau of Land & Waste Management

December 31, 2010 Vernon Terry VWT, Inc. 483 Belleview Road Rock Hill, SC 29730 Re: Temporary Monitoring Well Approval Request received December 29, 2010 York County Site ID: 46-04669 Dear Mr. Terry: The South Carolina Department of Health and Environmental Control (SCDHEC) has reviewed and approved the referenced temporary monitoring well approval request submitted December 29, 2010. The original temporary monitoring well approval has been sent to Ty Hawkins of HRP Associates and a copy is enclosed for your records. The analytical results from the groundwater samples should be submitted to my attention on or before March 18, 2011. Please note the following:

Well construction and sampling derived waste including but not limited to drill cuttings, drilling fluids, and

development/purge water should be managed properly and in compliance with applicable requirements. If containerized, each vessel should be clearly labeled with regards to contents, source, and date of activity.

Monitoring wells are to yield groundwater samples representative of the zone monitored per R.61-71 H.1.c

of the South Carolina Well Standards and Regulations (e.g. low flow sampling techniques are recommended for samples to be analyzed for metals to reduce induced turbidity).

If this investigation is conducted as part of a potential real estate transaction, the potential purchaser may

want to contact SCDHEC’s Brownfields Program before this work is performed. The Brownfields Program offers a mechanism to avoid liability for contamination that may be found during this investigation. The investigation proposed may satisfy part or all of the required assessment if pre-approved by the Brownfields Program. The Brownfields Program may be reached at 1-866-576-3432.

If you have any questions, please contact me at (803) 896-4061. Sincerely, Jonathan G. McInnis, Program Manager Federal & State Site Assessment Section enc: Monitor well approval cc: SCDHEC EQC Region 3 Ty Hawkins, HRP Associates, 1327-D Miller Rd, Greenville, SC 29607