results of samples collected by adpc&e for epa in ... · region 6 environmental protection...

UNITED STATE^ ENVIRONMENTAL PROTECTION AGENCYHATE 13 March 1981 \ ^ * ^

:UBJECT Sample Management Repor

FROM Charles Gazda (6ASASC)

TO Gerald Fontenot (6AEGH)

Attached is the lab results on samples collected by Arkansas Dept.of Pollution Control & Ecology for EPA in compliance with themonthly court ordered sampling of the Vertac facility at Jacksonville,AR. The results represent samples collected on 1-29-81.

Organics sample numbers: F-433 thru F-0441 ( 9 )

Case N o . 3 9 2 .l

r<^^—oo

YT7.1

; PA Form 13204 W»-. 3-76)

RCPORTprepared For ^ ^ Environmental Protection Agency

First International Building1201 Elm StreetDallas, TX 75270Attention: Charles Gazda

Job No

20797/jlgMarch 9, 1981Date Received

January 30. 198168-01-6035Description of Samples

WESTCOASTTECHNICALSERVICEINC.17605 FabncaWayCerntos, California 90701213/921-9831714/523-9200

Enclosed are the results for sample numbers: F0433-F0441,Case #392. Chain of Custody was received.

00

We would appreciate a telephone call if you have any questions regarding this report Page 1 of . -pages

I certify that this report truly represents the findings of workperformed by me, or under my direct supervision

Reviewed & Approved

Richa rd AmanoAna ly t i ca l Chemis t

D. J. Northington, Ph. D.Technical Director OVIOIS^S

This report pertains only to the samples investigated and does not necessarily apply 1o other apparently identical or similar materials This report is submitted for theexclusive use of the client to whom it is addressed Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes withoutwritten authorization is prohibited

Reg ion 6

E N V I R O N M E N T A L PROTECTION AGENCY1201 Elm S t , Da l l a s , IX 7 5 2 7 0

CHAIN OF CUSTODY RECORD

lagettient Office

ORGANICS TRAFnC REPORTSample Number

F 0433

Q Case Number.3^

©

Sample Site Name/Code:l - 'C . W.J^(

2) Sample Type: (Check One)

RunOff

WeH

Fteoeiving Water

Leachate

Effluent*'

t^— Oflier (speafy) _ '•îli • / /<..

@ StqpTo:

(A/?J^ CO^JS/ Tecî ê^

^foQS !p^b^^f\ W^^S^^ D /C€^''^-s'i C^/J^

' 9P7^/

Attn:

/-//U^T Bll^^^S

@ Regional Office:Sampling Personnel:

(y Mark Volume Level on Sample Bottle

(Name)Extractable

(Phone)

Sampling Date:Extractable

(Begin) (End)Extractable

(y Shipping Information Extractable

\.^ . eVOA Unpreserved

' Name of Shipper:

•;' /

VOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number:

(T) Description of Sample Location:

(s) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

REGIONAL OFFICE FILE COW

ORGANICS TRAFFIC REPORT©Case Number:

3^

Sample Site Name/Code:i /ayf^C ^ Jh(

T^.^v.//< ^

Q Sample Type: (Check One)

—— RunQff

_^WeH

Receiving Wcrtsr

Leacfaate

Effluent

CXher (specify)

(j) Shy To:

fVfJ^ C^^f 7^'^ ^^

^76>^5 /^^/^ )/^^2? /

Ce>/''-7^ ^ ( ^ 1 ' ^ -

Attn:

/.. / '\ c< -•, ^/ (•'•J

^W I

©Regional Office:

Sampling Persca-mel:

^, '^^C^ftO^

Q[) Mark Volume Level on Sample Botfle

7. • f————*•«————————————

(Name); 3 ^ t - / ^ l

(Phone)

Sampling Date:

•'-^.•7' i^/______^fiW ('


(6^) Shipping Information

--T- "r, .^/'^ ^•^J^'.P

Extractable

VOAUnpreserved

Name of Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

k.. -i-^^^0Airbill Number

CT^ Description of Sample Location:

\\.^ , ! •^ i

(J) Spedal Hanaling Instructions:(eg., safety precautions, hazardous nature)

? ' " , "> / , ' - • ' ^ ;"•" -'/\ '"' '

REGIONAL OFTICE FILE COPY

ipie management <

ORGANICS TRAFnC REPORT©Case Number?^

Sample Site Name/Code:(Ay^c . T-i^"•T^.-/Q^^//> 4^

©2) Sample Type: (Check One)

—— RunOff

^WeU

Receiving Water

Leachate

Effluent

Oner (specify) —

® Shy To:

k/^ Co^sr ie^ 6i'/]7^o5 A^/'(^ ^^yJ^f ^ ,. /C(^^^) C^f^

' 9^70/Attn:

/,/..; J»/ O^^-TCJ

©Regional Office:

Sampling Personnel:

-P.. ^4-,^^!)^,

(^) Mark Volume Level on Sample Bottle

/ ( N a m e ) "

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(Phone)

Sampling Date:

;-^>-^7

Ebctractable

(Begin) (End)Exiractable

(^) Shipping Information Extractable

— -T' ^ 'J ".•L^ vJ^ ^•7" • ' ' ^

VOA Unpreserved

,.•'' Name of Shipper:

^•f- 8 - 1


Date Shipped:

Airbill Number:

(7) Description of Sample Location:

(J) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

•- •" .••; / . /^^• '^ ' . .^ ' /i /',•';

\ •" 'Yt /),^

REGIONAL OFnCE FILE COPY

ORGANICS TRAFFIC REPORT(J) Case Number:

3^/2

Sample Site Name/Code:>/P / . ( J T>, ( .

"T^<^.y,/^.

© Sample Type: (Check One)

—— RunOfi

^'WonWeH

Receiving Water

Leachate

Effluent

Other (spedfy)

(j) ShipTo:

l4/^^ Co^f^ ^^ s^/l

l7bos ^^/^ ^y^>k D , •/

c?^^ Gl^^c>l

Attn:

/.,i^- S^^es

Q Regional Office:

Sampling Personnel:

(y Mark Volume Level on Sample Botfle

/ ( N a m e )

.f^/ 3~7i-^ojExtractable

(Phone)

Sampling Date:

:-^/-^!

Extractable


( ) Shipping Information

J^., J'y.')'//1

Extractable

. ., ^^.'i'r/ccL.' Name of Shipper:

/-.l^- •y/

VOA Unpreserved


Date Shipped:

Airbill Number:

Q Description of Sample Location:

' . / f t ' /"• ./ ( '

(J) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

/ <'

REGIONAL OFFICE FILE COPY

HWI Sample MaKpgement Office

ORGANICS TRAFFIC REPORTQJ Case Number:

5^

Sample Site Name/Code:i/' M.J -T^C

3) Sample Type: (Check One)

RunQff

^w^n

Receiving Water

Leachate

Effluent

Other (specify)

@ Ship To:

iv^ 60^^ 7^ ^/^l^^os /^^<t ^^y^- /c ^ /

c€//'/^^//^0/

Attn:

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(^) Regional Qt&ce:

Sampling Personnel:

(j) Mark Volume Level on Sample Bottle

/ (Name)

J^/ JT/-/-;-P/(Phone)

Sampling Date:

Extractable

Extractable


(^) Shipping Information

X J3,J^^

Extractable

VOA Unpreserved

Name of Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number:

DateSampled

< -i .- - //'^--^/

(T) Description of Sample Locatiorc

(H) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

!• ' '' :'i,- ^i f •_- ,.. / , , ... n;;-. •/••'. ;:' I ' . - • • • • " /•/ - -

REGIONAL OFnCE FILE COPY

ipie ivjiâgement Office

ORGANICS TRAFnC REPORT|<: Sample Number

t F 0438

(^) Case Number:ô2

Sample Site Name/Code:t /?/r^c ^ .T^ L

Tf,C^JQJl^//<

(J) Sample Type: (Check One)

___ RunOff

J^WeU

Reoeiving Water

Leacfaate

Effluent

Other (specify)

(j) Shy To:

Wî C^t Tft^ SQ^î^^S ^^^<-fr ^V

S.^c P f

Attn:

L,^^t, (S<i^rs ,

@ Regional Office:Sampling Personnel:

"~T 1'J.JT^


/ ( N a m e )•••), 3 7 / - /7^>/ Extractable

(Phone)

Sampling Date:

-^-^/


(^) Shipping Information

~T<,,..

Extractable

• - / .(A/if^r

VOA Unpreserved

âme of Shipper:

C/ -


Date Shipped:

Airbill Number:


-?-7

Cg) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

1 :-,^ !€/

REGIONAL CmC'E FILE COPY


3^2.

Sample Site Name/Code:l/^ t^c J J^f.

»• i

© Sample Type: (Check One)

___ RunQff

-J^Well

Receiving Water

Leachate

Effluent

Ofher (specify)

(D Ship To:

West Cc^sf 7-e^ J<"><

i^^QS ff^î<-^^^

^ /<• 2)r...;/o^ ^01

Attn:

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Q Regional Office:Sampling Personnel:

~J^J'T'\e


~ 7 ( N a m e )Extractable

(Phone)

Sampling Date:

-.^^

Extractable


(y Shipping Information

•J^/ J^JT/^

Extractable

VOA Unpreserved

tâme of Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number:

DateSampled

•' • " :? i'

("T) Description of Sample Location:

i ;

(s) Special Hanaling Instructions:(eg., safety precautions, hazardous nature)

'(' , .-./.-^î", ' :)

REGIONAL CrTICE FILE COPY


3^:2.

Sample Site Name/Code:|/<? ^YZ<( ^ J^c

.37^/<".?J^.7/^ y%^

(D Sample Type: (Check One)

Run Off

Well

Receiving Water

Leachate

Effluent

Other (spedfy)

© Ship To:WeJi fo^J7 7^<^ Se^^.

/^05 ^^/^ ^/J^/^ t>Cpk^'^s^ ^/;^^^^/

Atin:

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Q Regional Office:

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--r- ---T—" /

J. , UJstice

(y Mark Volume Level on Sample Bottle

/ (Name)

^/ 3^/-/ '?0/(Phone)

Sampling Date:

•-l^l-S'l S^n.e(Begin) (End)

Extractable

Extractetble

Extractable


"•-"r" ~V -/'^a., J^'sT'i

Extractable

<^f ( . , ^)^S " i g• Name of Shipper:

/- .2^7- ^/

VOA Unpreserved


Date Shipped:

-• - ' / / B r~ ^/i "< ^~i<. •-''-f-^xy-/^ C/Airbill Number:


• / ! /.., ; /V \! Q i I

-H n^r /

( ) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

• - - ^ ^ - •w J-^/e

REGIONAL OFUCE FILE COPY


-?^

Sample Site Name/Code:

l/^ffrf . J"n c^ / — - ~ -

©

) Sample Type: (Check One)

_ RunOff

f^ UMlWeU

Receiving Water

Leachate

Effluent

-* Ofher (specify)

@ Ship To:

West- C^^reih

/>^c?s ^^'^ y^'^z;? ^Ce..;^^/^^^

Attn:

/-<'7^ B^^hf^

(4) Regional Office:

Sampling Personnel:

Z7L D^JT^g

(j) Mark Volume Level on Sample Bottle

/ ( N a r n e )

5 - Q / J7/-/ '70/ Extractable

(Phone)

Sampling Date:Ebdractable



J^-/ ^•A^^

Extractable

VOA Unpreserved

Name of Shipper:

/- 2 - ^ /


Date Shipped:

,-;-,•;< (, c, .--.^--9^(9Airbill Number:

(?) Description of Sample Location:

/ ,7 < /

(y Special Handling Instructions:(e.g., safety precautions, hazardous nature)

REGIONAL OFFICE FILE 'COPY

CS3 WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

DATE

STD

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base,

1B

5B

8B

9B

12B

18B

20B

25 B

26B

27B28B

35B

36 B

37B

39B

40B

LE ID F0433

ID ?0797A1EXTRACTED 1-31-81

INJECTED 2-16-81ID DFTPP1258 PHEN308

. FACTOR 1000

Compounds u;

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4 , 6-dinitro-o-cresol

pentachlorophenol

phenol

/Neutra l Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3 '-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl e ther

§/1

ND

ND

ND

ND

N D

ND

ND

ND

ND

N D

ND

ND

NDN D

ND .,NDND

N D

ND

ND

ND

ND

ND

ND

N D

ND

ND

SAMP]

LAB I

DATE

DATE

STD I

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56B

61B

62 B

63B

66 B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

SOB

81B

82B

83B

84B

129B

p-dio:

,E ID F0433 tS^L^

•D POZ^BIEXTRACTED 1-30-81

INJECTED 2-25-81D DFTPP1266 BNSTD363

FACTOR 1000

Neutral Compounds uc

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene—————————————————————^hexachlorocyclopentadiene N-^

isophorone <—

naphthalene <^

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a ) anthracene

benzo(a )pyrene

3,4-benzofluoranthene

benzo( k ) fluoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

d i b e n z o ( a , h ) a n t h r a c e n e

indeno(1,2 ,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-

xin

/I

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND*

ND*

ND*

ND

ND

ND

NONDNDNDN DNDN DNnN DNnND

Nn

CS23 WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMPLE ID F0433

LAB ID 207q7V1

DATE INJECTED 2 8 "1STD ID DFTPP1250 VOA113

CONC. FACTOR

Volatiles

2V acrolein

3V acrylonitrile

4V benzene

6V carbon tetrachloride

7V chlorobenzene

10V 1,2-dichloroethane

11V 1,1,1-trichloroethane



15V 1,1,2,2-tetrachloroethane

l6V chloroethane

)tmXX%X$(k<X6(X<X((«i<i)eX)t^X)©t)t-(©tXXXX)

19V 2-chloroethylvinyl ether

23V chloroform

29V 1,1-dichloroethylene

30V 1,2-trans-dichloroethylene

32V 1,2-dichloropropane

33V 1,3-dichloropropylene

38V ethylbenzene

44V methylene chloride

45V methyl chloride

46V methyl bromide

47V bromoform

48V dichlorobromomethane

49V trichlorofluoromethane

50V dichlorodlfluoromethane

51V chlorodibromomethane

85V tetrachloroethylene

86V toluene

87V trichloroethylene

fc'^V vinyl chloride

ug/1

NO

ND

NO

ND

ND

N D*

ND

ND

ND

ND

C X X X X X

ND*

ND

NDND

NnNP35

NnND

ND

ND

ND

ND

ND

ND

*

ND

N D

SAMPLE ID F0433

LAB ID 20797 trace* 2195

DATE EXTRACTED i - ^n -R l

DATE INJECTED - 2/3/81

STD ID TRACE #2194

CONC. FACTOR 100

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4 , 4 ' - D D E

94P 4 , 4 ' - D D D

95P alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P •gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected

** = Not confirmed by GCMS

ug/1

NOND

ND^0^ N D

m ND

^- N D0 ND

^ ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

C^3 WEST COAST TECHNICAL SERVICE INCORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 26Sample Number

F0433

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

A. SURROGATE

Fract ion

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

S P I K E RESULTS

C o n e . ( u g / 1 )

54

52

56

61

ND

76

105

128

(SurrogaSpike

Added ( u g / 1 )

50

50

50

142

103

98

100

102

tes only)yla

Recovery

108

104

112

^c<im

105"-^rB . TENTATIVELY IDENTIFIED COMPOUNDS

1.2,

3.

4.

5.

6.

7.

8.

9.

10.

11.

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

U N K N O W N

M E T H Y L C Y C L O P E N T A N E

2 . 2 . 2 - T R I C H L O R O E T H A N O L

3 ,3 ,3 -TRICHLORO-I -

P R O P E N E

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

D I E T H Y L P H T H A L A T E

U N K N O W N

FRACTION

VOA #39

VOA #182VOA #300

B/N #76

ACID #98

A C I D #106

A C I D #124

A C I D #14£

A C I D #154

A C I D #15c

A C I D #16^

A C I D #17£

A C I D #192

A C I D #20C

% M a x i m u m Score Attained

Mass Match ing Rout ine: FITspecify)

NO GOOD FIT

901

970

899

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

929

NO GOOD FIT

^SAMP

LAB •

DATE

DATE

STD 1

CONC

Acid

21A

22A

2^A

31A

34A

57A

58A

59A

60A

6M

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25 B

26B

27B

28B

35B

36B

37B

39B

Z.OB

^ W€ST COAST TECHNICAL!

LE ID F0434

I D 9n7Q7fl9

E X T R A C T E D i-31-Si9-1f i -QI

I N J E C T E D " 10 ;-i

:D DFTPPT7SR PHFT\J.?nS

FACTOR 1000

Compounds ui


p-chloro-m-cresol

2-chlorophenol

2,^-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,^-dinitrophenol

L,,6-dinitro-o-cresol

pentachlorophenol

phenol

''Neutral Compounds

acenaphthene

benzidine


hexachlorobenzene

hexachloroethane


2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1 ,^-dichlorobenzene

3,3 '-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene


(as azobenzene)

f luoran thene

^-chlorophenyl phenyl ether

56RVH

^/lND

ND

ND

*•

ND

ND

ND

ND

ND

N D

ND

ND

ND*

ND

ND

N D

ND

ND

ND

ND

ND

ND

N D

ND

N D

ND

re INC.SAMP

LAB

DATE

DATE

STD

CONC

Base,

41B

42B

43B

52B

53B

5^B

55B

56B

61B

62 B

63B

66 B67B68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

SOB

81B

82B

83 B

8^B

129B

p-dic

INDUSTRIAL CATEGORY

LE ID F0434ID 20797B2

EXTRACTED 1-30-81

I N J E C T E D ^S-ai

ID DFTPP12fi6 BNSTD.?fi.3

FACTOR 100C

/Neutral Compounds u(




hexachlorobutadiene 00

hexachlorocyclopentadiener<\

isophorone——————£——————————————————————————————^-~.

naphthalene o

nitrobenzene 0






di-n-butyl phtha la te


diethyl phthalate

dimethyl phthalate


benzo(a)pyrene


benzo (k ) f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi )perylene

fluorene

phenanthrene


indeno(1 ,2 ,3 -cd)pyrene

pyrene


)xln ^^,

^/l

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND*

ND*

ND*

ND

ND

ND

ND

NDNDND

N DNDNON DND

NnND

^

r^.—^ • ,

SAMP

LAB

DATE

STD

CONC

Volal

2V

3V

4V

6V

7V

10V

11V

13V

14V

15Vl6V

xm>19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

0 W€ST COAST T€CHNICAL

LE ID F0434

ID 20797V5

I N J E C T E D 9 R a i

ID DFTPP 1250 VOA 113

. FACTOR

•Ales

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dlchloroethane


1,1,2,2-tetrachloroethane

chloroethane

;x^te(^x<x^<xOT«m^xmi©txxxx>2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

. 56RVIG

ug/1

ND

ND

ND

ND

ND

N D*

N D

ND

ND

ND;xxxxx

Nn*

NnNDNnN DMn34

NnND

ND

ND

ND

ND

ND*

[w ,ND""

E I N C .

SAMP

LAB

DATE

DATE

STD• ± LJ

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P108P

109PHOPHIP

112P

113P

* = I

(pe

ND =.'- -'-

INDUSTRIAL CATEGORY

LE ID F0434 i^

ID 20797 tracer 2196, 2197

EXTRACTED ^ -,Q^

INJECTED 2-3-81,D tracer 2194L \J

. FACTOR 50

cides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4 , 4 ' - D D E

4 , 4 ' - D D D

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

-ess than 10 ug/1

'sticides less than 5 ug/1)

Not detected

Not confirmed by GCMS

^/)

ug/1

0.1**3.0**

NDQ\ ND

—(M———^ ND

^- ND

0 ND0 ND

ND

ND0.2**

ND

ND

0.7**1.2**

1.0**

0.8**

ND

ND

N D

ND

ND

ND

ND

ND

88V vinyl chloride

(K'101890

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No:_ -2£-Sample Number

F0434

COMPOUND

Benzene - d6


Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-D8

A. SURROGATE

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

S P I K E RESULTS

C o n e . ( u g / 1 )

54

51

55

27

ND

84

104

131

(SurrogaSpike

Added ( u g / 1 )

50

50

50

142

103

98

100

102

tes on ly)i

Recovery

lOR

m?no

1<&t?p>

8^

loIZ——or—i2b

B . TENTATIVELY IDENTIFIED COMPOUNDS

1.2 ^

3.

4.

5.

6.

7.

8.

9.

10.

11.

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

U N K N O W N


2 , 2 , 2 - T R I C H L O R O E T H A N O l

3 , 3 , 3 - T R I C H L O R O - t -

P R O P E N E

U N K N O W N

U N K N O W N

U N K N O W NU N K N O W N

U N K N O W N

U N K N O W N

U N K N O W ND I E T H Y L PHTHALATE

U N K N O W N

U N K N O W N

FRACTION

VOA #42

VOA #185

. VOA #303

B / N #75

A C I D #97

A C I D #113

'\CID tf l^A C I D fl'147

A C I D #165

A C I D #177

A C I D fM86A C I D #191

A C I D #199

A C I D #243

% Max imum Score Attained

Mass Matching Rout ine : FIT(specify)

NO GOOD FIT

854

801

932

NO GOOD FIT

NO GOOD FIT

,. .-Nfr-GOQD-W———————————NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT921

NO GOOD F IT

NO GOOD FIT

c^SAMI

LAB

DATI

DATI

STD

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base

1B

5B8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

3 W€ST COAST TECHNIQ

'LE ID F0435

ID 20797A6

; EXTRACTED 1-31-81

I I N J E C T E D 2-1R-81ID DFTPP1258 PHEN308

: FACTOR 1000

Compounds

2 ,4 , 6-trlchlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

'/Neutral Compounds

acenaphthene

benzidine


hexachlorobenzene

hexachloroethane


2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1, -dichlorobenzene3.3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene


(as azobenzene)

f luoranthene

\LS€RVI(

ug/l

N D

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

N0

ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

:e INC.SAMP

LAB

DATE

DATE

STD :

CONC

Base/

41B

42B

43B

52B

53 B

54 B

55B56B61B62B

63 B

66 B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80 B

81B

82B

83B

84 B

INDUSTRIAL CATEGORY

LE ID F0435

ID 20797B5

EXTRACTED 1-30-81

INJECTED 2-2R-R1[D DFTPP1266 .BNSTD363

FACTOR 1000

/Neutral Compounds ui


bis(2-chlorolsopropyl) ether


hexachlorobutadiene

hexachlorocyclopentadiene |sr

isophorone F^

naphthalene ''~"o

nitrobenzene








diethyl phthalate

dimethyl phthalate


benzo(a)pyrene

3.4-benzofluoranthene

benzo(k) f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene


indeno( 1,2,3-cd)pyrene

pyrene

?/1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND*

**

NDND

ND

ND

ND

N D

N DNDND* —,.

NDNO* —

N D

ND*

;1)

40B 4-chlorophenyl phenyl ether ^p 129B 2,3,7,8-tetrachlorodibenzo-

p-dioxin

( 1 ) UNRESOLVED COMPOUNDS

£^j3 W€ST COAST TECHNICAL

S A M P L E ID pn4^R

L A B ID ^Q^Q^^

DATE INJECTED 2-9-81

STD ID nFTPP1?..S1 VOA114

CONC. FACTOR

Volatiles

2V acrolem

3V acrylonitrlle

4V benzene

6V carbon tetrachloride

7V chlorobenzene



13V 1,1-dlchloroethane

14V 1,1, 2-trichloroethane

15V 1,1,2,2-tetrachloroethane

l6V chloroethane

xmxx^^xowxOTex)w^xm^xxxx19V 2-chloroethylvinyl ether

23V chloroform

29V 1,1-dichloroethylene

30V 1,2-trans-dichloroethylene

32V 1,2-dichloropropane

33V 1,3-dichloropropylene

38V ethylbenzene

44V methvlene chloride

45V methyl chloride

46V methyl bromide

47V bromoform

48V dichlorobromomethane49V trichlorofluoromethane

50V dichlorodifluoromethane

51V chlorodibromomethane

85V tetrachloroethylene

86V toluene

87V tr ichloroethylene

88V vinyl chloride

SERVIC

ug/1

ND

NOND

ND

N D

ND*

ND

ND

ND

NDX X X X X

NnND

ND

NDNn

N ONn30

NnND

ND

NDNDND

ND

ND

(W )

ND

ND

€ INC. INDUSTRIAL CATEGORY

SAMPLE ID F0435LAB ID 20797 trace#2199

DATE EXTRACTED 1-30-81

DATE INJECTED 2-4-81

STD ID TRACE ^2198

CONC. FACTOR 50

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4 , 4 ' - D D E

94P 4 , 4 ' - D D D


96P beta-endosulfan


98P endrin

99P endrin aldehyde

100P heptachlor


102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected


ug/1

NOND

ND

C\J ND

^ ND

^ N D

^ND

O N D

ND

ND

ND

ND

ND

ND

ND

N D

ND

N D

ND

N D

ND

ND

ND

ND

ND


QC Report No:Sample Number

F0435

COMPOUND

Benzene - d6


Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

A. SURROGATE

Fraction

VGA

VGA

VOA

ACID

ACID

B/N

B/N

B/N

S P I K E RESULTS

C o n e . ( u g / 1 )

52

51

51

ND

NO

75

93

124

(SurroqaSpike

Added ( u q / 1 )

50

50

50

142

103

98

100

102

tes only)%

Recovery

104

102

102

0

(P

^93-

1223————0—


1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

11.

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

T E T R A H Y D R O F U R A N


U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N


U N K N O W N

FRACTION

VOA #117

VOA #185

B / N #540

A C I D #84

A C I D #10^

A C I D ^E

A C I D #13E

A C I D #14£

A C I D #15^

A C I D #166

A C I D #17£

A C I D #192

ACID #20S

% Maximum Score Attained

Mass Match ing Rout ine : FIT(spec i fy)

981

926

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

923

NO GOOD F I T

.... -.- , -n^i m

r—" ..•J

SAMP

LAB •

DATE

DATE

STD 1

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

l8B

20B

25 B

26B

27B

28B

35B

36B

37B

39B

40B

3 WEST COAST TECHNICAL;

LE ID F0436

^D 9n7Q7Rfi

EXTRACTED ] - - ^ ] - o - ^

INJECTED 2-16-81

^ nFTPPISP.fi PHEN318

FACTOR mnn

Compounds UJ


p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol


pentachlorophenol

phenol

'Neutral Compounds

acenaphthene

benzidine


hexachlorobenzene

hexachloroethane


2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinltrotoluene

2,6-dlnitrotoluene


(as azobenzene)

f luo ran thene

4-chlorophenyl phenvl ether

5€RVI

^/lND

ND

ND

ND

N D

ND

ND

ND

N D

N D

ND

ND

ND

N D

ND -

ND

N D

ND

ND

ND

ND

ND

ND

ND

N D

N D

ND

C€ INC.

SAMP

L A B

DATE

DATE

STD

CONC

Base,

41B

42B

43B

52B

53B

54B

55B

56B

61B

62B

63B

66B

. 67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79 B

SOB

81B

82B

83 B

84 B

129B

p-dic

INDUSTRIAL CATEGORY

LE ID F0436ID 20797B6

EXTRACTED 1-30-81

I N J E C T E D 2-25-81

ID DFTPP1266 BNSTD363

FACTOR mnn

/Neutral Compounds u^




hexachlorobutadiene '=j-

hexachlorocyclopentadiene ^, m

isophorone————c——————————————————————^—

naphthalene c^

nitrobenzene 0

N-nitrosodi methyl a mine






di-n-octyl phthala te

diethyl phthalate

dimethyl phtha la te

benzo(a) anthracene

benzo(a)pyrene


benzo(k) f luoran thene

chrysene

acenaphthylene

anthracene

benzo(ghl )pery lene

fluorene

phenan threne


indeno( 1,2,3-cd )pyrene

pyrene


ixin

O"*!

iZLND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND*

ND*

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

N D

ND

ND

ND

ND

Nn

01895

cSAMP

LAB

DATE

STD

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

mxx19V

23V

29V

30V

32V

33V

38V

44V

45V46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

3 WEST COAST TECHNICAL

LE ID F0436

ID 9n7Q7Vfl

I N J E C T E D 2-9-81

ID DFTPP1251 VOA114. F A F T n R

iles

acrolein

acrylonitrile

benzene


chlorobenzene

1,2-dichloroethane


1,1-dichloroethane

1,1, 2-trichloroethane


chloroethane

;xyx$(to^x<w<x9wx)Wx^)^xxxx2-chloroethylvinyl ether

chloroform



1,2-dichloropropane


ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform





tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

sepvii

ug/l

N D

ND

N D

N D

ND

N D*

N D

ND

ND

ND

X X X X X

NnNn

NnNnNnNnNn

31

NnND

ND

ND

ND

ND

N D

ND

^MD''1

ND

ND

C6 INC. INDUSTRIAL CATEGORY

SAMPLE ID F0436

LAB ID 907Q7 tT-^pA 77^

DATE EXTRACTED 1-30-81

DATE INJECTED .2-4-81STD ID trace* 2204

CONC. FACTOR 100

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4 .4 ' -DDE

94P 4 ,4 ' -DDD


96P beta-endosulfan


98P endrin

99P endrin aldehyde

100P heptachlor


102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232-

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/l

(pesticides less than 5 ug/l)

ND = Not detected


ug/l

NPND

N D

LU ND

^ N DN \

ND

O N D

O N D

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

N D

ND

ND

ND

N D

•

W€5T COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 26Sample NumberF0436

COMPOUND

Benzene - d6


Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

A. SURROGATE

Fract ion

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

SPIKE RESULTS

C o n e . ( u g / 1 )

50

47

51

ND

ND

84

99

132

(SurroqaSpike

Added ( u q / 1 )

50

50

50

142

103

98

100

102

tes only)<yh

Recovery

100

94

102

&vD

^

8^9^-

12?


1.2.

3.

4.

5.

6.

7.

8.

9.

10.

11.

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N

U N K N O W N


U N K N O W N

FRACTION

VOA #115

B/N #77

B / N #540

A C I D #80

ACID #97

A C I D #113

ACID #125

A C I D #147

A C I D #151

A C I D #165

ACID #177

A C I D #191

A C I D #243


Mass Match ing Rout ine : FIT(specify)

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD F I T

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

928

NO GOOD FIT

c-"•-—-a

SAMP

LAB

DATE

DATE

STD I

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36 B

37B

39B

3 WEST COAST TECHNK

LE ID F0437

ID 9n7q7&R

EXTRACTED 1-31-81

I N J E C T E D 2-16-81

D nFTPPIP.sa PHF.N.^nS

FACTOR ioo0

Compounds


p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol


pentachlorophenol

phenol

''Neutral Compounds

acenaphthene

benzidine


hexachlorobenzene

hexachloroethane


2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene


2,4-dinitrotoluene

2,6-dlnitrotoluene

1,2-diphenylhydrazlne

( a s azobenzene)

f luoranthene

CAL S€RVI

ug/1

^ 166

522

ND

^ 73fi

ND

ND

ND

ND

N D

ND

*

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

ND

ND

ND

N D

ND

ce INC.SAMP

LAB

DATE

DATE

STD

CONC

Base

41B

42B

43B

52B

53B

54B

55B

56 B

61B

62B

63B

66B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76 B

77B

78B

79B

80 B

81B

82B

83B

84B

INDUSTRIAL CATEGORY

LE ID F0437

ID 2n7-q7B7

EXTRACTED- 1-30-81

I N J E C T E D 2-25-81

ID DFTPP1266 BNSTD364

FACTOR mnn

/Neutral Compounds u




hexachlorobutadiene ^~K\

hexachlorocyclopentadiene^-

isophorone ^-

naphthalene 0

nitrobenzene ~

N-nitrosodi methyl a mine







diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene


benzo(k) f luoran thene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

d ibenzo (a ,h )an th racene

indeno( 1,2,3-cd )pyrene

pyrene

g/1

ND

ND

ND

ND

ND

ND

ND

ND

ND*

ND

^•**

*

*

ND

NnNDND

NDND

ND

^(1)Nn

ND

Nn*

^OB 4-chlorophenyl pheny l ether ^p 129B 2,3,7,8-tetrachlorodibenzo-

p-dioxin______________________NQ_

( 1 ) UNRESOLVED COMP^y^ggQ

i er,

SAMP

LAB

DATE

STD

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

mx>19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

P W€ST COAST TECHNICA

LE ID NO SAMPLES

ID

INJECTED

ID

. FACTOR

iles

acrolein

acrylonitrile

benzene


chlorobenzene

1,2-dichloroethane

1,1,1-trlchloroethane

1,1-dichloroethane



chloroethane

c )^^t(wwmixxx x KX m x x)2-chloroethylvinyl ether

chloroform



1,2-dichloropropane


ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform




chlorodibromome thane

tetrachloroethvlene

toluene

trichloroethylene

vinyl chloride

L56RV

ug/1

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

( X X X X X X

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA.

< NA

NA"

NA

^ice INC.SAMP

LAB

DATE

DATE

STD

CONC

Pesti

89P

90 P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = I

(pe

- ND =

'"' '''•' =

INDUSTRIAL CATEGORY

LE ID F0437

ID 20797 TRACE ^2205

EXTRACTED 1/30/81

INJECTED 2/4/81

ID TRACE #2204

. FACTOR 100

cides u

aldrin

dieldrin

chlordane

4 ,4 ' -DDT c0

4 , 4 ' - D D E rn——;———————————————————^,

4 .4 ' -DDD

alpha-endosulfan 0

beta-endosulfan <—^

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

. PCB-1248

PCB-1260

PCB-1016

toxaphene

-ess than 10 ug/1

•sticides less than 5 ug/1)

Not detected


g/1

ND

ND

ND

ND

NDNDNDNDNDNDN DNON DNDNDN DNnNnNnND

ND

N DNDN DN D

17605 Fabrica Way Suite D Cerntos California 90701 2 1 3 , 921-9831 07101899



F0437

COMPOUND

Benzene - d6


Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

A. SURROGATE

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

: S P I K E RESULTS

C o n e . ( u g / 1 )

•

-

127

13

60

70

75

(SurrogaSpike

Added ( u q / 1 )

142

103

98

100

102

tes o n l y )°/h

Recovery

..

89

13^

62^

70^-

740<">


1.

2 ^

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15 .

16 .

17 .

18.

19.

20.

CAS # COMPOUND NAME

llNi^niAlM

?,fi-nTrm npnpHFNni

UNKNOWN

2-BROMO-4-CHIOROPHFNni

UNKNOWN

4-CHLOROPHENOL

2,4,5-TRICHLOROPHENOL

UNKNOWN

3,5-DICHLOROPHENOL

UNKNOWN

CHLOROPHENOL

METHYLPHENOL

CHLOROPHENOL

DICHLOROMETHOXYBENZENE

TRICHLOROMETHOXYBENZEF

UNKNOWN

UNKNOWN

UNKNOWN

FRACTION

AfTr i *qfi

A C T n ^ 1 ? 4

ACTri # 1 4 6

ACTn # 1 R 2

ACID # 1 5 7

ACID # 1 7 3

ACID # 1 8 5

ACID # 1 9 9

ACID #233

ACID #321

B/N # 1 0 4

B/N # 1 3 1

B/N #185

B/N # 2 1 1

IE B/N #263

B/N #291

B/N #297

B/N #338


Mass Matching Routine: FIT(specify)

NO noon FITwa.

NO Rnnn FIT

8RR

NO GOOD FTT

996

997

NO GOOD FIT

979

NO GOOD FIT

970

950

990

924

970,

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

———————————————————n>"«^ n

r - "^ . iSAMP

LAB

DATE

DATE

STD 1

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

l8B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

3 WEST COAST TECHNICAL

LE ID F0438

ID 20797A9

EXTRACTED i ^ i a i

INJECTED 2-16-81

^ D DFTPP1258 PHEN308

FACTOR mnn

Compounds u


p-chloro-m-cresol

2-chlorophenol

2, 4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol


pentachlorophenol

phenol

^Neutral Compounds

acenaphthene

benzldine


hexachlorobenzene

hexachloroethane


2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1 ,^-dichlorobenzene


2, Zt-dinitrotoluene

2,6-dinitrotoluene


(as azobenzene)

f luoranthene

^-chlorophenyl phenyl ether

SGRVI

g/116"

ND

ND

32 '-'

ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

N D

ND

ND

ND

N D

ND

ND

ND

ND

N D

ND

ce INC.SAMPI

LAB I

DATE

DATE

STD I

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56 B

61B

62B

63B

66B

67B

68 B

69B

70B

71B

72B

73B

74B

75B

76 B

77B

78B

79B

SOB

81B

82B

83B

84B

129B

p-dio;

INDUSTRIAL CATEGORY

.E ID F0438

D 20797B8

EXTRACTED i on 01

INJECTED 2-25-81

D DFTPP1266 BNSTD364

FACTOR mnn

Neutral Compounds ue


bis(2-chlorolsopropyl) ether


hexachlorobutadiene

hexachlorocyclopentadiene 0

isophorone ';;: "

naphthalene ^-nitrobenzene /-,.

N-nltrosodimethylamine o





di-n-butyl phthalate i

di-n-octyl phthalate ''

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a )pyrene


benzo ( k ) fluoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

d ibenzo(a ,h )an th racene


pyrene


<in

sZlND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND15"*

^ir •

N D

ND

ND

ND

ND

NDNDND

NDNDNDNDND

NnND

Nn07101901

W€5T COAST TECHNICAL 56RVIC6 INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

STD •

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15Vl6V

x^o19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

LE ID NO SAMPLESID

INJECTED

ID

. FACTOR

lies

acrolein

acrylonitrile

benzene


chlorobenzene

1,2-dichloroethane


1,1-dichloroethane



chloroethane

:»X§IXKKXi[M^K^lQXXXBeXXX:

2-chloroethylvinyl ether

chloroform



1,2-dichloropropane


ethylbenzene

methvlene chloride

methvl chloride

methvl bromide

bromoform

dichlorobromo methane




tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

ug/1

NANAHA

NA-TTO——

NANA

NANA

NA

NA

KXXXXNA

NANA

M2\

NANA

NANA

NANAMA

NANANA

NA/"ITA>VJSIA >

NA

NA

SAMP

LAB

DATE

DATE

STD

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = 1

(pe

ND =-;.- * ^

LE ID Ffu-iR

ID 20797 trace# 2206

EXTRACTED 1-30-81

INJECTED 2-4-81

ID trace 2204

. FACTOR 100

cides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4 ,4 ' -DDE

4,4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

-ess than 10 ug/1

•sticides less than 5 ug/1)

Not detected


ug/1

NDNDMD

^ND^D

ND^—

9in^D

ND

NnNDND

NDNDND

NDND

N D

NDNDND

NDND

MD

ND

17605 Fabnca Way. Suite 0 Cerntos, Cal i fornia 90701 2 1 3 9 2 1 - 9 8 3 1


QC Report No:_ 26Sample Number

F0438

COMPOUND

Benzene - d6


Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

A. SURROGATE

i

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

S P I K E RESULTS

C o n e . ( u q / 1 )

-

-

-

142

67

76

84

87

(SurrogaSpike

Added (uq /1 )

-

-

142

103

98

100

102

tes on ly)%

Recovery

-

103

^^

84-

8?

B. TENTATIVELY IDENTIFIED COMPOUNDS

1.

2,

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

UNKNOWN

UNKNOWN

2.6,-DICHLOROPHENOL

UNKNOWN

UNKNOWN

UNKNOWN


UNKNOWN

UNKNOWN

3,3,3-TRICHLORO-t-

PROPENE

DIETHYLPHTHALATE

UNKNOWN

FRACTION

Ar.Tn #97

ACID # 1 1 2

ACID # 1 2 5

ACID # 1 4 6

ACID # 1 5 1

ACID # 1 7 5

ACID # 1 8 6

ACID #207

ACID #272

B/N #73

B/N # 3 1 9

B/N #337



NO finnn FTT

NO GOOD FIT

995

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

953

NO GOOD FIT

NO GOOD FIT

'

927

888

NO GOOD FIT

E:gj

SAMP

LAB

DATE

DATE

STD 1

CONC

Acid

21A

22A

24A

31A

3U

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

^OB

9 WEST COAST TGCHrs

LE ID F0439

ID 20797/

EXTRACTED 1/31/?

INJECTED 2/16/(

[D DFTPP1258 1

FACTOR 1000

Compounds

2, U, 6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol


pentachlorophenol

phenol

^Neutral Compounds

acenaphthene

benzidine

1, 2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane


2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3.3'-dichlorobenzidine

2,^-dinitrotoluene

2,6-dinltrotoluene


(as azobenzene)

fluoranthene

4-chlorophenyl phenyl

11CALS6RVK

\10

3131

^N01.309

ug/1

*

ND

ND

30

ND

ND

ND

ND

ND

ND

ND

ND

ND

77

ND

ND

N D

ND

15

39

526

ND

ND

ND

ND

N D

ether ND

C:6 INC.

SAMP]

LAB I

DATE

DATE

STD I

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56B

61B

62B

63B

66B67B68B69B

70B

71B

72B

73B

74B

75B

76 B

77B

78B

79B

80B

81B

82B

83B

8^B

129B

p-dio:

INDUSTRIAL CATEGORY

-E ID F0439

•D 20797R9

EXTRACTED 1/30/81

INJECTED 2/26/81

D DFTPP1267 BNSTD365

FACTOR 1000

Neutral Compounds u$




hexachlorobutadiene 1 \

hexachlorocyclopentadiene ': ", m

isophorone———-——————————————————^~"

naphthalene Q

nitrobenzene 0



N-nitrosodi-n-propyl-amine





diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3, -benzofluoranthene

benzo(k)f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

d ibenzo(a ,h )an thracene


pyrene


<in

i/1

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

NO*

N D*

ND*

ND

ND

ND

ND

NDNDNDNDNDNDNDND

NDND

m

fT .T .r , • ' ' " • •' -—^

SAMP

LAB

DATE

STD

CUNC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

l6V

xm>19V23V

29V

30V

32V

33V

38V44V

45V46V47V

48V

49V

50V51V85V

86V

87V

88V

3 WGST COAST TECHNICAL!

LE ID F0439

ID 20797V9

INJECTED 2/9/81

ID nFTPPl9Rl V O A l l d

. t -ACTOR

:iles

acrolein

acrylonitrile

benzene


chlorobenzene

1,2-dichloroethane


1,1-dichloroethane



chloroethane

(XimfcX%X<X«<X»»Xl^Xm^XXXX)2-chloroethylvinyl ether

chloroform

1,1-dlchloroethylene


1,2-dichloropropane


ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethanetrichlorofluoromethane



tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

56RVK

ug/l

ND

ND*

ND

419ND

*

ND

ND

ND

ND( X X X X

ND

NDNR

Nn

Nn

NnNn

30

NnND

ND

NDNDNDND

ND*

ND

ND

:6 INC.

SAMP

LAB

DATE

DATE

STD •

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P96 P

97P98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = I(p.

ND =;'? * ^

INDUSTRIAL CATEGORY

LE ID F0439

ID 20797 TRACE

EXTRACTED 1/31/81

INJECTED 2 / f i /R l

ID TRACE #2199

. FACTOR 100

cides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4,4 ' -DDE

4,4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016toxaphene

.ess than 10 ug/l

'sticides less than 5 ug/l)

Not detected


#2198

ug/l

NnND

ND

^r ND^ ND

^ N D

^ 1.0**

O N D

ND

ND

ND

ND

0.9**

ND

ND

ND

0.3**

ND

ND

ND

N D

ND

ND

. ND

ND

^S W€5T COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3


F0439

COMPOUND

Benzene - d6


Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

A. SURROGATE

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

: SPIKE RESULTS

Cone. (ug /1)

52

49

50

ND

ND

85

102

136

(SurrogaSpike

Added (ug /1 )

50

50

50

142

103

98

100

102

tes only)%

Recovery

104

98

100

0-^in L

———^-.8^

1&?

13?

B. TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5./-

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

TRIDECANE

UNKNOWN

5-PROPYLTRIDECANE

TETRACHLORO BENZENE

HYDROCARBON

HYDROCARBON

HYDROCARBON

HYDROCARBON

4-CHLOROPHENOL

CHLOROBENZENE

HYDROCARBON

HYDROCARBON

1,2,4,5-TETRACHLORO-

BENZENE

HYDROCARBON

UNKNOWN

UNKNOWN

UNKNOWN

UNKNOWN

FRACTION

ACID #B9

ACID #76

ACID #95

ACID # 1 0 0

ACID # 1 0 9

ACID # 1 1 4

ACID # 1 4 0

ACID # 1 5 1

ACID # 1 7 5

B/N #63

B/N # 2 1 5

B/N #230

B/N #239

B/N #245

B/N #285

B/N #327

B/N #354

B/N #566


Mass Matching Routine: FITspecify)

947

NO Gnnn FTT933

979

855

918

9 1 9

866

997

994

GENERAL FIT

GENERAL FIT

990

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

^P> WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMI

LAB

DATI

DATI

STD

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base

1B

5B

8B

9B

12B

18B

20 B

25B

26B

27B

28B

35B

36B

37B

39B

40B

^LE ID F0440

ID 2n7q7A11

:; EXTRACTED 1-31-81

:; INJECTED 2-16-81Ip DFTPP1258 PHENC

; FACTOR mn

Compounds

2,4,6-trlchlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol


pentachlorophenol

phenol

'/Neutral Compounds

acenaphthene

benzidine

1,2,4-trlchlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ethel

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene


2,4-dinitrotoluene

2,6-dinitrotoluene


(as azobenzene)

fluoranthene


)L309

u

' /

'

ether

g/1

7^

ND

ND

45

ND

ND

ND

ND

N D

N D

ND

ND

ND*

ND

ND

ND

ND*

ND

10

ND

ND

ND

ND

ND

ND

SAMP

LAB

DATE

DATE

STD

CONC

Base,

41B

42B

43 B

52B

53 B

54 B

55B

' 56B

61B

62B

63B

66 B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80 B

81B

82B

83 B

84B

129B

p-dic

LE ID F0440

ID 20797B10EXTRACTED 1-30-81

INJECTED 2-26-81Ip DFTPP1267 BNSTD365

FACTOR i n n n

/Neutral Compounds u$




hexachlorobutadiene \D

•yhexachlorocyclopentadiene ^

isophorone ^-

naphthalene 0

nitrobenzene 0








•diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene



chrysene

acenaphthylene

anthracene

benzo(ghi)pery'!'ene

fluorene

phenanthrene

dibenzo(a ,h)anthracene


pyrene


ixin

O^'lOl^

^1ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

* ^

ND*

ND*

ND

NDND

ND

ND

NO

ND

ND

ND

N D

ND

ND

NnND

Nn07

aggjSAMP

LAB

DATE

STD

rnNC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

xmx19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

9 WEST COAST T6CHNICAI

LE ID F0440

ID 20797V15

INJECTED 2-9-81

ID DFTPP1251 VOA115r' A^mo

:iles

acrolein

acrylonitrile

benzene


chlorobenzene

1,2-dichloroethane


1,1-dichloroethane



chloroethane

:X^X$(to^X<X«<XWX)^X5<^)t-mXXX:2-chloroethylvinyl ether

chloroform



1,2-dichloropropane


ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform





tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

- SGRVICt

ug/1

ND

NON'D

ND*

ND*

ND

ND

ND

NDX X X X X X

Nn

Nn

NnNnNnNn

Nn38

NDND

ND

ND

ND

ND

ND

•NO

( ND - x

"^Tr-"ND

E I N C .

SAMP

LAB

DATE

DATE

STD<»J A L/

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = I

(P<=ND =** ^

INDUSTRIAL CATEGORY

LE ID F0440

ID 20797 trace* 2203EXTRACTED 1-31-81

INJECTED 2-6-81

ID traced 2203

. FACTOR 100

cides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4,4 ' -DDE

4.4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016 .

toxaphene

.ess than 10 ug/1


Not detected


ug/1

NnND

N D

r-ND

^"ND—TV • •

ND

OND

OND

ND

ND

ND

ND

ND

ND

ND

N D

ND

N D

ND

ND

N D

ND

ND

ND

ND


QC Report No:_ 26Sample Number

F0440

COMPOUND

Benzene - d6


Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

A. SURROGATE

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

- SPIKE RESULTS

Cone.(ug/1)

54

51

50

ND

ND

98

1 1 5

149

(SurrogaSpike

Added (uq /1 )

50

50

50

142

103

98

100

102

tes only)%

Recovery

108

102

100

0CO^

10l(h

ns-14P


1.

2^

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

UNKNOWN

TETRAHYDROFURAN

UNKNOWN

CHLOROBENZENE

FRACTION

VOA #43

VOA # 1 1 5

B/N #62



NO GOOD FIT

988

NO GOOD FIT

988

07101909

^S WeST COAST TECHNICAL S6RV1CG INC. INDUSTRIAL CATEGORY

SAMF

LAB

DATI

DATE

STD

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A60A

64A

65A

Base

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B28B35B36B37B

39B

40B

'LE ID F0441

ID 2n7q7A1.-i

: EXTRACTED 1-31-81

: INJECTED 2-22-81ID DFTPP1263 PHEN3

: FACTOR 10

Compounds

2,4.6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol


pentachlorophenol

phenol

/Neutral Compounds

acenaphthene

benzidine


hexachlorobenzene

hexachloroethane

bis (2-chloroethyDethei

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1, 4-dichlorobenzene3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene


(as azobenzene)

f luoranthene


10

^

• ,'•-J

eth

ug/1

.wnND

5078

9148

N D

NO

ND

ND

N D

ND

574

NDND

46

NDND

ND

ND*

ND*

ND

ND

ND

ND

NDer ND

SAMP

LAB

DATE

DATE

STD I

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56 B

61B

62 B

63B

66B

67B

68B

69 B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80B

81B

82B

83B

84 B

129B

p-dio

LE ID F0441

ID 9n7Q7-Rn

EXTRACTED 1-30-81

INJECTED 1-26-81[D DFTPP1267 BNSTD365

FACTOR 1000

^Neutral Compounds us




hexachlorobutadiene 0^-

hexachlorocyclopentadiene ':::^• i, tr\isophorone

naphthalene c-»

nitrobenzene 0








diethyl phthalate ^

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene



chrysene

acenaphthylene

anthracenebenzo(g hi )perylene

fluorene

phenanthrene

d ibenzo(a ,h )an th racene

indenod ,2,3-cd)pyrene

pyrene

2,3.7,8-tetrachlorodibenzo-

xin

^/l

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND*

ND

**

MD

ND

ND

ND

NONDNDND* —i

NDND* ——

NnNDND

Nn

Cde-" lu t im

Com-pound

W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

STD

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

l6V

xmx19V

23V

29V

30V

32V

33V

38V

44V

45V

^6V

47V

48V

49V

50V

51V

85V

86V

87V

88V

LE ID F0441

ID 7n7q7vnINJECTED 2-9-81

ID DFTPP1251 VOA114

. f A C l U K

ties

acrolein

acrylonitrlle

benzene


chlorobenzene

1,2-dichloroethane


1,1-dichloroethane



chloroethane

;X^X$(k<X%X««<X^XTOteX%mXXX

2-chloroethylvinyl ether

chloroform



1,2-dichloropropane


ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform


trichlorofluoro methane



tetrachloroethylene

toluene (

trichloroethylene

vinyl chloride

ug/1

ND

ND

84

ND

*

ND*

ND •

NDND

ND

X X X X X

ND*

11

NnND

ND13

31

NDND

ND

ND

ND

ND

ND

-W--

30305\

' ^L-^

ND

SAMP

LAB

DATE

DATE

STD :

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = 1

(pe

ND =** ^

LE ID F0441

ID ?.n7Q7 tr-^p* 77.07 ?.?nR

EXTRACTED 1-31-81

INJECTED 2-9-81

ID fr^rpa ?.2nfi. FACTOR 100

cides

aldrin

dieldrin

chlordane

4,4 '-DDT

4.4 ' -DDE

4,4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

.ess than 10 ug/1


Not detected


ug/1

NnND

ND

^ ND

^ ND

<- ND

° N D

^ ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

N D

ND

ND

ND

NDNDND

W€5T COAST TECHNICAL S6RVICG INC.ORGANICS ANALYSIS DATA SHEET - Page 3


F0441

COMPOUND

Benzene - d6


Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

A. SURROGATE

Fraction

VGA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

SPIKE RESULTS

C o n e . ( u g / 1 )

BO

45

44

134

74

117

112

153

(SurrogaSpike

Added (ug /1)

50

50

50

142

103

98

100

102

tes only)"ih

Recovery

100

90

88

94

^———tPi—1-^

. Tk2-

1^


1.

2^

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15 .

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

BUTANAL

CYCLOHEXANE

METHYCYCLOHEXANE

1-CHLORO-2-METHYL-

BENZENE

2-ETHYL-1-HEXANOL

2-METHYLPHENOL

DICHLOROMETHOXYBENZENE

I,2,3-TRICHLORO-4-METHO

BENZENE

UNKNOWN

UNKNOWN

UNKNOWN

UNKNOWN

XYLENE

2,6,-DICHLOROPHENOL

4-CHLOROPHENOL


UNKNOWN

FRACTION

VOA # 1 4 0

VOA # 1 7 1

VOA #272

B/N #97

B/N # 1 1 7

B/N # 1 5 1

B/N #237

<Y-

B/N #290

B/N #322

B/N #470

B/N #499

B/N #565

B/N #59

ACID #144

ACID #187

ACID # 1 9 9

ACID #424



977

972

987

995

951

980

979

998

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

984

996

997

980

NO GOOD FIT

07101912, f^r~i^ fyfrw <-» '

results of samples collected by adpc&e for epa in ... · region 6 environmental protection...

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